全文获取类型
收费全文 | 1289篇 |
免费 | 11篇 |
国内免费 | 28篇 |
专业分类
化学 | 53篇 |
力学 | 4篇 |
综合类 | 4篇 |
数学 | 15篇 |
物理学 | 25篇 |
综合类 | 1227篇 |
出版年
2024年 | 2篇 |
2023年 | 5篇 |
2022年 | 7篇 |
2021年 | 11篇 |
2020年 | 12篇 |
2019年 | 4篇 |
2018年 | 9篇 |
2017年 | 6篇 |
2016年 | 17篇 |
2015年 | 28篇 |
2014年 | 63篇 |
2013年 | 47篇 |
2012年 | 60篇 |
2011年 | 114篇 |
2010年 | 78篇 |
2009年 | 94篇 |
2008年 | 118篇 |
2007年 | 140篇 |
2006年 | 119篇 |
2005年 | 93篇 |
2004年 | 74篇 |
2003年 | 58篇 |
2002年 | 40篇 |
2001年 | 34篇 |
2000年 | 19篇 |
1999年 | 18篇 |
1998年 | 5篇 |
1997年 | 12篇 |
1996年 | 8篇 |
1995年 | 8篇 |
1994年 | 8篇 |
1993年 | 6篇 |
1992年 | 2篇 |
1991年 | 4篇 |
1988年 | 4篇 |
1987年 | 1篇 |
排序方式: 共有1328条查询结果,搜索用时 0 毫秒
71.
大学生马基雅维利主义倾向探微 总被引:1,自引:0,他引:1
个体的马基雅维利主义倾向影响其对人际交往的态度与实践。文章采用西方成熟量表,通过对南京某高校274名大学生样本研究结果发现:多数人的马基雅维利主义水平比较低,约三分之一强的人属于高马基雅维利主义者;男生要比女生表现出较高的马氏水平;非商科学生比商科学生表现出较高的水平;三个年级中,大一学生的马氏水平最高;在所有学生中,城市大学生的马氏水平最高,来自农村与小城镇大学生的马氏水平几乎相同。 相似文献
72.
姜云鹤 《科技情报开发与经济》2016,(3):153-154
社会保障在维系社会稳定、推动社会公共服务事业发展的过程中发挥着重要作用,必须给予高度重视。阐释了信息化建设对于推动社会保障档案管理的必要性,从应用策略、管理策略及安全保障策略3个方面提出了社会保障档案管理的信息化建设的具体方案。 相似文献
73.
Jingkang Li Yanxiao Jiang Ying Sun Xinghua Wang Pinyi Ma Daqian Song Qiang Fei 《Journal of separation science》2022,45(3):697-705
In the present study, we propose a novel method for the extraction of parabens in personal care products. A new, simple adsorptive material was obtained by combining metal-organic frameworks and melamine sponges using the adhesive property of polyvinylidene fluoride. This new material, metal-organic frameworks/melamine sponges, was found to be particularly suitable for solid-phase extraction. The structural characteristics of metal-organic frameworks/melamine sponges were first analyzed by scanning electron microscopy. Subsequently, solid-phase extraction was performed on sample solutions, and the extracted substances were then analyzed by high-performance liquid chromatography. Following optimization of important experimental conditions, excellent recovery rates were obtained. Our novel method was then applied to the extraction of four parabens (methylparahydroxybenzoates, ethylparahydroxybenzoates, propylparahydroxybenzoates, and butylparahydroxybenzoates) from real samples. The results yielded limits of detection of 0.26–0.41 ng/mL. The inter- and intra-day recoveries were 104.0–109.7% and 91.2–98.1%, respectively (relative standard deviation, <13.8%). 相似文献
74.
Mohsen Gorji Saeedeh Mazinani Abdol-Rahim Faramarzi Saeedeh Ghadimi Mohammadreza Kalaee Ali Sadeghianmaryan Lee D. Wilson 《Molecules (Basel, Switzerland)》2021,26(12)
Textiles coated with silver nanowires (AgNWs) are effective at suppressing radiative heat loss without sacrificing breathability. Many reports present the applicability of AgNWs as IR-reflective wearable textiles, where such studies partially evaluate the parameters for practical usage for large-scale production. In this study, the effect of the two industrial coating methods and the loading value of AgNWs on the performance of AgNWs-coated fabric (AgNWs-CF) is reported. The AgNWs were synthesized by the polyol process and applied onto the surface of cotton fabric using either dip- or spray-coating methods with variable loading levels of AgNWs. X-ray diffraction, scanning electron microscopy (SEM), infrared (IR) reflectance, water vapor permeability (WVP), and electrical resistance properties were characterized. The results report the successful synthesis of AgNWs with a 30 μm length. The results also show that the spray coating method has a better performance for reflecting the IR radiation to the body, which increases with a greater loading level of the AgNWs. The antibacterial results show a good inhibition zone for cotton fabric coated by both methods, where the spray-coated fabric has a better performance overall. The results also show the coated fabric with AgNWs maintains the level of fabric breathability similar to control samples. AgNWs-CFs have potential utility for cold weather protective clothing in which heat dissipation is attenuated, along with applications such as wound dressing materials that provide antibacterial protection. 相似文献
75.
