药用辅料——高分子聚合材料测定方法的正交试验

设计正交试验,建立药用辅料——高分子聚合材料测定方法.以L9(34)正交试验考查该方法的4个重要因素及水平.确立方法后按2010年中国药典要求做方法学研究.结果表明:该法检测的线性范围为2～100μg.mL-1;r=0.999 8;检出限为0.5μg.mL-1;该方法的平均回收率为0.96;日内RSD为0.02.该方法符合2010年中国药典关于杂质限量检测方法的规定,是检测此类PLLA辅料中乳酸含量的可行方法.     

基于Vray材质表达真实性在室内效果图制作中的研究

材质传达的真实性是室内设计方案表现的重要因素,真实的材质表现能准确的诠释设计师对于方案中各个结构、装饰物、家具等的质感设计,也更能与客户的审美产生共鸣.本文研究了Vray材质编辑的基本原理,并提供室内常用材质调节的基本思路,希望能够为室内设计人员的设计与表现提供参考.     

Magnetic fluid poly(ethylene glycol) with moderate anticancer activity

Poly(ethylene glycol) (PEG)-containing magnetic fluids - magnetite (Fe₃O₄) stabilized by sodium oleate - were prepared. Magnetic measurements confirmed superparamagnetic behaviour at room temperature. The structure of that kind of magnetic fluid was characterized using different techniques, including electron microscopy, photon cross correlation spectroscopy and small-angle neutron scattering, while the adsorption of PEG on magnetic particles was analyzed by differential scanning calorimetry and Fourier transform infrared spectroscopy. From the in vitro toxicity tests it was found that a magnetic fluid containing PEG (MFPEG) partially inhibited the growth of cancerous B16 cells at the highest tested dose (2.1 mg/ml of Fe₃O₄ in MFPEG).     

长壁软底工作面柱鞋参数分析

为有效控制单体支柱长壁工作面顶板,针对属于Ⅰ级极软底板的工作面,建立了单体柱鞋的力学模型,分析了柱鞋受力的载荷分布.计算了柱鞋的合理尺寸,包括柱鞋的厚度,柱鞋的大小等.通过对工作面现有支护方式的分析,确定其合理的柱鞋选型和参数,确保了支护系统的刚度,该支护系统在现场取得了良好的应用效果.     

栀子蓝色素的制备及其抗氧化活性研究

用米曲霉发酵产物水解栀子苷,水解产物与味精反应制备栀子蓝色素,采用DM-2大孔树脂对产品进行精制,通过DPPH·捕获分光光度法测定栀子蓝色素精制前后的抗氧化活性.栀子蓝制备的最佳条件为:10.64 g栀子苷和129.36 g水混合后,加入米曲霉发酵液9.8 m L,在50℃,160¹80 r/min下水解6 h后,与3.15 g味精反应40 h,80℃保温30 min.所获栀子蓝色素粗品的色价(E1%1cm)为90.56,经DM-2大孔树脂纯化后产品色价提高至180.01%,收率为90.96%.抗氧化实验表明栀子蓝色素粗品和精制品均能有效清除DPPH·,且精制后的栀子蓝色素产品清除DPPH·的能力增强.     

Statistical inference for simple tree order in the means of stochastic order on stratified contingency tables

In this paper, we consider testing the hypothesis that all multinomial populations in the stratified contingency table are identically distributed against the alternative that all these popula-tions are in simple tree order. We provide an asymptotic represen-tation of the order-restricted maximum likelihood estimate of the unknown parameters. The resulting estimators are proven to be n-consistent and asymptotically normal under appropriate con-ditions. A chi-squared test method is used for this hypothesis t...     

光散射及其对血液流变参数的测量

 物理学中光散射现象的应用是通过捕捉散射源的散射光谱而获得被试物中丰富信息的，尤其是拉曼散射光谱和布里渊散射光谱，更能给出散射源的精细信息。这种检测具有无毒、无创、快速、准确等优点，若能应用于医学临床中，将使医学临床检测数据更加趋于准确，并能减轻病人的痛苦。本文描述了试图将这一物理现象应用于血液流变参数的检测中时所做的前期分类检测，以及对实验光路、设备、实验方法等所做的研究探索工作。     

The effect of resistant starches on fat oxidation in healthy adults as measured by a 13CO2-breath test

A resistant starch (RS) mixture (MIX) consisting of fibre of potatoes (FP) and wrinkled pea starch (WPS), and high amylose maize starch (HAMS) were supplemented in adults to evaluate their effects on fat oxidation by means of a ¹³CO₂-breath test. Sixteen subjects received a regular diet either without or with the supplementation of MIX and HAMS in randomised order. After administration of a [U-¹³C]algal lipid mixture, exhaled air was collected over 14?h in 0.5- and 1-h intervals. The ¹³C abundances were measured by nondispersive infrared spectroscopy. In comparison to the dry run (DR), supplementation with MIX and with HAMS increased the cumulative percentage dose recovery: (DR: 16.7?%, MIX: 16.9?%, HAMS: 18.0?%), but without statistical significance. The colonic degradation of MIX and HAMS to short-chain fatty acids tends to lower the formation of carbohydrate-derived acetyl-CoA and contributes to a postprandial lipid oxidation increase by using fat-derived acetyl-CoA as a compensatory fuel source.     

基于WLAN技术的楼宇内网络建设方案及其高频电磁辐射测试分析

基于WLAN技术设计了一种楼宇内网络建设方案，给出了该方案的详细设计步骤，包括频谱环境分析、规划设计、安装施工、测试和验收共5个阶段重点论述了设计阶段，对设计阶段的关键技术进行了深入的探讨，给出了合理的解决方案．对WLAN信号的高频电磁辐射进行了专门的实验测试，并将测试结果与国家标准进行了对比，证明其对人体健康没有影响．