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铂(Ⅳ)—钼酸盐—丁基罗丹明B缔合显色反应的研究 总被引:7,自引:0,他引:7
本文研究在聚乙烯醇(PVA)存在下,铂与钼酸铵和丁基罗丹明B(BRB)形成离子缔合物,该缔合物的最大吸收位于570nm,摩尔吸光系数ε值为9.26×10~5L·mol~(-1)·cm~(-1),服从比耳定律范围0~3.0μg Pt/25ml,缔合物至少稳定3周。测定铂的条件为C_(HClO_4)=1.4mol/L,C_(MoO_4~(2-)=1.1×10~(-3)mol/L,C_(BRB)=3.8×10~(-5)mol/L,0.08%PVA。考察了40多种共存离子的影响,除形成杂多酸的元素外,大多数不干扰。本法已用于催化剂和某些铂矿中铂的测定,结果较满意。 相似文献
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Models for weather and climate prediction are complex, and each
model typi-cally has at least a small number of phenomena that are
poorly represented, such as perhaps the Madden-Julian Oscillation
(MJO for short) or El Ni\~{n}o-Southern Oscillation (ENSO for short)
or sea ice. Furthermore, it is often a very challenging task to
modify and improve a complex model without creating new
deficiencies. On the other hand, it is sometimes possible to design
a low-dimensional model for a particular phenomenon, such as the MJO
or ENSO, with significant skill, although the model may not
represent the dynamics of the full weather-climate system. Here a
strategy is proposed to mitigate these model errors by taking
advantage of each model''s strengths. The strategy involves
inter-model data assimilation, during a forecast simulation, whereby
models can exchange information in order to obtain more faithful
representations of the full weather-climate system. As an initial
investigation, the method is examined here using a simplified
scenario of linear models, involving a system of stochastic partial
differential equations (SPDEs for short) as an imperfect tropical
climate model and stochastic differential equations (SDEs for short)
as a low-dimensional model for the MJO. It is shown that the MJO
prediction skill of the imperfect climate model can be enhanced to
equal the predictive skill of the low-dimensional model. Such an
approach could provide a route to improving global model forecasts
in a minimally invasive way, with modifications to the prediction
system but without modifying the complex global physical model
itself. 相似文献
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It is shown that an n × n matrix of continuous linear maps from a pro-C^*-algebra A to L(H), which verifies the condition of complete positivity, is of the form [V^*TijФ(·)V]^n i,where Ф is a representation of A on a Hilbert space K, V is a bounded linear operator from H to K, and j=1,[Tij]^n i,j=1 is a positive element in the C^*-algebra of all n×n matrices over the commutant of Ф(A) in L(K). This generalizes a result of C. Y.Suen in Proc. Amer. Math. Soc., 112(3), 1991, 709-712. Also, a covariant version of this construction is given. 相似文献
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采用Nd0 .7Sr0 .3MnO3/SrTiO3/YBa2 Cu3O7-δ的异质结构 ,研究了自旋极化准粒子的注入效应 .在 5 6 μm宽的YBCO膜条上成功地制备了与超导膜条同样宽度但不同长度的六个注入结区 ,长度L分别为 80 μm ,4 0 μm ,2 0 μm ,10 μm ,5 μm和 2 μm .80nm厚的YBCO薄膜在 16K温度下Jc 为 2× 10 5A/cm2 .Iin=0 .5mA的自旋电流注入下 ,随L从 80 μm逐渐顺次减小时 ,注入效率 η =ΔJc/ΔJin逐渐增大 .而当L≤ 2 0 μm后 ,η不再增加 ,达到几乎相同的值 (~ 6 ) .初步分析认为这与自旋极化准粒子在超导膜内的有效自旋扩散长度有关 .异质结构中YBCO薄膜的超导电性以及注入窗口的尺寸对获得大的自旋注入效率十分重要 . 相似文献
5.
Existence of $\mu$-pseudo almost automorphic solutions to abstract partial neutral functional differential equations with infinite delay 下载免费PDF全文
Yong-Kui Chang G. M. N''Gu ''{e}r ''{e}kat Rui Zhang 《Journal of Applied Analysis & Computation》2016,6(3):628-664
In this article, we introduce and investigate the concept of $\mu$-Stepanov-like pseudo almost automorphic functions of class $h$ and class infinity via measure theory. We present new results on completeness and composition theorems for the space of such functions. To illustrate our main results, we provide some applications to an abstract partial neutral functional differential equation with infinite delay. 相似文献
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本文研究 Birkhoff 系统和广义 Birkhoff 系统平衡稳定性的动力学控制. 首先建立系统的运动方程和平衡方程. 其次,研究 Birkhoff 系统中控制参数出现在 Birkhoff 函数中平衡稳 定性的动力学控制. 方法是通过选取控制参数使得 Birkhoff 函数 $B$ 成为定号函数,而其时间导数 $\dot {B}$ 为与 $B$ 反号的常号函数. 再次,研究广义 Birkhoff 系统平衡稳定性的动力学控制,通过选取 Birkhoff 函数或附加项中包含控制参数的方法,使得 Birkhoff 函数是定号函数,而其时间导数为反号的常号函数,从而控制系统的平衡稳定性. 最后举例说明结果的应用. 相似文献
8.
根据发光层中电子能量分布的不均匀性,在分层优化薄膜电致发光器件的发光层中插入SiO2层,即级联分层优化薄膜电致发光器件。结果表明:由于SiO2的加速作用,这种方法确实可以提高过热电子的能量。但发光强度及发光效率的提高还受发光层的结晶状态的影响。插入一层SiO2后,样品的绿光强度提高了60%,发光效率也有所增加。插入两层SiO2后,由于发光层结晶状态变差,绿光强度及发光效率都降低了。 相似文献
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