Reinforcement effect of MAA on nano‐CaCo3‐filled EPDM vulcanizates and possible mechanism

Methacrylic acid (MAA) was used as in situ surface modifier to improve the interface interaction between nano‐CaCO₃ particle and ethylene–propylene–diene monomer (EPDM) matrix, and hence the mechanical properties of nano‐CaCO₃‐filled EPDM vulcanizates. The results showed that the incorporation of MAA improved the filler–matrix interaction, which was proved by Fourier transformation infrared spectrometer (FTIR), Kraus equation, crosslink density determination, and scanning electron microscope (SEM). The formation of carboxylate and the participation of MAA in the crosslinking of EPDM indicated the strong filler–matrix interaction from the aspect of chemical reaction. The results of Kraus equation showed that the presence of MAA enhanced the reinforcement extent of nano‐CaCO₃ on EPDM vulcanizates. Crosslink density determination proved the formation of the ionic crosslinks in EPDM vulcanizates with the existence of MAA. The filler particles on tensile fracture were embedded in the matrix and could not be observed obviously, indicating that a strong interfacial interaction between the filler and the matrix had been achieved with the incorporation of MAA. Meanwhile, the presence of MAA remarkably increased the modulus and tensile strength of the vulcanizates, without negative effect on the high elongation at break. Furthermore, the ionic bond was thought to be formed only on filler surface because of the absolute deficiency of MAA, which resulted in the possible structure where filler particles were considered as crosslink points. © 2006 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 44: 1226–1236, 2006     

体育专业在校生运动损伤情况调查分析

采用问卷调查和实地访问相结合的方法,对河南省部分高校体育院、系的体育教育专业在校学生受伤情况进行了调查,从发生运动损伤的性质、运动项目、受伤的部位、引起损伤的原因等方面分析,结果表明：在大学期间学生受伤情况相当普遍,已严重影响正常教学和训练.建议应尽快强化学生预防损伤的意识并提出预防运动损伤的综合性措施.     

论行政机关的公司登记行为

行政机关的公司登记行为是一种特殊的具体行政行为。公司登记机关应对登记申请材料进行形式审查而非实质审查。因此，公司登记机关是否违法，及法院对公司登记行为的合击性进行审查，也主要是围绕公司登记机关是否尽到形式审查之义务这一中心。     

枣离体授粉及胚珠培养初探

对晋矮1号×壶瓶枣的离体杂交以及杂交子房和胚珠的离体培养进行了研究.结果表明:附加1.0mg/LIBA的KM8p培养基对枣子房的离体培养较为适宜,ZT对子房的成活具有促进作用,子房的愈伤组织化可减缓子房室内胚珠的败育程度.     

英国维多利亚时期"家庭天使"的内涵和特点

英国维多利亚时期伴随工业化的深入,强大的中产阶级不仅创造了这一时期的时代价值观,而且还形成了与以往不同的妇女观."家庭天使"成为他们心目中完美的女性形象.     

北方铜业冶炼厂硫酸系统风机单机运行实践

详细介绍了S1200-16型鼓风机在北方铜业冶炼厂的使用情况，以及S1200-16型鼓风机的结构、技术参数，提出了为确保风机的正常运行所采取的处理措施。     

二十世纪上半叶中国农村婚姻制度探微

20世纪上半叶中国社会经历了剧烈的变迁。农村的婚姻制度并没有在择偶方式即“父母之命，媒妁之言”上发生根本的变化。“父母之命”依然代表着农村择偶方式的主流。而在一些交通便利、距离大城市较近的农村，尤其是沿海、沿江的农村地区出现了一些新变化。择偶方式要产生根本的变化将是一个长期的过程。     

Moisture sorption, transport, and hydrolytic degradation in polylactide

Management of moisture penetration and hydrolytic degradation of polylactide (PLA) is extremely important during the manufacturing, shipping, storage, and end-use of PLA products. Moisture transport, crystallization, and degradation, in PLA have been measured through a variety of experimental techniques including size-exclusion chromatography, differential scanning calorimetry, and X-ray diffraction. Quartz crystal microbalance and dynamic vapor sorption experiments have also been used to measure moisture sorption isotherms in PLA films with varying crystallinity. A surprising result is that, within the accuracy of the experiments, crystalline and amorphous PLA films exhibit identical sorption isotherms.