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941.
942.
Karel Minnaar 《Journal of the mechanics and physics of solids》2004,52(12):2771-2799
A novel experimental technique is developed for time-resolved detection and tracking of damage in the forms of delamination and matrix cracking in layered materials such as composite laminates. The technique is non-contact in nature and uses dual or quadruple laser interferometers for high temporal resolution. Simultaneous measurements of differential displacement and velocity at individual locations are obtained to analyze the initiation and progression of interfacial fracture and/or matrix cracking/delamination in a polymer matrix composite laminate system reinforced by graphite fibers. The measurements at multiple locations allow the speeds at which interfacial crack front (mode-I) or matrix cracking/delamination front (mode-II dominated) propagates to be determined. Experiments carried out use three-point bend configurations. Impact loading is achieved using a modified Kolsky bar apparatus with a complete set of diagnostics for load, deformation, deformation rate, and input energy measurement. This technique is used to characterize the full process of damage initiation and growth. The experiments also focused on the quantification of the speed at which delamination or damage propagates under primarily mode-I and mode-II conditions. The results show that the speed of delamination (mode-I) or the speed of matrix cracking/delamination (primarily mode-II) increases linearly with impact velocity. Furthermore, speeds of matrix failure/delamination under primarily mode-II conditions are much higher than the speeds of mode-I crack induced delamination under mode-I conditions. 相似文献
943.
G.?JourdanEmail author L.?Houas L.?Schwaederlé G.?Layes R.?Carrey F.?Diaz 《Shock Waves》2004,13(6):501-504
A new variable inclination shock tube has been set up especially for the visualization of shock induced high speed flows. This device allows for the generation of shock waves of Mach numbers ranging from 1.05 to 4, moving horizontally, vertically from up to down or the opposite, or with any inclination angle. It is coupled with a suitable high-speed camera shadowgraph visualization system, and the whole facility has been realized so as to be both very easy to use and movable. We believe this example could be of interest to scientists interested in starting experiments on shock wave induced multi-phase complex flows. 相似文献
944.
Dynamic crack growth along the interface of a fiber-reinforced polymer composite-Homalite bimaterial subjected to impact shear loading is investigated experimentally and numerically. In the experiments, the polymer composite-Homalite specimens are impacted with a projectile causing shear dominated interfacial cracks to initiate and subsequently grow along the interface at speeds faster than the shear wave speed of Homalite. Crack growth is observed using dynamic photoelasticity in conjunction with high-speed photography. The calculations are carried out for a plane stress model of the experimental configuration and are based on a cohesive surface formulation that allows crack growth, when it occurs, to emerge as a natural outcome of the deformation history. The effect of impact velocity and loading rate is explored numerically. The experiments and calculations are consistent in identifying discrete crack speed regimes within which crack growth at sustained crack speeds is possible. We present the first conclusive experimental evidence of interfacial crack speeds faster than any characteristic elastic wave speed of the more compliant material. The occurrence of this crack speed was predicted numerically and the calculations were used to design the experiments. In addition, the first experimental observation of a mother-daughter crack mechanism allowing a subsonic crack to evolve into an intersonic crack is documented. The calculations exhibit all the crack growth regimes seen in the experiments and, in addition, predict a regime with a pulse-like traction distribution along the bond line. 相似文献
945.
阐述中小企业在整个国民经济中的重要地位,指出电子商务对于中小企业具有天然的适应性和可行的推广性.揭示研究对象中蕴含着广泛的模糊性,应用区间直觉模糊不确定语言的必要性.介绍区间直觉模糊不确定语言的基本概念、基本运算、算术平均和加权平均、距离、期望函数、精度函数、期望函数值、精度函数值以及对象比较方法等内容.提出区间直觉模糊不确定语言决策步骤:设定方案集、指标集、专家集,确定评判矩阵,确定指标权重,计算加权平均,计算期望函数、精度函数,期望函数值、精度函数值,进行排序.以盛东商贸有限公司电子商务网站设计方案测评为例,碍出方案3优于方案2优于方案5优于方案1优于方案4的结论. 相似文献
946.
