一种石英晶体谐振器频率粗调机系统

设计一个基于单片机及OPLD的针对32768Hz石英谐振音叉片进行自动加工的机器,该机器用于实现对石英音叉片谐振频率及阻抗的磨削调整。分析了机器结构及磨削机理,并根据多个参考变量设计加工算法以提高加工效率与产品精度。通过一个串口通信网络实现多机器的加工数据通信以增强生产管理效能。     

长微圆管道气体流动的简化计算

从N－S方程出发,考虑稀薄气体效应,推导出长微圆管道中压力驱动的可压缩气体流动的简化控制方程组;采用迭代方法求解此方程组,得到了流动的速度分布、密度分布、质量流量;并分析了影响流量的因素。     

大尺寸石英砂环氧树脂胶结人造岩心制备

大尺寸人造岩心不仅可以模拟储层的非均质性、注采井网关系,还可以模拟油水在平面或者纵向上的运移规律及饱和度分布,近年来大尺寸人造岩心被广泛地应用在油气藏开发各类物理模拟实验中。为制作出与真实油藏物性尽可能接近的大尺寸人造岩心,从渗透率、孔隙结构、润湿性控制、黏土矿物添加等方面研究了其制作工艺,并研究了石英砂粒度中值、加压强度、胶粘剂用量、黏土矿物含量等对人造岩心渗透率和孔隙度的影响。通过介绍的制作方法实际制作了与某非均质油藏物性相似的层内、层间、平面非均质大尺寸石英砂环氧树脂胶结人造岩心,物性参数测定结果显示制作的大尺寸非均质人造岩心渗透率、孔隙结构等物性参数与实际油藏非常接近,可以代替真实油藏岩心进行部分模拟实验,为油藏物理模拟实验的发展提供了新的技术和手段。     

A Novel Ion-Selective Sensor for Procaine Hydrochloride Based on a Piezoelectric Quartz Crystal Coated with a Procaine Tetraphenylborate PVC Membrane

 A novel ion-selective sensor for procaine hydrochloride has been proposed and applied successfully to analysis of pharmaceutical preparations. The sensor is based on modification of the Ag-electrode of an AT-cut piezoelectric quartz crystal with a PVC membrane containing procaine tetraphenylborate. A linear relation between the logarithm of the response frequency and the logarithm of the procaine hydrochloride concentration was found experimentally and could be explained by combination of a modified Sauerbrey equation and the Freundlich isotherm. The detection range was from 8.3 × 10⁻⁸ to 5.0 × 10⁻³ M with a detection limit of 8.3 × 10⁻⁸ M. The selectivity of the sensor and the influence of experimental parameters such as solution pH and detection time were investigated. Received February 10, 1999. Revision October 10, 1999.     

矩形AT切割石英晶体谐振器的振动分析与设计

随着石英体波谐振器向小型化和高性能方向的发展 ,控制晶片中的模式耦合问题便成了保证晶振性能的关键 从R .D .Mindlin的两维方程入手 ,分析了AT切石英晶片中的振动模式 首先得出了无穷大晶片中的色散关系 ,继而又得到了矩形晶片振动频率和长厚比 (晶片的长度与厚度的比值 )、宽厚比 (晶片的宽度与厚度的比值 )之间的关系 ,并与实际生产中所采用的数据进行对比 ,符合得十分好 最后以计算结果为指导 ,举例了一种 4MHz谐振器的分析设计     

TiO2对粉煤灰及石英砂制备微晶玻璃组织转变的影响

利用粉煤灰与石英砂制备微晶玻璃,并对其进行不同工艺的热处理．通过对热处理后的试样研究发现：当粉煤灰质量分数为30％,未加TiO2时,试样在780℃加热时首先析出过渡相Ca2SiO。,在随后的高温晶化过程中,过渡相溶解消失,析出更稳定的平衡相钙长石;当TiO2质量分数为0—15％时,随着TiO2含量的增加,在780℃加热时由析出梭形的Ca2SiO。微晶转变为析出粒状的钙长石微晶;当粉煤灰质量分数增加到40％,TiO2质量分数为3．5％时试样中出现网状微晶组织,而加入的形核剂TiO2质量分数达到5％时试样中无网状微晶组织出现,说明TiO2对网状组织的析出具有明显抑制作用．     

Signal Enhancement using A Swellable Polymer TSM Acoustic Wave Sensor Coating

ABSTRACT

The generation of large changes in the crystal frequency is a highly sought-after goal in designing a successful thickness-shear mode (TSM) acoustic wave sensor application. We examined the potential for modulating the mass loading and viscoelastic properties of a swellable polymeric coating to achieve this goal. Using a 10 MHz AT-cut crystal with an immobilized coating of a styrene-divinylbenzene copolymer, a high molecular weight target analyte with complementary ionic and molecular binding properties was selected. Injection of the antibiotic cefoperazone in a sodium acetate buffer generated exceptionally large changes in frequency, in the range 500 - 5000 Hz. The rate of change in frequency is proportional to the analytical concentration. A multi-step regeneration protocol allows the coating to be reused multiple times. These results suggest that TSM sensor sensitivities can be significantly enhanced for selected analytes by the judicious selection of an appropriate swellable polymer coating.     

The preparation of thick-film glass capillary columns

A detailed method for the routine preparation of glass capillary columns is presented. The method consists of coating a glass tube with quartz powder prior to pulling the tube into a capillary. The inner surface of the capillary consists of an even distribution of quartz particles fused to the walls. This surface has been found readily deactivated by standard procedures and ideal for the preparation of thick-film glass capillary columns. The method has been thoroughly tested in two independent laboratories to ensure that the procedures described are reproducible.     

X-ray diffraction in AT-cut quartz single crystal at acoustic excitation at the fundamental frequency

X-ray diffraction on different atomic planes of an AT-cut quartz crystal is studied experimentally in the Laue geometry in case of excitation by acoustic waves at the first resonant (fundamental) frequency. Acoustic waves lead to an increase in the integral intensity of the reflection-diffracted beam. The amplification coefficients in reflection are measured in dependence on the amplitude of a.c. voltage applied to the crystal at the resonant frequency. The frontal distributions of the intensity of the beam diffracted in the reflection direction are obtained for different atomic planes.     

火焰原子吸收法测定大豆、茶叶及合金中微量铁和锰

本文用ＦＡＡＳ法对大豆、茶叶及合金中的铁和锰进行研究［１－４］。根据实验结果，铁的变异系数为１．０～３．７％，回收率为９８～１０１％；锰的变异系数为２．４～３．５％，回收率９７～１０３％，均得到较为满意的结果，具有较好的实用价值。