柔性液晶微透镜阵列的制备与性能研究

针对集成成像视场角狭小的问题,设计并制备了一种柔性圆孔驱动电极控制液晶分子偏转的可弯曲和焦距可调的柔性液晶微透镜阵列。利用光刻技术在柔性ITO基板表面刻蚀并形成规则的圆孔阵列电极,旋涂工艺制备柔性聚酰亚胺(PI)膜层,PI膜层经60℃加热5 min后,再利用等离子体在功率630 W条件下处理5 min固化成PI取向层。利用液晶盒成盒工艺将上、下基板组装成液晶透镜,研究未弯曲和弯曲曲率半径7.5 cm条件下液晶微透镜阵列的光学性能。实验结果表明,所制备的液晶透镜在未弯曲和曲率半径为7.5 cm的情况下均可实现聚焦功能,且液晶微透镜阵列的干涉圆环均匀,聚焦光斑小。在驱动电压3~5.3 Vrms下,弯曲曲率半径为7.5 cm的液晶微透镜阵列焦距可调的范围为0.43~1.05 mm。     

基于马铃薯叶片光纤光谱信息的晚疫病患病程度预测

针对马铃薯晚疫病害的早期检测和防治问题,利用光谱技术对马铃薯晚疫病叶片过氧化物酶(POD)活性进行预测,并基于POD酶活性实现了马铃薯晚疫病的患病程度预测.采集和测定处于不同温湿度及接菌时间的马铃薯叶片样本的光谱反射率和POD酶活性,选用中心化(MC)预处理方法以消除原始光谱数据的误差.为降低模型复杂程度,利用随机青蛙...     

隆回富硒区山银花不同花期硒分布规律研究

通过分析山银花不同花期硒含量,探讨了山银花中硒的积蓄规律与土壤硒之间的关系。选择湖南省隆回县小沙江地区加油站北和岩背村两处土壤硒含量分别为0.968 mg/kg和0.837mg/kg的山地,种植灰毡毛忍冬的两个不同品种:白云一号和金蕾一号,在花期内连续采收绿蕾期、白蕾期、白花期和金花期样本,脱水后,用电化学法测定硒含量。结果表明,白云一号和金蕾一号的绿蕾期、白蕾期、白花期和金花期硒平均含量分别为0.111、0.191、0.191、0.295 mg/kg和0.146、0.260、0.272、0.363 mg/kg,金蕾一号的硒积蓄能力优于白云一号。结论是富硒区山银花中硒的积蓄量与品种、花期密切相关,但与土壤中硒含量无明显相关性。     

o-ZrW_(1.6)Mo_(0.4)O_8:A Novel Orthorhombic Intermediate Phase Formed During the Synthesis of the Negative Thermal Expansion Cubic ZrW_(1.6)Mo_(0.4)O_8 Material by the Precursor Dehydration Route

Negativethermalexpansion (NTE)materialshavere ceivedconsiderableattentioninrecentyears ,1 6 especiallythecubicphasesZrW2 O8(c ZrW2 O8)andZrMo2 O8(c ZrMo2 O8) .TheseparticularmaterialsundergoisotropicNTEbehavioroverawidetemperaturerange ,0 3Kto10 5 0Kand 1378Kto 15 30KforZrW2 O81,2 and 0to 6 6 0KforZrMo2 O8,respectively .7c ZrMo2 O8possessesbenefi cialintrinsicproperties7 9overZrW2 O8,suchaslowerden sityandlowerphasetransitiontemperature ,butitstemper aturerangeforNTEisnarrowerth…     

o-ZrWl.6Mo0.408： A Novel Orthorhombic Intermediate Phase Formed During the Synthesis of the Negative Thermal Expansion Cubic ZrWl.6Mo0.4O8 Material by the Precursor Dehydration Route

The mechanism of the precursor dehydration route was revealed for the synthesis of NTE c-ZrW1.6Mo0.4O8. The hydrate precursor was dehydrated at 473 K and transformed to a NTE cubic compound above 800 K. A novel intermediate phase o-ZrWl.6Mo0.4O8 occurs between the temperature range of 573-800 K. The XRD pattern of novel intermediate was refined with the structural model of LT-ZrMo2O8 by using Rietveld method.The residuals are Rwp=7.80% and Rp=5.79%. The space group is Pmn21 and the lattice parameters are α=0.5917(4)nm, b=0.7273(4) nm, c =0.9148(6) nm, and Z=2.     

o-ZrW1.6Mo0.4O8·H2O正交相的合成与表征

The precursor ZrW_1.6Mo_0.4O₇(OH)₂(H₂O)₂ was characterized by IR and XRD methods. δ′-ZrW_1.6Mo_0.4O₈ was prepared by careful controlling the annealing conditions from the precursor and was determined to have the formula as o-ZrW_1.6Mo_0.4O₈·H₂O by TG-DSC, IR, and XRD methods. The relation between o-ZrW_1.6Mo_0.4O₈·H₂O and o-ZrW_1.6Mo_0.4O₈ was discussed through variable temperature XRD patterns. Further more, the mechanism of the precursor dehydration was suggested.