《Journal of separation science》2017,40(6):1273-1282
10‐Deacetylbaccatin III, an important semisynthetic precursor of paclitaxel and docetaxel, can be extracted from Taxus wallichiana Zucc. A process for the isolation and purification of 10‐deacetylbaccatin III ( 1 ), baccatin III ( 2 ), and 7β‐xylosyl‐10‐deacetyltaxol ( 3 ) from the leaves and branches of Taxus wallichiana Zucc. via macroporous resin column chromatography combined with high‐speed countercurrent chromatography or reversed‐phase flash chromatography was developed in this study. After fractionation by macroporous resin column chromatography, 80% methanol fraction was selected based on high‐performance liquid chromatography and liquid chromatography with mass spectrometry qualitative analysis. A solvent system composed of n‐hexane, ethyl acetate, methanol, and water (1.6:2.5:1.6:2.5, v/v/v/v) was used for the high‐speed countercurrent chromatography separation at a flow rate of 2.5 mL/min. The reversed‐phase flash chromatography separation was performed using methanol/water as the mobile phase at a flow rate of 3 mL/min. The high‐speed countercurrent chromatography separation produced compounds 1 (10.2 mg, 94.4%), 2 (2.1 mg, 98.0%), and 3 (4.6 mg, 98.8%) from 100 mg of sample within 110 min, while the reversed‐phase flash chromatography separation purified compounds 1 (9.8 mg, 95.6%) and 3 (4.9 mg, 97.9%) from 100 mg of sample within 120 min. 相似文献
947.
《Journal of separation science》2017,40(14):2906-2913
A novel method was developed for the purification of two typical diarrhetic shellfish poisoning toxins from toxin‐producing marine microalgae using macroporous resin, high‐speed countercurrent chromatography–mass spectrometry, and semipreparative high‐performance liquid chromatography–mass spectrometry. Analytical high‐performance liquid chromatography–mass spectrometry was used for identification and purity analysis of okadaic acid and dinophysistoxin‐1 because they exhibit no visible or ultraviolet absorption. First, four kinds of macroporous resins were investigated, and HP‐20 macroporous resin was selected for the preenrichment and cleanup of the two target toxins. Second, the resin‐purified sample was further purified using high‐speed countercurrent chromatography coupled with a mass spectrometer. The purities of the obtained okadaic acid and dinophysistoxin‐1 were 89.0 and 83.0%, respectively, as determined through analytical high‐performance liquid chromatography–mass spectrometry. Finally, further purification was carried out using semipreparative high‐performance liquid chromatography with mass spectrometry, and the purities of the final okadaic acid and dinophysistoxin‐1 products were both over 98.0% based on the analytical high‐performance liquid chromatography–mass spectrometry chromatograms and fraction spectra. This work demonstrates that the proposed purification process is a powerful method for the preparation of high‐purity okadaic acid and dinophysistoxin‐1 from toxin‐producing marine microalgae. Moreover, it is particularly important for the purification and preparation of minor toxins that exhibit no visible or ultraviolet absorption from harmful marine algae. 相似文献
948.
This paper extends the framework for the valuation of life insurance policies and annuities by Andrés-Sánchez and González-Vila (2012, 2014) in two ways. First we allow various uncertain magnitudes to be estimated by means of fuzzy numbers. This applies not only to interest rates but also to the amounts to be paid out by the insurance company. Second, the use of symmetrical triangular fuzzy numbers allows us to obtain expressions for the pricing of life contingencies and their variability that are closely linked to standard financial and actuarial mathematics. Moreover, they are relatively straightforward to compute and understand from a standard actuarial point of view. 相似文献
949.
M. Hladík 《Optimization》2017,66(3):331-349
We consider a linear regression model where neither regressors nor the dependent variable is observable; only intervals are available which are assumed to cover the unobservable data points. Our task is to compute tight bounds for the residual errors of minimum-norm estimators of regression parameters with various norms (corresponding to least absolute deviations (LAD), ordinary least squares (OLS), generalized least squares (GLS) and Chebyshev approximation). The computation of the error bounds can be formulated as a pair of max–min and min–min box-constrained optimization problems. We give a detailed complexity-theoretic analysis of them. First, we prove that they are NP-hard in general. Then, further analysis explains the sources of NP-hardness. We investigate three restrictions when the problem is solvable in polynomial time: the case when the parameter space is known apriori to be restricted into a particular orthant, the case when the regression model has a fixed number of regression parameters, and the case when only the dependent variable is observed with errors. We propose a method, called orthant decomposition of the parameter space, which is the main tool for obtaining polynomial-time computability results. 相似文献
950.
多属性决策时因掌握的信息有限,加之问题本身的复杂性、不确定性以及人类思维的模糊性,其属性的精确值往往难以获取,常用区间数形式表示针对多属性决策中各指标区间数不能直接进行大小比较的问题,提出一种基于集对分析联系数的区间数型多属性决策投影模型.模型用备择方案在理想方案上的投影进行集结,根据区间数的误差分布形式,沟通区间数与联系数的关系,根据a+bi型联系数大小比较法则,综合评价方案优劣.以某大厦基坑支护拟用的4种方案优化选择为例,说明方法的应用与模糊优化理论模型和灰色物元分析优化模型进行了对比,得到的结果一致. 相似文献