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161.
通过使用“可磨式”人工热电偶进行的不同条件下的磨削温度测量试验研究了钢坯磨削工件表层温度,结果表明钢坯被磨削表层温度分布与热强呈三角形分布时的理论分析结果相同,表层峰值温度随磨削压力及磨削功率增大而提高,且随工件进给速度提高而略有降低,峰值温度还随磨削角度减小而提高,90°磨削的峰值温度比0°磨削要低250℃左右,砂轮种类也对峰值温度有重要影响,使用锆刚玉砂轮时磨削温度低于棕刚玉砂轮,试验结果表明高效钢坯磨削的磨削区温度远比普通磨削为高,可达1200℃左右,还从不同方面探讨了磨削高温对钢坯磨削的影响,认为尽管磨削高温有若干不利影响,但对高效钢坯磨削却是重要条件,上述讨论,从一个方面揭示了钢坯磨削机理,并验证了关于钢坯磨削温度的理论分析结果。 相似文献
162.
E. A. Zheligovskaya 《Journal of Structural Chemistry》2003,44(5):827-835
A computer simulation of proton-ordered ice IX and its proton-disordered analog III (768 molecules, 90 K) was carried out by the molecular dynamics method using Poltev–Malenkov's potential. For ice IX, the differences in the dynamic characteristics of molecules with O(1) and O(2) are much wider than those in the case of ice III. The libration spectrum of ice IX has a number of distinct acute peaks, and the spectrum of ice III is strongly smoothed. These peculiarities are explained by the proton ordering of ice IX and disordering of ice III. The latter is responsible for the great differences in the short- and especially long-range environment of water molecules in ice crystals and hence for the presence of many molecules with different dynamic characteristics. Thus averaging over a large number of different vibrational spectra of molecules leads to a smoothed total spectrum in the case of the proton-disordered crystal modification of ice. 相似文献
163.
This is the second part of a paper which deals with the advantages and disadvantages of relative instrumental neutron activation
analysis concerning traceability and uncertainty, and the current scope and possible future extensions of neutron activation
analysis as a primary ratio method. The first part of this paper has been published in this Journal [1].
Received: 19 March 2001 Accepted: 2 October 2001 相似文献
164.
AN Ya XU Jun ZHANG Jin HU Changgang LI Ganzuo WANG Zhining WANG Zhongni ZHANG Xiaoyi & ZHENG Liqiang . Key Lab of Colloid Interface Chemistry for State Education Ministry Jinan China . College of Science Guizhou Normal University Guiyang China 《中国科学B辑(英文版)》2006,49(5)
The pseudo-quaternary phase diagram of Brij35/sodium oleate/oleic acid/water systems has been investigated, and the liquid crystal area has been identified, which covers about two thirds of the whole phase diagram. The liquid crystal structure and behavior have been also studied by using polarizing texture, small angle X-ray scattering, 2H-NMR and rheometer etc. The result shows that when the composition of the system changes along the line of AA′ in this large liquid crystal region, the structural change is cubic→cubic/lamellar→lamellar→lamellar/hexagonal→hexagonal. Meanwhile, we made the first attempt of systematic study of the rheological properties of the above system. The lattice constants of cubic and hexagonal liquid crystals are 10.53 and 5.68 nm, respectively. 相似文献
165.
Silver halide (AgX) microcrystal was used as template to synthesize hollow polyelectrolyte capsules. These hollow capsules were characterized by laser light scattering (LLS) used to measure the size of the capsules in solution. The ratio of hydrodynamic radius (Rh) from dynamic LLS to the radius of gyration (Rg) from static LLS is almost unity, revealing that the entities are hollow in solution. The results suggest that the LLS method can be regarded as a good complement to the confocal laser scanning microscopy (CLSM) method for the characterization of small hollow capsules, and it possesses the advantage of not needing fluorescence labeling. 相似文献
166.
167.
Summary To match the need of high efficiency capillary column (plate number N2, Plate height H2 and carrier gas linear velocity U2), a new high efficiency packed column (N1, H1 and U1) at high carrier gas velocity with small capacity factor has been developed in the light of theoretical discussion of factors
effecting the column efficiency utilization ratio. 相似文献
168.
Band broadening in capillary columns is satisfactorily described by the Golay-equation extended to situations of appreciable pressure drop by Giddings. In practice, however, several simplifications are often made. The effect of these simplifications on the calculated values of the minimum plate height and optimum carrier gas velocity are treated systematically. 相似文献
169.
在乙烯-四氟乙烯溶液共聚合体系研究中,我们曾编制了一个简易的计算机程序,用于测定二种单体的共聚竞聚率,这一方法计算方便,而且可以避免原先作图法中的误差,结果较为可靠。前文我们报道了四氟乙烯与两个新的全氟烷基乙烯基醚的共聚合反应,并对其中一个新单体——7,7-二氯-3-氧杂-全氟庚烯-1——与四氟乙烯的共聚进行了单体竞聚率的测定。结果表明,这一新的含氟烯醚单体的聚合活性较其它已有报道的同类单体大。为了验证这一 相似文献
170.
We have investigated the effect of the Ca/P molar ratio on the structural and morphological properties of hydroxyapatite (HA) gels and nanocrystals. The sol-gel process was carried out in aqueous, and alternatively in alcoholic medium (50% water-50% ethanol), at 37°C. Gel samples were obtained by drying the sols at 37°C or at 80°C, whereas powder samples were obtained by filtering the sols. Heat treatment at temperatures as low as 300°C is enough to obtain pure HA from the gels with a Ca/P molar ratio of 1.00 and 1.67. At variance, heat treatment of the gels with a Ca/P of 2.55 always produces secondary phases. The degree of crystallinity of HA increases with the Ca/P molar ratio of the sols, and it is slightly affected by the presence of ethanol in the precipitation medium. Filtering of the sols provides powders constituted of nanocrystalline HA that exhibit degree of crystallinity, crystal morphology and thermal stability closely related to the sols composition. 相似文献