超高效液相色谱法同时测定食品塑料包装材料中的紫外吸收剂和抗氧化剂

超声萃取结合超高效液相色谱(UPLC)技术,建立了食品塑料包装材料中14种紫外吸收剂及抗氧化剂(UV-0,UV-9,UV-71,UV-329,UV-326,UV-327,UV-234,UV-360,抗氧化剂2246,抗氧化剂425,TH-1790,抗氧化剂3114,抗氧化剂1010和抗氧化剂1076)的高通量检测方法。样品经三氯甲烷-甲醇超声提取,C18色谱柱分离后,乙腈和0.1%甲酸水为流动相梯度洗脱,二极管阵列检测器测定。14种物质在一定的浓度范围内线性关系良好,相关系数(r2)均不低于0.999 2,方法定量下限(S/N=10)为8.0~33.0 mg/kg,平均回收率为83.6%~116.2%,相对标准偏差(RSD,n=6)为1.3%~9.5%。方法具有前处理简单、净化效果好等特点,适用于食品塑料包装中14种紫外吸收剂及抗氧化剂的同时测定。     

硬聚氯乙烯三通管挤胀成型的有限元模拟及优化

采用Ansys^®通用分析软件对硬聚氯乙烯(UPVC)三通管的挤胀成型过程进行了有限元模拟和优化。通过模拟获得了三通管挤胀成型过程中的主要失效形式。采用单步循环法模拟了不同过渡圆角情况下三通管的成型过程,确定了合理的设计域,在此基础上分别采用子问题逼近法和一阶优化法获得了对于不同过渡圆角情况下三通管优化的设计参数组合。在模拟和优化的基础上,利用自行设计的实验台成功地实现了UPVC三通管的挤胀成型。实验和模拟研究结果表明,挤胀成型方法对于一些特定类型制品的成型是可行的。     

《塑料成型工艺及模具设计》课程教学改革与实践

就模具设计与制造专业主干课程《塑料成型工艺及模具设计》的教学内容、教学手段与方法、教学实训的改革进行了探讨,提出了具体的改革方案。从而改善了教学效果,提高了学生的实践能力,为突出高职办学特色,提高人才培养质量做出了有益探索。     

二维塑性变形中应变分布测量的新方法

为了解决复杂构件体积成形过程中金属变形流线和塑性应变分布难于定量测量的问题,本文提出了一种用套环螺纹的测量方法.该方法不用替代材料即可实现对体积成形过程的三维塑性变形的测定,进行定量分析.利用该方法对轮毂件成形过程中四条流线及其轴向应变进行了测量分析,并将实验结果与数值模拟进行了对比.用套环螺纹法获得的应变分布与有限元模拟的应变分布吻合.说明该方法是测量体积成形过程中塑性应变分布较为有效的实验方法.     

直缝焊管排辊成形中预成形段的动力显式仿真

考虑到直缝焊管的排辊成形过程非常复杂,其间涉及明显的非线性,为了更好地了解板带的成形规律,针对406 mm焊管排辊成形机组的预成形段建立了弹塑性大变形有限元模型,采用动力显式算法进行了仿真计算,分别得到了预成形段管坯的等效塑性应变分布和几何变形,并通过开口度和板宽的测量验证了仿真的准确性.研究结果表明:在预成形段时最大塑性变形发生在带钢的边缘,其次是带钢中心以及带钢与粗成形轧辊端面接触的区域;弯边轧辊对带钢边缘的变形贡献最大.     

Novel Plastic Encapsulation Holding Method for Automobile Glass Using Injection Molding Process