Felix Burkhardt Carl G. Schirmeister Christian Wesemann Massimo Nutini Stefano Pieralli Erik H. Licht Marc Metzger Frederik Wenz Rolf Mülhaupt Benedikt C. Spies 《Molecules (Basel, Switzerland)》2020,25(24)
A polyolefin with certified biocompatibility according to USP class VI was used by our group as feedstock for filament-based 3D printing to meet the highest medical standards in order to print personal protective equipment for our university hospital during the ongoing pandemic. Besides the chemical resistance and durability, as well as the ability to withstand steam sterilization, this polypropylene (PP) copolymer is characterized by its high purity, as achieved by highly efficient and selective catalytic polymerization. As the PP copolymer is suited to be printed with all common printers in fused filament fabrication (FFF), it offers an eco-friendly cost–benefit ratio, even for large-scale production. In addition, a digital workflow was established focusing on common desktop FFF printers in the medical sector. It comprises the simulation-based optimization of personalized print objects, considering the inherent material properties such as warping tendency, through to validation of the process chain by 3D scanning, sterilization, and biocompatibility analysis of the printed part. This combination of digital data processing and 3D printing with a sustainable and medically certified material showed great promise in establishing decentralized additive manufacturing in everyday hospital life to meet peaks in demand, supply bottlenecks, and enhanced personalized patient treatment. 相似文献
76.
Ramandeep Kaur Heena Ripneel Kaur Aman Grover Susheela Rani Ashok Kumar Malik Abuzar Kabir Kenneth G. Furton 《Journal of separation science》2020,43(13):2626-2635
A simple, fast, and sensitive analytical protocol using fabric‐phase sorptive extraction followed by high performance liquid chromatography with ultraviolet detection has been developed and validated for the extraction of five parabens including methylparaben, ethylparaben, propylparaben, butylparaben, and benzylparaben. In the present work, sol‐gel polyethylene glycol coated fabric‐phase sorptive extraction membrane is used for the preconcentration of parabens (polar) from complex matrices. The use of fabric‐phase sorptive extraction membrane provides a high surface area which offers high sorbent loading, shortened equilibrium time, and overall decrease in the sample preparation time. Various factors affecting the performance of fabric‐phase sorptive extraction, including extraction time, eluting solvent, elution time, and pH of the sample matrix, were optimized. Separation was performed using a mobile phase consisting of water:acetonitrile (63:37; v/v) at an isocratic elution mode at a flow rate of 0.9 mL/min with wavelength at 254 nm. The calibration curves of the target analytes were prepared with good correlation coefficient values (r2 > 0.9955). The limit of detection values range from 0.252 to 0.580 ng/mL. Finally, the method was successfully applied to various cosmetics and personal care product samples such as rose water, deodorant, hair serum, and cream with extraction recoveries ranged between 88 and 122% with relative standard deviation <5%. 相似文献
77.
浅谈信息时代的档案管理和档案资源开发 总被引:2,自引:1,他引:1
孟庆琳 《科技情报开发与经济》2006,16(2):77-78
新时期全新的档案管理体系要求档案工作者不断提高自身素质,根据社会需求,主动开发档案信息资源,创新档案管理体系,以充分发挥档案的价值作用。 相似文献
78.
完善的市场经济离不开信用经济,我国目前的个人信用经济还不太发达,主要是信用保证缺失,没有完善的个人信用体系。要发展我国的个人信用经济就要打破这个桎梏,学习外国先进经验,结合我们自身的实际,阶段性地建立我国的个人信用体系。 相似文献
79.
提出一种基于Ultra Search的桌面搜索设计和实现方案,简要介绍了Ultra Search体系架构和各个组件的功能,然后给出该桌面搜索的框架和各个组件的实现细节,并和多个桌面搜索工具在相同的数据源上进行测试,结果表明,该桌面搜索有不错的搜索性能。 相似文献
80.
随着高校教师越来越多地同时从事教学、科研和行政等各方面工作,有必要对各类相关信息进行简单方便的管理查询。笔者利用手机携带方便的特点,在基于Java 2 Micro Edition(J2ME)规范的手机上研制了教师个人信息助理软件。该软件功能系结合高校实际情况而设计,解决了手机数据导入和更新的问题。经过在多种手机上使用,证明该软件可以正常使用,并有助于提高教师的工作效率。 相似文献