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Junfei Ou Ying Wang Changquan Li Fajun Wang Mingshan Xue Jinqing Wang 《Surface and interface analysis : SIA》2013,45(7):1182-1187
Polydopamine (coded as PDA) is reported to be very adhesive and reactive due to the attached functional groups, such as amine and hydroxyl groups. In this work, taking advantage of the condensation between Si–OH of the hydroxylated alkyltrichlorosilane (ATS) and C–OH on PDA surface, ATS molecules with different chain carbon number of 10, 14 and 18 were grafted onto the 3‐aminopropyl triethoxysilane (APTES)‐PDA dual‐layer film, which was composed of PDA outerlayer and APTES underlayer, on Si substrate. Thus, hydrophobic trilayer films coded as APTES‐PDA‐ATS were prepared successfully. In order to reveal the dependence of the tribological behaviors upon the microstructures of the film, tribological experiments were conducted on an atomic force microscope and a ball‐on‐plate tribometer. Experimental results showed that the (micro‐) friction reducing (characterized by a parameter of relative friction coefficient or friction coefficient, RFC or FC) and macro‐wear resisting (characterized by anti‐wear life) behaviors were related with the chain length of outerlayer and the PDA thickness. Specifically, on one hand, as the chain length increases, RFC/FC decreased and macro anti‐wear life lengthened; on the other hand, as PDA gets thicker, RFC increased and the anti‐wear life enhanced. Copyright © 2013 John Wiley & Sons, Ltd. 相似文献
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The liquid crystalline behaviour of methyl-6-O-(n-dodecanoyl)-α-D-glucopyranoside, 1, has been characterised using X-ray diffraction and variable temperature Fourier transform infrared (FTIR spectroscopy). 1 exhibits a monotropic interdigitated smectic A phase consisting of bilayers in which the alkyl chains are overlapped. The crystal–isotropic transition is accompanied by a pronounced decrease in the strength of the hydrogen bonding network involving the sugar groups resulting in a marked change in the environment of the alkyl chains. The isotropic phase consists of disordered smectic-like domains stabilised via hydrogen bonding between the sugar groups. At the transition to the smectic A phase, a subtle change in hydrogen bonding is observed which is manifested by a change in the temperature dependence of the OH stretching peak position in the FTIR spectrum. On crystallisation, the strong hydrogen bonding network is re-established accompanied by a change in the conformational distribution of the alkyl chains. A model is proposed in which a combination of hydrogen bonding (enthalpic effects) and conformational arrangements (entropic effects) promotes initially the formation of smectic-like domains in the isotropic phase and subsequently stabilises the smectic A phase by inhibiting the microphase separation leading to the crystal phase. 相似文献
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考虑了带二元连续变利息力的Sparre Andersen风险模型.研究了积累值盈余过程的表达式与性质;在利率递增环境下,利用推广后的调节系数方程组与递归技术推导了最终破产概率的上界,结论表明得到的破产概率上界是更为一般的Lundberg指数上界. 相似文献
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Peggy Cénac Brigitte Chauvin Frédéric Paccaut Nicolas Pouyanne 《Random Structures and Algorithms》2015,46(1):117-141
Common assumptions on the source producing the words inserted in a suffix trie with n leaves lead to a height and saturation level. We provide an example of a suffix trie whose height increases faster than a power of n and another one whose saturation level is negligible with respect to . Both are built from VLMC (Variable Length Markov Chain) probabilistic sources and are easily extended to families of tries having the same properties. The first example corresponds to a “logarithmic infinite comb” and enjoys a non uniform polynomial mixing. The second one corresponds to a “factorial infinite comb” for which mixing is uniform and exponential. © 2013 Wiley Periodicals, Inc. Random Struct. Alg., 46, 117–141, 2015 相似文献
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Stability criteria in terms of two measures for functional differential equation with variable‐time impulses 下载免费PDF全文
Chao Liu Chuandong Li Tingwen Huang Hui Wang 《Mathematical Methods in the Applied Sciences》2015,38(14):2922-2936
This paper focuses on the stability in terms of two measures for functional differential equation with variable‐time impulses. Being different from most of existing literatures, the impulses of functional differential equation are assumed to be closely associated to the current state. We propose a new comparison principle for the considered systems and establish several stability criteria in terms of two measures. Also, the theoretical results are applied in a class of delayed neural network systems with variable‐tine impulses, and numerical simulations are introduced to illustrate the effectiveness of our results. Copyright © 2014 John Wiley & Sons, Ltd. 相似文献
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变截面钢管混凝土格构柱轴压极限承载力 总被引:2,自引:1,他引:1
变截面钢管混凝土格构柱的轴压试验结果表明,随着试件高度的增大和柱肢坡度的减小,其极限荷载逐渐降低.基于上述规律,在等截面钢管混凝土格构柱计算框架的基础上,研究了变截面钢管混凝土格构柱轴压极限承载力的计算方法.提出变截面钢管混凝土格构柱等效长度的概念和等效长度法的计算公式,其承载力计算结果与试验结果吻合良好.最后在有限元数值分析验证的基础上,给出适合工程应用的四肢变截面钢管混凝土格构柱轴压极限承载力的实用算法,为钢管混凝土设计规程的进一步完善提供参考. 相似文献