改进的图象小波域水印算法

本文以数字图象为例，通过对人类视觉系统（HVS）模型的改进，在数字图象中加入了鲁棒性强的水印。     

海水中氯氟烃测定方法研究

描述了用气相色谱法测定海水中氯氟烃的方法.用Niskin采水器采集海水后转移玻璃注射器中储藏.30mL海水于玻璃气提器中,用吹扫捕集法将海水中氯氟烃(CFC's)送入气相色谱柱,分离后用电子捕获检测器(ECD)检测,以外校法计算其含量.该方法快速,灵敏度高,分离效果好,适用于分析测定水体中氯氟烃.     

High temperature (70°C) size exclusion chromatography of petroleum waxes with RI and FID detection

Molecular weight distribution of solid petroleum waxes is a key parameter for the general characterization of these materials. Particular interest concerns extremely large components, typically present in oil distillation residua, and solid deposits found in oil production facilities. Molecular weight distributions of oil waxes were determined in this work by high temperature size exclusion chromatography. Separations were carried out with two different eluents, namely toluene and ortho-dichlorobenzene and two detection systems, these being a differential refractive index and a flame ionization detector. Toluene proved to be the best choice when combined with flame ionization detection. Better uniformity of response was the greatest advantage achieved by this approach. The experimental set up permitted analysis of samples containing molecules with up to 138 carbon atoms. Burning properties of very large molecules, isomerism affecting calibration, and signal asymmetry when flame ionization detection was adopted were three issues still requiring additional efforts to understand and to improve analysis accuracy.     

Hanning低通滤波在PSD法测量直管不直度中的应用

该文介绍了利用ＰＳＤ测量直管不直度的新颖方法,利用频谱分析的方法分别对不直度理论模型和实验数据作了分析,得出了不直度信号具有低频占优的频谱特征的结论,并由此提出了利用Ｈａｎｎｉｎｇ低通数字滤波器除高频噪声,从而解决了直管不直度曲线这种空域信号无法利用电学滤波的困难。     

风扇磨煤机微机实时监控系统

介绍了一种采用工业 Ｐ Ｃ机对山东龙口发电厂风扇磨煤机进行实时监控系统的设计思路、系统结构、软件设计及技术特点。系统设计完善、精度高、速度快,集监控与管理于一体,既可实现对磨机振值实时检测与控制,又可描述其振动曲线、历史趋势图,为磨机合理调配、科学的维护起指导作用。结果表明：系统运行可靠,动作准确,数次排除了飞磨的隐患,取得了可观的经济效益。     

冶炼过程的在线光谱分析

利用石英光纤、光栅光谱仪、CCD探测器、微机组成在线光谱分析系统．测量该系统的光谱分辨率、时间响应及探测灵敏度,并对模拟炼钢过程进行在线光谱分析．     

摩尔响应值与分子连接性指数关系的再研究

对链烷烃、链烷醇、苯系列和酮类化合物选择适当的分子连接性指数,用摩尔响应值对它们进行多元线性回归,结果表明两者之间存在良好的相关性。     

Response of CZT drift-strip detector to X- and gamma rays

The drift-strip method for improving the energy response of a CdZnTe (CZT) detector to hard X- and gamma rays is discussed. Results for a 10×10×3 mm³ detector crystal demonstrate a remarkable improvement of the energy resolution. The full width at half maximum (FWHM) is 2.18 keV (3.6%), 2.45 keV (3.0%), 2.86 keV (0.8%) and 3.89 keV (0.6%) at 60, 80, 356 and 661 keV, respectively. The resolution is limited by electronic noise below 100 keV.     

Triton and alpha-particle contribution from LiF converter for neutron dosimeter

A personnel neutron dosimeter prototype based on chemical and electrochemical etched CR-39 detector, combined with LiF converter, has been calibrated using an ICRP-like phantom, under a heavy-water moderated Californium source neutron spectra; A conversion factor of 1.052±126 spots cm⁻² mSv⁻¹ was obtained. The sealing properties of the detector holder showed a ten-fold reduction in radon background when it was tested in a high radon atmosphere. A convenient mechanical shock resistance was achieved in LiF converters by sintering to 11 tons pressure LiF powder at 650°C, during one hour.     

Anionic synthesis and detection of fluorescence‐labeled polymers with a terminal anhydride group

To monitor polymer–polymer coupling reactions between two different monofunctional polymers in dilute polymer blends, fluorescence‐labeled anhydride‐functional polystyrene (PS) and poly(methyl methacrylate) (PMMA) were prepared by conventional anionic polymerization. Sequential trapping of lithiopolystyrene by 1‐(2‐anthryl)‐1‐phenylethylene (APE) and then di‐t‐butyl maleate (4) provided, after pyrolysis, anhydride‐functional fluorescent PS. Fluorescent PMMA anhydride (8) was synthesized with sec‐butyllithium/APE as an initiator for the anionic polymerization of methyl methacrylate, trapping by 4, and pyrolysis. These polymers could be reacted with amine‐functional polymers by melt blending, and the reaction progress could be monitored by gel permeation chromatography coupled with fluorescence detection. This technique not only allows monitoring of the coupling reaction with high sensitivity (ca. 100 times more sensitive than refractive index detection) but also permits selective detection because unlabeled polymers are invisible to fluorescence detection. This highly sensitive and selective detection methodology was also used to monitor the coupling reaction of 8 with PS‐NH₂ at a thin‐film interface, which was otherwise difficult to detect by conventional methods. © 2000 John Wiley & Sons, Inc. J Polym Sci A: Polym Chem 38: 2177–2185, 2000