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1.
C.J. Wu 《Applied Acoustics》2002,63(10):1143-1154
This work formulates the double-layer structural-acoustic coupling problem for cylindrical shell by using a combination of the wave-number domain approach (WDA) and the boundary integral equation (BIE). Expressions for the spectral radial velocity of the outer surface of a finite fluid-filled/submerged (FFS) cylindrical thin shell are formulated by means of the transfer matrix equation in wave-number domain. It is shown that the spectral variables on the inner surface of the shell are related to those on the outer surface of the shell. The far field sound radiation from this kind of shell is numerically evaluated for various fluid cases. An experimental verification is performed, and a good correlation between the theoretical results and the experimental results shows that the theoretical study work in this paper is correct. 相似文献
2.
The microstructure evolution of decagonal quasicrystals in Al72Ni12Co16 alloy was investigated by the electromagnetic melting and cyclic superheating method. Single-phase decagonal quasicrystals have been obtained when the undercoolings were larger than 60 K. The decagonal quasicrystals formed at various undercoolings show different microstructural morphologies. Furthermore, grain refinement was found near the undercooling of 120 K. Based on current thermodynamic and dendrite growth theories, a dimensionless superheating parameter was adopted to explain the effect of processing conditions on the microstructure of Al72Ni12Co16 alloy. The result indicate that the fine equiaxied microstructure of decagonal quasicrystal (D-phase) formed near on undercooling of 120 K originates from the break-up of dendrites. 相似文献
3.
Numerical studies were conducted to investigate the natural convection heat transfer around a uniformly heated thin plate
with arbitrary inclination in an infinite space. The numerical approach was based on the finite volume technique with a nonstaggered
grid arrangement. For handling the pressure–velocity coupling the SIMPLE-algorithm was used. QUICK scheme and first order
upwind scheme were employed for discretization of the momentum and energy convective terms respectively. Plate width and heating
rate were used to vary the modified Rayleigh number over the range of 4.8×106 to 1.87×108. Local and average heat transfer characteristics were compared with regarding to the inclination angle. The empirical expressions
for local and average Nusselt number were correlated. It has been found that for inclination angle less than 10∘, the flow and heat transfer characteristics are complicated and the average Nusselt number can not be correlated by one equation
while for inclination angle larger than 10∘, the average Nusselt number can be correlated into an elegant correlation.
Received on 18 April 2001 / Published online: 29 November 2001 相似文献
4.
2,6-O-diethyl-β-cyclodextrins were prepared and immobilized onto silica gel to develop a fluorosensor for dipyridamole. The
analytical performance characteristics of the proposed sensor for analysis of dipyridamole were as follows: the detection
limit was 0.8 nmol/L with a relative standard deviation of 1.4% for 10 determinations of 50 nmol/L of dipyridamole. The modification
of β-CD improved the sensitivity and selectivity for measuring dipyridamole. The recommended method has been successfully
tested for the determination of dipyridamole in clinical samples (urine and pharmaceutical preparations).
Received: 23 January 1997 / Revised: 14 April 1997 / Accepted: 21 April 1997 相似文献
5.
Zheng J. Maharaj C. Liu J. Chai H. Liu H. Dear J. P. 《Mechanics of Composite Materials》2022,58(1):125-140
Mechanics of Composite Materials - In this research, the maximum stress, Hashin, Puck, LaRC03, and Northwestern University (NU) criteria are analyzed based literature data, analytical results... 相似文献
6.
A flow injection catalytic spectrophotometric method is proposed for the determination of nitrite based on its catalytic effect on the redox reaction between naphthol green B and potassium bromate in phosphoric acid medium. The reaction is monitored spectrophotometrically by measuring the decrease in absorbance of naphthol green B at the maximum absorption wavelength of 722 nm. The detection limit is 0.5 ng cm(-3) in a sample volume of 90 mm(3). Up to 50 samples can be analyzed per hour with a relative precision of ca. 2%. The method is free from most interferences, especially from large amounts of nitrate. The procedure was successfully applied to the determination of trace nitrite in natural waters. 相似文献
7.
《Spectrochimica Acta Part B: Atomic Spectroscopy》2005,60(11):1468-1471
Five minerals containing aluminium in different crystal configurations are studied. The different kinds of chemical bonding between aluminium and oxygen originate molecular orbitals with energy levels and transition probabilities varying from one compound to another. This effect appears as shifts and changes in relative intensities of Kα emission lines and as modifications of the Kβ characteristic spectrum. In the present work, the aluminium K characteristic spectra obtained by means of an electron microprobe with a wavelength dispersive system are compared for topaz, albite, spodumene, biotite and corundum. 相似文献
8.
Anyun Zhang Jingxin Hu Xianye Zhang Fangding Wang 《Journal of Radioanalytical and Nuclear Chemistry》2002,253(1):107-113
N,Ndiethylhydroxylamine (DEHAN) can rapidly reduce Pu(IV) and Np(VI) extractable with trinbutyl phosphate (TBP) to Pu(III) and Np(V) unextractable with TBP in nitric acid solution. In order to apply DEHAN in the purification cycle step of U (noted as contactor 2D) of the secondcycle of the Purex Process to separate Np and Pu from U, the reduction of Np(VI) and the stability of Np(V) with DEHAN and the singlestage reduction extraction and backextraction of Np(VI) have been studied according to the experimental conditions of contactor 2D. The results show that more than 99% of Np(VI) can entirely be reduced to Np(V) with DEHAN within a few minutes either in aqueous or in organic phase containing uranium and without containing uranium, and more than 99% of Np(VI) can be backextracted from the organic to the aqueous phase with DEHAN as a reductant. More than 99% of Np(V) exists in nitric acid solution at least for 8 hours in presence of 0.01 mol/l DEHAN. These results are of benefit to the cascade extractionseparation of U/Np in contactor 2D in order to decontaminate Np from U. 相似文献
9.
The kinetics of oxidation-reduction reaction between N,N-diethylhydroxylamine (DEHAN) and neptunium (VI) in nitric acid media has been studied by spectrophotometry at 25.2 °C. The rate equation is -d[Np(VI)/dt=k[Np(VI)][DEHAN]/[H+] found by investigating the influence of concentration, acidity, ionic strength and temperature on the reaction. The rate constant of the reaction k is 23.0±1.8 min–1 for = 2.0 mol/l. A possible mechanism of reaction has been suggested according to the ESR spectra of nitroxide radical produced in the DEHAN+V(V) system. 相似文献
10.
Porous SiO2 films were successfully deposited on silicon substrates by a modified base-catalyzed Sol-Gel process (MBCP) containing polyvinyl alcohol (PVA). The process conditions, such as the gelation time, the synthesis temperature, the stabilizing agent of the precursor solution and the spin coating speed, the heat-treatment, the annealing temperature of the film on the microstructure and porosity of porous SiO2 films were systematically investigated by SEM, XRD and ellipsometry techniques. This study provides a novel preparation technique for the porous SiO2 film. Using this process, the resultant film can reach a thickness of 3.6 m for one layer, a porosity of 25–50%, a low thermal conductivity of 0.11 W/m·K. This film will be used as a low dielectric layer, an thermal-insulating layer and a low refractive index layer. 相似文献