Synthesis and self‐assembly of highly incompatible polybutadiene–poly(hexafluoropropylene oxide) diblock copolymers

A versatile coupling reaction for the preparation of polybutadiene–poly‐(hexafluoropropylene oxide) (BF) diblock copolymers is described. Six diblock copolymers with different block lengths were characterized by nuclear magnetic resonance spectroscopy and size exclusion chromatography; all six had total molecular weights below 15,000. Microphase separation of the block copolymers in the bulk state was established by small‐angle X‐ray scattering (SAXS) and differential scanning calorimetry. SAXS data suggest that the diblocks are characterized by an unusually large Flory‐Huggins interaction parameter, χ, on the order of 10. However, extraction of χ from the order–disorder transition gave large (order 1) but significantly different values, thereby suggesting that these copolymers are too small and too strongly interacting to be described by block copolymer mean‐field theory. Dynamic light scattering was used to analyze dilute solutions of the title block copolymers in four selective organic solvents; the sizes of the micelles formed were solvent dependent. The micellar aggregates were large and nonspherical, and this is also attributed to the high degree of incompatibility between the two immiscible blocks. © 2005 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 43: 3685–3694, 2005     

中小企业会计规范化问题及建议

从中小企业的发展现状入手,对中小企业在发展中存在的会计规范化问题进行了探讨,对如何加强中小企业会计规范化提出了合理化建议。     

加强人力资源管理提升中小企业执行力

介绍了执行力的定义,分析了提升执行力对中小企业的重要性,指出中小企业应从选人、育人、用人以及留人4个方面来完善人力资源管理制度。     

小功率高转速蒸汽透平试验研究和优化

小功率高转速蒸汽透平试验研究和优化邵振麒（同济大学汽车工程系上海２０００９２）关键词：小蒸汽透平，效率，优化１前言回收能量和工业装置的余热及利用太阳能等新能源是节能和环保的重要措施，由此产生的机械能可供发电，气体增压等多种用途。在一些废热量不大且不宜...     

T‐joins intersecting small edge‐cuts in graphs

In an earlier paper 3 , we studied cycles in graphs that intersect all edge‐cuts of prescribed sizes. Passing to a more general setting, we examine the existence of T‐joins in grafts that intersect all edge‐cuts whose size is in a given set A ?{1,2,3}. In particular, we characterize all the contraction‐minimal grafts admitting no T‐joins that intersect all edge‐cuts of size 1 and 2. We also show that every 3‐edge‐connected graft admits a T‐join intersecting all 3‐edge‐cuts. © 2007 Wiley Periodicals, Inc. J Graph Theory 56: 64–71, 2007     

TWO ENTIRE FUNCTIONS SHARING FOUR SMALL FUNCTIONS IN THE SENSE OF _(k))(β,f)=_(k))(β,g)

This paper proves a result that if two entire functions f(z) and g(z) share four small functions aj(z) (j = 1,2,3,4) in the sense of Ek)(aj, f) = Ek)(aj,g), (j = 1,2,3,4) (k ≥ 11), then there exists f(z) = g(z).     

住宅楼人工挖孔桩的高低应变动力测试探讨

人工挖孔灌注桩是烟台市应用广泛的桩型之一．这种桩具有较高的承戴力，桩-土相互作用情况较预制桩复杂。因此探讨高低应变动力试桩法对这类桩的适宜性问题显得日益重要．本文以某住宅楱为例，探讨了人工挖孔灌注桩高低应变动力测试的原理和仪器设备、测试过程与结果，并对高应变动测中的承栽力确定、动阻力取值等问题进行了分析研究．     

三层流体界面内波的二阶Stokes解

以小振幅波理论为基础，利用摄动方法研究了三层密度成层状态下的界面内波，求得了三层成层状态下各层速度势的二阶渐近解及界面内波波面位移的二阶Stokes解.结果表明：一阶解为正弦波解，与传统线性理论的结果相一致；二阶解描述了界面波的二阶非线性修正及两界面波之间的非线性相互作用；一阶解及二阶解都依赖于各层流体的厚度及密度.Umeyama导出的理论结果为本文的特殊情形. 关键词： 三层密度成层流体 内波 二阶Stokes解 小振幅波理论     

发酵工程研究的新进展

简要介绍了DNA重组技术与发酵工程的关系,揭示了当代发酵工程研究取得的新进展,并对其未来的发展前景进行了展望。     

浅析我国小城镇交通安全现状及对策

近几年来，随着小城镇经济的发展，城镇道路建设步伐加快，机动车大量增多，小城镇道路交通安全问题也越来越突出。文章分析了小城镇道路交通安全状况及面临的突出问题，试提出一些有针对性的综合治理措施。