内蒙古乌拉特前旗脑包沟—北召沟金矿床特征及其成因

通过区域地质背景、构造格局、构造递变序列、矿床地质特征及成因研究，论述了脑包沟-北召沟石英钾长石蚀变脉型金矿床的多源复成热液成因，并对研究区找矿前景进行了探讨。     

新疆富蕴县萨尔布拉克金矿预测区断裂特征及其控矿规律

在全面、系统收集和研究新疆富蕴县萨尔布拉克地区地质、地球物理、地球化学、矿产普查和科研资料的基础上，深入分析金矿成矿地质条件、控矿因素和找矿方法组合，对萨尔布拉克预测区95条断裂的地质、地球物理、地球化学特征进行了全面统计分析，确定了42条赋金断裂．其中早期断裂8条，占19％；晚期断裂34条，占81％．赋金断裂以晚期南北向为主，次为东西向和北西向．航磁异常向上延拓高度大者，即赋金断裂延深大者对金的成矿有利．     

基于证据权模型的宁芜盆地中段玢岩铁矿资源预测

基于证据权模型,对宁芜盆地中段玢岩铁矿进行矿产资源评价.首先,结合研究区的成矿地质背景,提取地层、岩体、构造、物探异常等四大类证据因子.然后,分析各证据因子与铁矿点之间的空间关系,认为大王山旋回火山岩与次火山岩与玢岩铁矿的关系最为密切,是寻找玢岩铁矿的岩石标志,深成侵入体则与铁矿空间上无明显关系,构造、物探异常在空间上与玢岩铁矿也有较大关联.根据计算结果,选取与玢岩铁矿密切相关的大王山旋回火山岩地层、闪长玢岩岩体、各方向(EW,NW,NE)构造缓冲区、航磁异常和布格重力异常七类证据图层.最后,采用证据权模型进行成矿后验概率计算,结合成矿地质背景及物探异常,圈定5个成矿预测区,它们在区域上具明显的NE向展布特征,并且普遍分布与成矿密切相关的闪长玢岩岩体,同时位于航磁高值以及NW向和NE向构造发育密集处.     

钨极惰性气体保护焊熔池三维自由表面特征参数的激光视觉测量

摘要： 针对现有的钨极惰性气体保护焊熔池三维自由表面测量方法难以应用于强弧光、高温辐射、液态金属表面镜面反射等问题,提出一种激光视觉测量法. 利用小功率点或线阵模式结构激光照射覆盖整个熔池表面,采用高速摄像机实时采集经熔池液态金属表面反射畸变的激光图像.设计图像处理算法提取成像激光点位置坐标,建立与投射激光点位置坐标的空间转换数学模型,离线获得熔池三维自由表面的几何特征参数值,对比实测凝固熔池表面对应参数值发现,所提取的几何特征参数值与实测值吻合较好,熔宽、长度和凸度误差分别为0.8%、0.6%和4.7%,证明激光视觉法能够实现熔池自由表面三维信息的动态测量,为采用几何特征参数调整熔池自由表面形貌变化控制焊缝成形及缺陷提供一种新方法.     

诸广地区构造的分形特征及其找铀指示

热液型铀矿的成矿作用复杂,构造是最重要控矿因素之一.利用ARCGIS9.2及ARCVIEW3.2软件,对诸广铀矿集区中巴尖兵三号高空间分辨率遥感数据所解译的构造进行分形分析,并进一步研究其分形特征与铀成矿的关系.研究发现,构造分维值的大小和矿床(点)的疏密呈现出良好的正相关性,分维值可以作为勘查靶区选择的定量指标.     

氧化钨纳米棒的制备及其形貌控制

报道了一种利用溶胶-凝胶法和水热法相结合制备纳米氧化钨的新方法.首先在丙醇-四丁基溴化铵-环己烷体系中,由钨酸钠和盐酸反应出发制备凝胶状的钨酸,然后将其置于高压反应釜中200℃下处理12 h即可制得氧化钨纳米棒.使用X-射线衍射分析仪(XRD)和扫描电子显微镜(SEM)对产物的结构与形貌进行表征.     

Precipitates originating from tungsten crucible parts in AlN bulk crystals grown by the PVT method

In order to evaluate the possible involvement of crucible materials in the growth of AlN bulk crystals grown by physical vapor transport, we applied growth conditions with a high vertical thermal gradient and hence high supersaturation of aluminum vapor. Under these conditions, precipitates formed causing diffuse grayish substructures at the initial growth interface and in the crystal body, decorating dislocations. Electron microscopy studies revealed that the precipitates are elongated, single‐phase particles with sizes of 50–500 nm of commensurate structure, oriented along the <110> direction. Chemical analysis of the precipitates showed tungsten as well as carbon and oxygen. The lattice parameters of the precipitates are in close agreement to hexagonal tungsten hemicarbide (W₂C). The possible transport from the tungsten parts and its conversion into tungsten hemicarbide precipitates is discussed. We thus conclude that the W₂C precipitates may contribute to the decoration of dislocations, even in growth with moderate thermal gradients.     

Characterization of solid standards prepared by freeze‐drying

Solid standards prepared by freeze‐drying consistently showed a high degree of homogeneity. The freezing process, completed in fractions of a second, preserves the original homogeneous distribution of the dopants, and the subsequent sublimation step would minimize any disturbance. Compared to those prepared by conventional methods such as blending and spiking, freeze‐dried standards exhibited superior lateral distribution and better uniform depth distribution. There is, however, a concentration constraint for achieving homogeneity. At 5% doping, segregation was observed in both lateral and depth distribution. Many tungsten standards doped with 10–28 elements ranging from 10 to 200 ppm were successfully prepared and used as controls for a number of analytical techniques including glow discharge mass spectrometry (GDMS) and d.c.‐arc optical emission spectroscopy (OES). Copyright © 2009 John Wiley & Sons, Ltd.     

New high permittivity tetragonal tungsten bronze dielectrics Ba2LaMNb4O15: M=Mn, Fe

The new phases Ba₂LaMNb₄O₁₅: M=Mn, Fe were prepared by solid state reaction at 1100 °C. They have the tetragonal tungsten bronze structure, space group P4/mbm, at room temperature. The two octahedral sites show partial order of M and Nb with preferential occupancy of the smaller B(1) sites by M. Both phases have high permittivities 90±15 over the range 10-320 K. Ba₂LaFeNb₄O₁₅ is highly insulating with bulk conductivity ?10⁻⁸ ohm⁻¹ cm⁻¹ at 25 °C and tan δ?0.001 over the range 100-320 K and at 10⁵ Hz. Solid solutions between these new phases and the compositionally and structurally related relaxor ferroelectric Ba₂LaTi₂Nb₃O₁₅ show gradual loss of ferroelectric behaviour attributed to replacement of polarisable Ti⁴⁺ by a mixture of (Mn, Fe)³⁺ and Nb⁵⁺.