古籍的地域收藏与传承——以辽宁省图书馆为例

阐述了辽宁省图书馆古籍收藏的特色,探讨了古籍收藏与传承中的地域性问题。     

实验室安全环保意识的调查与分析——以中山大学化学类专业学生为例

A survey about students' laboratory safety and environmental protection consciousness was performed in the freshmen majored in chemistry at Sun Yat-Sen University. Results showed that laboratory safety and environmental protection consciousness of most students' are weak. After analyzing the reasons, we put forward some suggestions. Cultivating students' laboratory safety and environmental protection consciousness should be carried out from several aspects such as emphasizing and regulating from school level, training in laboratory teaching, maintaining good cultural atmosphere of laboratory, as well as providing perfect laboratory safety and environmental protection facilities. We should guide students to actively learn knowledge and skills of laboratory safety and environmental protection in order to develop their good behavior and raise their consciousness.     

对古籍保护修复工作标准化建设的思考

阐述了古籍保护修复工作标准化建设的重要性,分析了古籍保护修复工作标准化建设的现状,指出古籍保护修复工作标准化建设存在的问题并提出了相应的解决办法。     

Deprotection‐free preparation of propargyl ether‐containing phosphinated benzoxazine and the structure–property relationship of the resulting thermosets

Generally, protection and deprotection procedures of amino groups are required in preparing propargyl ether‐containing benzoxazines. In this study, we report a facile, deprotection‐free preparation of a propargyl ether‐containing phosphinated benzoxazine (2) from the nucleophilic substitution of a phenolic OH‐containing phosphinated benzoxazine (1) and propargyl bromide in the catalysis of potassium carbonate. The structure of (2) was characterized and confirmed by a high‐resolution mass spectrum, ¹H, ¹³C, ¹H‐¹H, ¹H‐¹³C nuclear magnetic resonance (NMR) spectra, and X‐ray single crystal diffractogram. infrared (IR) and differential scanning calorimetry were used to monitor the ring‐opening of benzoxazine and crosslinking of propargyl ether. The microstructure and the structure–property relationship of the resulting homopolymers and copolymers are discussed. The T_g of homopolymer of (2) is 208 °C by dynamic mechanical analysis, the coefficient of thermal expansion is 43 ppm/°C, and T_d 5% (N₂) is 393 °C, respectively, which are higher than those of the homopolymer of (1) . Similar trends were observed in the copolymerization system. The results demonstrate the beneficial effect of crosslinking afforded by the propargyl ether group is higher than that by the phenolic OH group. © 2011 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem, 2012     

不同蓄水水位下大华斜坡体稳定性分析

结合坡体的地形地貌、水文地质条件、地层岩性特征,进行了不同水位情况下的斜坡稳定性计算.分析了不同蓄水水位对坡体稳定性的影响及其控制因素.     

Betaine and Carnitine Derivatives as Herbicidal Ionic Liquids

This study focused on the synthesis and subsequent characterization of herbicidal ionic liquids based on betaine and carnitine, two derivatives of amino acids, which were used as cations. Four commonly used herbicides (2,4‐D, MCPA, MCPP and Dicamba) were used as anions in simple (single anion) and oligomeric (two anions) salts. The obtained salts were subjected to analyzes regarding physicochemical properties (density, viscosity, refractive index, thermal decomposition profiles and solubility) as well as evaluation of their herbicidal activity under greenhouse and field conditions, toxicity towards rats and biodegradability. The obtained results suggest that the synthesized herbicidal ionic liquids displayed low toxicity (classified as category 4 compounds) and showed similar or improved efficacy against weed compared to reference herbicides. The highest increase was observed during field trials for salts containing 2,4‐D as the anion, which also exhibited the highest biodegradability (>75 %).     

铝合金表面ZSM-5型分子筛涂层耐蚀性研究

【目的】探究分子筛作为填料添加到水性涂料中对涂层防腐性能的影响。【方法】利用光学显微镜、XRD及SEM对涂层的中分子筛填料分散效果和涂层微观形貌进行表征,利用极化曲线分析分子筛水性涂层的电化学性能。【结果】分子筛粉末在水性漆中的最大添加比例为15%,超过此比例会出现大块团聚现象。其中10%的分子筛粉末对涂料耐蚀性提升最大。【结论】分子筛良好的高温水热稳定性有助于提高涂料的耐蚀性,但由于水性树脂不能够将分子筛颗粒紧密粘结,其添加量过大时会导致涂层耐蚀性能下降。     

考虑专利保护和渠道偏好的再制造双渠道闭环供应链决策与协调

本文在电子商务环境下考虑消费者对零售渠道和直销渠道具有不同的渠道偏好,研究了专利许可零售商实施再制造的双渠道闭环供应链定价决策和协调问题。运用博弈论方法求得了集中决策和分散决策情形下的最优定价策略,并分析了消费者渠道偏好系数对节点企业最优定价策略及利润的影响。针对分散决策存在效率损失的问题,以集中决策的最优解为基准,通过联合运用一个由批发价格、直销价格和专利许可费构成的定价机制和一个利润分享机制,实现了双渠道闭环供应链的完美协调。     

10 Jahre Ständige Kommission des RGW für die friedliche Anwendung der Atomenergie

0. Einleitwng

1. Reaktorwissenschaft und -technik und Kernenergetik

2. Kerntechnischer Gerätebau

3. Produktion von Isotopenerzeugnissen

4. Strahlenschulz und Schutztechnik

5. Isotopenanwendung

6. Strahlentechnik

7. Zur weiteren Tätigkeit der Ständigen Kommission Atomenergie des RGW