2003年度图书馆学核心期刊中参考咨询服务论文的研究与分析

通过对2003年度在图书馆学核心期刊中所发有关参考咨询服务论文进行统计与分析，力求能客观真实地反映我国目前参考咨询服务的研究现状和水平，把握其发展脉络，为今后的研究提供借鉴和参考。     

Method to reduce the memory effect of mercury in the analysis of fish tissue using inductively coupled plasma mass spectrometry

The routine determination of mercury (Hg) by inductively coupled plasma mass spectrometry (ICP-MS) is affected by a pronounced memory effect in the sample introduction system. This results in long washout times for the analyte, which affects the accuracy and reliability of the analytical procedure. By using a combination of flow injection sample introduction and a sulfur-containing compound in the carrier solution, it was possible to decrease the memory effect of mercury to that for the internal standard (rhodium). The carrier solution contained 2-mercaptoethanol (2-ME) and the developed method was evaluated using three different fish tissue certified reference materials: CRM 464 (BCR, Brussels); DORM-1; and DORM-2 (NRC, Canada). The samples were mineralized using a combination of concentrated nitric acid and hydrogen peroxide and heating in a closed microwave oven. The developed flow injection ICP-MS procedure gave values for total mercury in all three CRM materials in agreement with the certified concentration range. Cold vapour atomic fluorescence spectrometry (CV-AFS) confirmed the results from the developed method. The developed flow injection method had a detection limit (defined as three times the standard deviation of the blank concentration) for mercury of 5.1 μg l⁻¹.     

西北师范大学图书馆文献资源的共建共享

分析了西北师范大学图书馆与各院系资料室文献资源的管理现状；指出“联合采购，统一编目”，建立全校文献书目数据库的必要性和可行性．并详细介绍了其实施方案。。     

定速风力发电机模型参考自适应控制

在对定速风力发电机建模的基础上,设计了模型参考自适应控制器,并进行了跟随性能和抗干扰性能仿真,仿真结果表明自适应控制器的自适应能力很好.     

Simultaneous confidence and prediction bands in the certification of pressure-volume curves for the pore size analysis of solids by means of mercury porosimetry

The pore size analysis of solids is widely applied in chemical industries, materials engineering, ceramic production, environmental engineering, catalysis, chromatography, nanotechnology, and many other fields. In spite of several new methods used for determining the pore size distribution of meso- and macropores [see IUPAC Recommendations of 1994], mercury porosimetry has remained one of the most popular methods employed for the characterisation of porous materials. In this paper, a new way is described for the estimation of certified pressure-volume curves from experimental curves measured by different laboratories in connection with the certification of new reference materials for a comparatively low-pressure range of mercury intrusion (<2 MPa). Simultaneous confidence and prediction bands for the certified pressure-volume curves are constructed by bootstrapping.     

论网络环境下的高校图书馆参考咨询服务

本文主要论述了网络环境下的高校图书馆参考咨询常见的服务项目及其特点,研究了网络环境下的高校图书馆参考咨询服务的发展方向。     

高校图书馆与资料室发展的协调互补

高校中,图书馆系统与各个学院、系、专业或研究所等并存着一个资料室系统。前者是为一个学校服务的,后者则是为一个学院、系、专业或研究所等科研单位服务的,这种现象的存在,在多大程度上影响着中国高校的教学和科研,我们很难在现行的层面上进行观察,但有一点是可以肯定的,那就是,图书馆与资料室之间,在工作上存在着不同的性质和内容,具有互补性,其间的协调发展是不容忽视的。     

国外高校筹资的主要方式与启示

资金问题是影响高等教育事业发展的关键因素。本文介绍了国外高校筹资的七种主要方式。实行收费政策；采取输出教育模式。发行教育债券；加强与政府和社区的联系；出让技术和专利；建立高校公司；制度化和规范化募捐工作等。文章简要分析了国外高校筹资方式对我国高校的启示，为我国高校筹资工作提供经验借鉴，指导我国高枝筹资工作实践。     

玉林话亲属称谓词语初探

比较详细地列举玉林话的亲属称谓词语,并通过与普通话的比较,从词汇的角度探讨玉林话亲属称谓词语的特点。     

对高校图书馆图书资料开发利用的思考

就高校图书馆图书资料如何开发利用提出了几点看法.