Glass positioning and holding is difficult in the process of injection molding encapsulation of automobile glass. A suction cup or soft resin is always introduced in this process. However, these materials cannot hold glass tightly, thus resulting in the unsteady quality of toughened glass and encapsulated plastic. To solve this problem, a novel holding method called magnetic high-pressure holding with twin bags is proposed to address the features of toughened glass and the encapsulation injection process. Firstly, a pair of permanent magnets is introduced as energy source, followed by the magnetization of a couple of magnetic particle bags. Contact between the single bag and the glass surface will enable the couple of magnetic particle bags to hold glass tightly and to self-adapt the freeform of the glass. Secondly, an experimental system with mechanical and control systems is designed. This system is controlled by the opening and closing force of the mold, which turns the magnetic field on or off to hold or loosen the glass. The magnetic field distributions are measured at important positions of the permanent magnets and in the magnetized particles in the experiments to determine the holding performance. Finally, the process of determining the parameters of the magnet and its attenuation is analyzed, including the minimum friction force between the glass and the particle bag during injection molding, the magnetic energy product and the magnetized filed distributions, and the re-checklng method for these parameters. The theoretical analysis and the experimental result show that this flexible holding system may produce sufficient holding force, which not only protects glass but serf-adapts the glass freeform as well. The production practice meets the technical requirements of injection molding with a defect-free surface, with no scratches and cracks on the glass and no slight glass movements in the mold cavity.     

基于应变的热采井套管设计方法

提出基于应变的热采井套管设计方法,确定基于应变的设计准则,通过建立三维弹塑性有限元模型,模拟分析热采井多轮次生产过程中应力和应变变化规律,并以胜利油田A井为例进行实例设计。结果表明,该设计方法密切结合热采井"注-焖-采"生产过程,可考虑多轮次循环温度载荷对套管的损伤程度,通过计算多轮次生产条件下套管上的累积塑性应变,依据热采井生产轮次要求及应变准则,科学灵活地设计套管,可以为热采井套管柱设计提供新思路。     

大长细比动能弹体弹塑性动力响应数值模拟

针对侵彻体结构动态响应问题,利用有限元程序得到Lagrange六面体常应力积分单元应力张量σij值,建立了获得侵彻体截面轴力、剪力、弯矩等广义载荷的方法.求解并分析了垂直侵彻和斜侵彻实验的大长细比弹体弹塑性动力响应.结果表明,基于最大惯性载荷的垂直侵彻弹体截面载荷分析对弹体强度设计是安全的,斜侵彻时轴向载荷与侧向载荷的交互作用可采用线性交互作用屈服面求解.     

The Principle of Interaction between Plastic Volumetric and Shear Strains for Unsaturated Soils

The principle of interaction between plastic volumetric and shear strains for rock and soil has been extended to the field of unsaturated soils. Two new interactions of suction-plastic volumetric strain and pore air pressure-plastic volumetric strain appear in the unsaturated state of a soil except the interaction between plastic volumetric and shear strains. It is very important to find that the suction possesses a dual property, which is the origin of generating its special functions. Thereby the effect of the suction on volumetric strain includes two opposite aspects. By means of this property of suction, the physical significance of effective stress parameter, effects of suction on volume change and preconsolidation pressure, and the mechanism of collapse upon wetting all can be explained. In addition, it is theoretically proved by application of this principle of interaction that the critical state line for unsaturated soils exists, and is unique and independent of the stress history.     

Dependence of the tidal deformability of neutron stars on the nuclear equation of state

Within the Bayesian framework, using an explicitly isospin-dependent parametric equation of state (EOS) for the core of neutron stars (NSs), we studied how the NS EOS behaves when we confront it with the tidal deformabilities \begin{document}$ \Lambda_{1.4} $\end{document} of canonical NSs with different error and different lower boundaries, and with the tidal deformabilities of massive NSs. We found that it does not significantly improve the constraints on the NS EOS but has a weak effect on narrowing down the slope parameter of the symmetry energy by decreasing the measurement errors of \begin{document}$ \Lambda_{1.4} $\end{document}. Both the isospin-dependent and isospin-independent parts of the NS EOS were significantly constrained and raised as the tidal deformabilities of massive NSs were adopted in the calculations, especially in high-density regions. We also found that \begin{document}$ \Lambda_{1.4} $\end{document} is more competent to limit the curvature parameter than the slope parameter of the symmetry energy, whereas the opposite occurs for the radius of canonical NSs \begin{document}$ R_{1.4} $\end{document}. The tidal deformability of an NS with two times the solar mass \begin{document}$ \Lambda_{2.0} $\end{document} is more sensitive to skewness than the curvature parameter of the symmetry energy, and \begin{document}$ \Lambda_{1.4} $\end{document} and \begin{document}$ R_{1.4} $\end{document} have no correlation with the former.