Analysis of nine rhubarb anthraquinones and bianthrones by micellar electrokinetic chromatography using experimental design

An efficient micellar electrokinetic chromatography (MEKC) method has been developed for the analysis of nine anthraquinones and bianthrones in rhubarb. A chemometric approach was used to search for the optimum conditions of separation. Those factors which were found to be significant with a screening design were further optimized with a central composite face-centered (CCF) design. Acetonitrile concentration was found to be the most influential, not only in resolution, but also in analysis time and peak asymmetry. With the optimized conditions: 15 mM sodium tetraborate/15 mM sodium dihydrogenphosphate buffer, 30 mM sodium deoxycholate, pH 8.6, 17 vol.% acetonitrile and 28 kV, nine tested analytes were baseline-separated within 14 min. The method was validated to analyze the rhubarb material. Solid-phase extraction (SPE) was manipulated to remove interfering substances. Five anthraquinones and two glycosidic bianthrones were detected and quantificated. The method should be suitable for determining these major active principles in rhubarb crude drugs.     

一种新颖的超结构光纤Bragg光栅梳状滤波器的设计

报道一种新颖的用于多波长光纤激光器的超结构光纤Bragg光栅（SFBG）梳状滤波器，其突出特点是仅由单个光栅构成、折射率调制和局部啁啾富于变化、反射峰均匀性好、窄带宽和标准的信道间隔.采用基于LP算法的IS光纤光栅设计技术，将整体加窗切趾法改进为各信道独立加窗切趾，成功地设计出所需的SFBG，同时对SFBG的制作技术也进行了探讨.用传输矩阵法分析反射谱、时延曲线和群时延抖动.结果表明，所设计的SFBG满足各项设计指标要求，在DWDM系统中，这种新颖的SFBG可望成为用于多波长光纤激光器的最理想的高性 能梳 关键词： 超结构光纤Bragg光栅 光栅设计 梳状滤波器     

基于人因工程的纳米铁粉生产线人机界面设计

综合运用人因工程的理论和技术,对纳米铁粉生产线的操作流程进行研究,建立了标准的人机操作界面,实现了降低成本、提高效率、以及安全、健康、舒适的目标.     

山西省吴家庄水库工业供水工程管线设计

介绍了山西省吴家庄水库工业供水管道工程管线的选材、水力计算及纵横断面设计。     

石灰粉煤灰稳定石屑的基层施工技术

文章详细论述了道路施工中石灰、粉煤灰、稳定石屑作为基层结构的要求、技术指标和施工工艺。     

论中国现代城市建筑设计中形式美的科技应用趋向

通过对结构、空间、色彩中科技应用的分析,述评了中国现代城市建筑设计中形式美的科技应用趋向。     

营销支撑平台现状及其发展

分析了目前营销支撑平台的发展现状,针对存在问题和经营、管理、运行效率方面的要求,从闭环式方案定制系统、系统化支撑程序设计、优惠处理模型优化3个方面探讨了营销支撑平台的发展方向。     

Microstation与AutoCAD在计算机辅助设计方面的比较

从常用二维工具、三维造型、外部图形数据的交换与图像处理和对Windows的支持等方面,探讨了Microstation与AutoCAD在计算机辅助设计方面各自的优劣及适用范围。     

基于ASP.NET的毕业设计选题系统构建

介绍了ASP.NET技术,并对基于ASP.NET技术开发的B/S结构毕业设计选题系统的功能进行了详释。     

Extremal Self-Dual [50, 25, 10] Codes with Automorphisms of Order 3 and Quasi-Symmetric 2-(49, 9,6) Designs

Five non-isomorphic quasi-symmetric 2-(49, 9, 6) designs are known. They arise from extremal self-dual [50, 25, 10] codes with a certain weight enumerator. Four of them have an automorphism of order 3 fixing two points. In this paper, it is shown that there are exactly 48 inequivalent extremal self-dual [50, 25, 10] code with this weight enumerator and an automorphism of order 3 fixing two points. 44 new quasi-symmetric 2-(49, 9, 6) designs with an automorphism of order 3 are constructed from these codes.