吴茱萸碱、吴茱萸次碱和去氢吴茱萸碱的碳氢NMR信号全指定

应用1DNMR和梯度2DNMR反相技术(gCOSY,gNOESY,gHMQC,gHMBC)研究了从疏毛吴茱萸中分离得到的三个生物碱:吴茱萸碱、吴茱萸次碱和去氢吴茱萸碱的结构,并对其碳氢NMR信号进行了全归属.     

基于多元统计学的青稞HPLC指纹图谱研究

为了筛选品质良好的青稞,选择不同产地的10批青稞样品,建立了青稞的高效液相指纹图谱,并进行了聚类分析和主成分分析,测定了儿茶素、表儿茶素和芦丁3种指标成分的含量.首先采用高效液相色谱法测得了10批青稞的色谱图,建立其共有模式,确定了11个共有峰,蓝青稞指标成分含量均高于白青稞.对共有峰数据进行聚类分析和主成分分析,10...     

木霉菌制剂对禾谷全蚀病的防治作用

木霉菌是对多种植物病原真菌有作用的拮抗体,包括Gaeumannomyces graminis var.tritici(Ggt),Pythium spp.,Rhizoctonia solani以及Fusarium spp．木霉菌能产生抑制植物病原真菌生长与活力的抗菌物质,是理想的植物病害生物防治菌。有效的生物防治方法可为农民提供低风险而又灵活的病害防治措施,特别是在需要减缓病原菌对化学杀菌剂产生抗药性的情况下。本文综合介绍了在南澳大利亚田间进行的利用康宁木霉菌(T.koningii)防治禾谷类根部病害的结果,并重点介绍澳大利亚在商品化开发方面的工作进展。在病害发生严重的情况下,康宁木霉菌可降低小麦全蚀病和丝核菌根腐病发病程度分别达2,4％和48％。小麦产量增加7％,也能降低大麦丝核菌根腐病发病程度达59％。康宁木霉菌也能够防治由Ceratocystis paradoxa引起的甘蔗凤梨病。     

南方红豆杉蒸腾强度与生态因子的关系

采用“三次称重法”测定南方红豆杉(Taxus chinensis var．mairei(Lemee et level)Cheng et L K Fu)换叶期蒸腾强度日变化、月变化,同步定点定位测定生态因子的变化,运用一元线性回归、多元回归分析蒸腾强度与生态因子的关系。结果表明：蒸腾强度日进程呈现早晚低、中午高的曲线,3月与4月为双峰,5月为单峰,即从3月到5月经历由轻蒸腾午休型到非蒸腾午休型的转变;蒸腾作用受生态因子的综合影响,与光照强度和气温显著正相关,与相对湿度显著负相关,其中光照强度影响最大,其次是气温和湿度;不同月份的蒸腾强度差异达到显著水平,引起这种差异的主导生态因子是气温。     

Two Triterpenoid Dimers from Rubus pungens Camb var. oldhamii

In the course of our continuous chemical studies of Rubus species'-', we have isolatedtwo new triterpenoid dimers (l) and (2), in their methyl ester forms (la) and (2a), fromthe aerial parts of Rubus pungens Camb var. oldhamii.Compound la, amorphous powder, m.p. 231-233'C, [a]." 12.32 (c 0.35,CH,OH ), gave a positive coloration in the Liebermann-Burchard and Molish tests whichsuggests that la was a triterpenoid glycoside. The iR spectrum revealed the presence ofhydroxyl (3435 cm-] ), est…     

日本无刺楤木离体茎段人工促成产芽技术

在自行研制的人工气候室内,以日本无刺楤木(Aralia elatavar.inermis)休眠枝条离体茎段为试验材料进行了水培人工促成产芽实验。结果表明:不同的茎段长度处理,以20 cm茎段产芽最好,差异极显著;不同的遮光处理,以遮光处理为好,但差异不明显;不同的营养条件处理,以50 mL水 50 mL全成分营养液处理最佳,但与100 mL全成分营养液无显著差异;不同的直径茎段处理,以最粗直径(平均直径12.3 mm)最佳,与最细直径之间差异极显著;不同的树龄相同直径处理,以2年生的产芽量最大,但差异不显著;同一茎段不同的芽位处理,以两侧芽产芽较好,但无显著性差异。     

Constituents of Helichrysum stoechas variety olonnense

The isolation of 18 phenolic compounds (-pyrones, phloroglucinols, phenolic acids, flavonoids, and coumarin) from the aerial parts of Helichrysum stoechas var. olonnense is reported.     

The maximum asymptotic bias of S-estimates for regression over the neighborhoods defined by certain special capacities

The maximum asymptotic bias of an S-estimate for regression in the linear model is evaluated over the neighborhoods (called (c,γ)-neighborhoods) defined by certain special capacities, and its lower and upper bounds are derived. As special cases, the (c,γ)-neighborhoods include those in terms of -contamination, total variation distance and Rieder's (,δ)-contamination. It is shown that when the model distribution is normal and the (,δ)-contamination neighborhood is adopted, the lower and upper bounds of an S-estimate (including the LMS-estimate) based on a jump function coincide with the maximum asymptotic bias. The tables of the maximum asymptotic bias of the LMS-estimate are given. These results are an extension of the corresponding ones due to Martin et al. (Ann. Statist. 17 (1989) 1608), who used -contamination neighborhoods.     

Seed Oils of Fifteen Ebenus Taxa Growing in Turkey

Oil yields and compositions from seeds of 15Ebenustaxa growing in Turkey were investigated. The yields were found between 4.0% and 13.0%. The seeds ofE. Barbigerashowed the highest whileE. Plumosavar.plumosashowed the lowest yield of oil among the 15 taxa investigated. GC/MS showed that linoleic acid (42.8-55.6%), palmitic acid (13.8-23.6%), and oleic acid (15.9-23.6%) are the main fatty acid components of all the species     

台湾扁柏和台湾杉的核型分析

分析了台湾扁柏Ｃｈａｍａｅｃｙｐａｒｉｓ ｏｂｔｕｓａ ｖａｒ．ｆｏｒｍｏｓａｎａ和台湾杉Ｔａｉｗａｎｉｎａ ｃｒｙｐｙｏｍｅｒｉｏｉｄｅｓ的核型,前者有８对中部着丝粒和３对近中着丝粒染色体,属２Ａ类型,７号染色体带一随体,后者有７对中部着丝粒和４对近中部着丝粒染色体,属２Ｂ类型。