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31.
This paper presents a fringe pattern normalization and noise-reduction algorithm. Locally the background noise is suppressed, the modulation normalized and the noise smoothed. An expression to calculate the cosine-only term is formulated. It is related to the directional derivatives of the intensity fringes. Two-dimensional Fourier series are used to calculate the parameters needed for the algorithm. Experimental work is presented using diffraction and ESPI images. The programming is relatively simple and involves mainly local convolutions. The processing time using a 2 GHz computer to normalize an image of 256 × 256 pixels is approximately one second. 相似文献
32.
Poly(ortho‐phenylene ethynylene)s (PoPEs) have been synthesized via an in situ activation/coupling AB′ polycondensation protocol. The resulting polymers have been characterized by several analytical methods and are shown to have no structural defects. Although the Sonogashira–Hagihara polycondensation reaction is less efficient than for the preparation of the corresponding meta‐ and para‐linked polymers, presumably because of steric hindrance caused by the ortho substituents, the process can be accelerated by the use of microwave irradiation. Optical spectroscopy indicates solvent‐dependent conformational changes between extended transoid and helical cisoid conformations, providing the first experimental evidence for solvophobically driven folding of the PoPE backbone. © 2006 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 44: 1619–1627, 2006 相似文献
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甜菜皂素是一种天然的非离子型表面活性剂,用无机酸回流甜菜废丝,将所得的滤液蒸发浓缩至粘稠,再加入一定量的无水乙醇反复回流,脱色,纯化后得乳白色甜菜皂素片状晶体。 相似文献
36.
C. N. Carducci S. E. Lucangioli V. G. Rodríguez G. C. Fernndez Otero 《Journal of chromatography. A》1996,730(1-2):313-319
Sample preparation procedures using octadecyl (C18) extraction disks were developed to obtain accurate and reproducible results for determinations of clenbuterol (20 μg per dose) and levothyroxine (100 μg per dose) in dissolution media of solid oral dosage forms. Preconcentration of samples allowed final concentrations of 1.1 μg/ml of clenbuterol and 4.0 μg/ml of levothyroxine to be reached prior to CE analysis. The results obtained by CE were in good agreement with those of HPLC. The precision of the migration time, peak area, peak height and accuracy were determined in both intea-day (n = 6) and inter-day (n =18) assays. Linearity was demonstrated over the ranges 0.5–80.0 μg/ml of clenbuterol and 1.0–30.0 μg/ml of levothyroxine. The mean recoveries were higher than 94.0%, ranging from 50 to 125% levels with respect to dose potencies. The proposed methodology may be generally applied to determine drugs at ng/ml concentrations. 相似文献
37.
从芒果皮中提取果胶的工艺研究 总被引:5,自引:0,他引:5
果胶是一种大分子多糖类物质 ,具有良好的胶凝作用 ,用途广泛 ,在国内外市场上的销量很好。 1 990年世界上果胶总产量约 2 5 0 0 0吨 ,而我国 1 990年仅在食品工业上消耗的果胶就达 1 0 0 0吨 ,但国内市场上销售的果胶大部分为进口货[1] 。果胶在我国的生产仍处于开发阶段 ,所以发掘新的提取资源、提高果胶质量、降低果胶生产成本的意义十分重大。目前 ,已有以柑桔皮、向日葵盘、苹果皮、香蕉皮、马铃薯渣为原料提取果胶的研究报道 ,如何从芒果皮中提取果胶却未见报道。芒果在制造罐头和饮料中副产大量下脚料———芒果皮 ,未能得到充分利用… 相似文献
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Based on the investigation of a non-ionic surfactant-salt-H2O liquid-liquid extraction system, general rules concerning salt selection are concluded and the mechanism of phase separation is explained. The extraction behavior of chlorpromazine hydrochloride (CPZ) and procaine hydrochloride (PCN) in such a system is studied. Research shows that the extraction efficiency of CPZ can amount to 96% by twice extraction, which means that quantitative extraction is realized, while that of PCN is 77%. This system produces distribution coefficients (KD) of 12.3 and 2.6, respectively, for CPZ and PCN. Extraction mechanism is deduced according to ultraviolet absorbance; and molecular fluorescence spectra change of the drugs in the system studied. 相似文献
40.
Simultaneous isolation and determination of esculin and rutin in natural materials using SPE and HPLC 总被引:1,自引:0,他引:1
Summary Esculin (ESC) and rutin (RUT) have been simultaneously isolated from pharmaceutical natural materials by solid phase extraction (SPE). Determination of both substances was performed by reversed phase high performance liquid chromatography (RPHPLC) with UV detection. Optimization of the separation conditions showed that simultaneous isolation and determination of rutin and esculin from pharmaceutical material was possible. The recovery obtained was not lower than 95±2%. 相似文献