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A comparison of chiral separation and analysis of selenomethionine in breast and formula milk, using high performance liquid chromatography (HPLC) on a glycopeptide teicoplanin-based chiral stationary phase (Chirobiotic T), coupled to atomic fluorescence spectrometry (AFS) and inductively coupled plasma (ICP) MS detectors has been performed. The coupling HPLC-microwave-assisted digestion hydride generation requires on-line post-column analytes treatment, and a severe sample clean-up for fat and proteins elimination using centrifugation and ultrafiltration. Underivatized -selenomethionine enantiomers were completely resolved in 10 min using unbuffered water mobile phase at 1 ml min−1 flow. Good selectivity and sensitivities (detection limits 3.1 and 3.5 ng ml−1 as Se for - and -selenomethionine, respectively) were obtained, and method robustness and simplicity, together to the low cost of AFS detector, makes it suitable for infant milk routine analysis. HPLC–ICP-MS coupling exhibits very low detection limits (0.9 ng ml−1, as Se) for each -selenomethionine enantiomers, but the method suffers from matrix influence, that produces a poor S/N ratio and low reliability.

The methods were applied to breast and formula milk samples with recoveries of 80% of the total selenium presence, which is attributable to the existence of other unknown species. -Selenomethionine was the only isomer present in breast milk, but a 30% of -selenomethionine was also detected in formula milk.  相似文献   

3.
A mathematical framework for translational Brownian motion on hypersurfaces is presented, using an imbedding of the surface and Ito diffusions in the ambient space. This includes a survey of Ito calculus and differential geometry. Computational methods for time correlation functions relevant to spin relaxation studies on curved interfaces are given, and explicit calculations of time correlation functions and order parameters for a Rippled surface are presented.  相似文献   
4.
dx(t)=g(x{t))dW(t) is proved using an approximating sequence of stochastic delay equationsGeneralizations of the approximation scheme are indicated for the Stratonovich case and when the Brownian motion W is replaced by a continuous semi-martingale.  相似文献   
5.
基于经典命题逻辑的真度理论,讨论了经典命题逻辑系统当中公式集的约简问题。提出了真度约简及α-真度约简的概念,为公式集的约简提供了一种可行的操作方法。  相似文献   
6.
Using an equivalent expression for solutions of second order Dirichlet problems in terms of Ito type stochastic differential equations, we develop a numerical solution method for Dirichlet boundary value problems. It is possible with this idea to solve for solution values of a partial differential equation at isolated points without having to construct any kind of mesh and without knowing approximations for the solution at any other points. Our method is similar to a recently published approach, but differs primarily in the handling of the boundary. Some numerical examples are presented, applying these techniques to model Laplace and Poisson equations on the unit disk. Visiting Professor, Universidad de Salamanca.  相似文献   
7.
Kortas  H.  Sifi  M. 《Potential Analysis》2001,15(1-2):43-58
In this work we consider a system of partial differential operators D 1,D 2 on K=[0,+[×R, whose eigenfunctions are the functions (x,t), (x,t)K, =((R0)×N)(0×[0,+[), which are related to the Laguerre functions for ((R 0)×N)(0,0) and which are the Bessel functions for (0×[0,+[). We provide K and with a convolution structure. We prove a Lévy–Khintchine formula on K, which permits us to characterize dual convolution semigroups on .  相似文献   
8.
分析了目前电子邮箱市场的情况,运用微分方程建立了邮箱用户增长模型,预测某邮箱未来几年内的用户数量及企业需要提供的硬盘容量。从减少成本的角度分析,运用Ito随机过程,对风险进行评估,建立硬盘容量动态分配模型,指导企业如何安排合适的硬盘容量,既能满足市场需要,又达到规避风险和降低成本的目的,提高市场竞争力。  相似文献   
9.
The paper discusses the pth moment exponential stability for a general class of neutral stochastic functional differential equations of the Ito type. This investigation can be very complicated, even in many special cases, by using usual methods based on Lyapunov functionals. In this paper we present criteria which are relatively easy to verify the pth moment exponential stability of the solutions of such equations.  相似文献   
10.
从定量的角度分析了随机利率下有股利分配的可转换债券的价值构成,并在股价服从广义O-U过程的条件下,利用鞅定价方法推导出可转换债券的定价公式.  相似文献   
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