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1.
The reaction of 2-(2 pyridytcarbonyl)benzoic acid with thionyl chloride affords an unexpected product of the intramolecular acylation of the pyridine nitrogen atom, namely, 6,11-dioxo-6,11-dihydrobenzo[blquinotizinium chloride. At the same time, 2-(2-quinotylcarbonyl)benzoic acid forms the expected cyclic acid chloride, namely, 3-(2-gitinotyl)-3-chlorophthalide in this reaction. Both compounds acylate ammonia and primary amines, including those with bulky alkyl groups (tert-butyl, 1-adamantyl, and 1,1,3,3-tetramethylbutyl) with the formation of 2-R-3-hydroxy-3-(2pyridyl- or 2-quinolyl)isoindolines. The protonation of the pyridine nitrogen atom of N-(1,1,3,3-tetramethylbutyl)-2-(2pyridylcarbonyl)benzamide, obtained in the open amide form, is accompanied by the closing of the isoindotinone ring; the deprotonation is accompanied by ring opening.Riga Technical University, Riga LV-1048. Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 4, pp. 499–504, April, 1994. Original article submitted March 17, 1994. 相似文献
2.
É. Abele Yu. Popelis É. Lukevits M. Shimanska Yu. Gol'dberg 《Chemistry of Heterocyclic Compounds》1994,30(1):14-19
Alkylation of 2 furanyl- and 2-thienylalkyl ketoximes with alkyl, allyl, and propargyl halides in the two phase catalytic system sol. K2CO3/C6H6/18-crown-6 at room temperature causes the formation of mixtures of E- and Z-isomers of the corresponding O-ethers with yields of 32–74%. Partial E/Z-isomerization takes place during the reaction.Translated from Khimiya Geterotsiklicheskikh Soedinenii, No. 1, pp. 18–23, January, 1994. 相似文献
3.
We consider the radiation from nonoscillating dipoles traveling with constant velocity directed parallel or antiparallel to
the velocity of a homogeneous transparent moving medium. It is assumed that the medium in its rest frame is isotropic and
has no spatial dispersion. We obtain expressions for the radiative energy losses and estimate the polarization energy losses
of electric and magnetic dipoles of different orientations. In particular, it is shown that the energy loss of a source is
negative if it moves in the direction of the medium motion and the source velocity is less than the medium velocity. Estimates
for the energy losses of dipoles in the cases of an electron beam and a flow of a weakly dispersive medium are given.
__________
Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Radiofizika, Vol. 49, No. 6, pp. 502–512, June 2006. 相似文献
4.
Afraimovich É. L. Vodyannikov V. V. Voyeikov S. V. Perevalova N. P. Yakovets A. F. 《Radiophysics and Quantum Electronics》2002,45(10):741-757
Using the COPHASE method and the GPS interferometry method for travelling ionospheric disturbances, we analyze in detail the spatio-temporal properties of travelling wave packets (TWP) of total electron content (TEC) disturbances. The analysis is performed on the example of a clearest TWP manifestation observed in California, USA, in October 18, 2001, using the GLOBDET technique, developed at the Institute of Solar-Terrestrial Physics of the Siberian Branch of RAS for global detection and monitoring of natural and technogenic ionospheric disturbances on the basis of TEC variations retrieved from the global network of GPS receivers. In the time domain, TWPs are quasi-periodic TEC oscillations of duration about 1 h, period of 10–20 min, and amplitude exceeding that of the background TEC fluctuations by at least one order of magnitude. The velocity and direction of TWP motion are similar to those of mid-latitude mesoscale travelling ionospheric disturbances, as obtained earlier from the analysis of phase parameters of HF radio signals and the signals of geostationary satellites and discrete space radio sources. 相似文献
5.
6.
É. L. Nagaev 《Physics of the Solid State》1997,39(9):1415-1419
The temperature peak of the resistance and the giant magnetoresistance of degenerate ferromagnetic semiconductors with an
arbitrary degree of electron spin polarization are investigated. The spin-wave and paramagnetic domains are considered. The
calculations are based on the notion of the magnetic-impurity scattering of carriers.
Fiz. Tverd. Tela (St. Petersburg) 39, 1589–1593 (September 1997) 相似文献
7.
8.
The energy characteristics of an XeCl exciplex lamp with planar construction pumped by a low-pressure gas discharge are investigated
experimentally. When a discharge gap of width 2 cm and a Xe-Cl2 mixture were used, average radiation powers up to 20 mW were obtained in the wavelength interval 200–380 nm at efficiencies
of ∼0.4%. In this case the total efficiency of radiation into an angle of 4π exceeded 4%. It is shown that increasing the working pressure and using low discharge currents can lead to “point” radiation
sources.
Zh. Tekh. Fiz. 67, 43–46 (December 1997) 相似文献
9.
E. D. Mishina N. É. Sherstyuk V. O. Val’dner A. V. Mishina K. A. Vorotilov V. A. Vasil’ev A. S. Sigov M. P. De Santo E. Cazzanelli R. Barberi Th. Rasing 《Physics of the Solid State》2006,48(6):1210-1213
Ferroelectric composite two-dimensional ferroelectric/aluminum oxide nanostructures were studied. A porous aluminum oxide matrix was used as a template into which a ferroelectric precursor was introduced, followed by annealing. The prepared nanostructures were studied using optical second harmonic generation and micro-Raman scattering. 相似文献
10.