分光光度法测定脯氨酸的含量

文章用分光光度法研究了脯氨酸与四氯对苯醌的荷移反应 .实验指出 ,在硼砂缓冲溶液中 ,脯氨酸与四氯对苯醌于 30℃的水浴中恒温 1 2 0 min,可形成 1∶ 1的稳定络合物 ,其λmax=35 8nm,表观摩尔吸光系数 ε=1 .5 0× 1 0 5L·mol- 1 ·cm- 1 ,在 60 ng·m L- 1 ～ 40 0 ng·m L- 1 的范围内符合比耳定律 ,用本方法测定药物制剂的含量与文献方法一致 ,回收率在 99.65 %～ 1 0 0 .7%范围内 ,相对标准偏差在 1 .4%以内 .     

新型制冷机冷凝器壳侧的传热强化研究

针对现行制冷机冷凝器的不足 ,设计了适用于冷凝传热的新型折流杆冷凝器的壳程内部结构 ,并分析了其传热强化机理。在重力控制条件下 ,对不同内部支承结构与管束组合的冷凝器进行了传热实验研究 ,得到了水蒸汽在冷凝器壳侧的冷凝传热特性曲线。采用冷凝传热强化因子的概念 ,建立了预测该种折流杆冷凝器壳侧冷凝传热膜系数的计算公式 ,为折流杆冷疑器在制冷系统中的设计应用提供了理论依据。     

Nonlinear Energy Transfer over the Wave Spectrum in Water Covered by Solid Ice

On the basis of the hydrodynamic equations for nonlinear elastic-gravity waves beneath a solid ice cover and their Hamiltonian representation, a three-wave kinetic equation for the time evolution of the wave spectrum is formulated. The properties of the kernel of the kinetic integral describing the nonlinear interactions between wave triplets are investigated. An algorithm for numerically calculating the kinetic integral is developed. The rate of nonlinear energy transfer over the wave spectrum is estimated quantitatively and its most important characteristics are found.     

Fourier regularization for a backward heat equation

In this paper a simple and convenient new regularization method for solving backward heat equation—Fourier regularization method is given. Meanwhile, some quite sharp error estimates between the approximate solution and exact solution are provided. A numerical example also shows that the method works effectively.     

Chip-calorimeter for small samples

A method for measuring heat capacities of small samples using a chip-calorimeter and a heat pulse technique is described. The theoretical background to calculate the heat transport properties and the heat capacity of the sample from the pulse response function is given. Problems and potentials of the method are discussed. An example is given.     

Study of local lattice relaxation of substitutional impurities in silicon and germanium

Local lattice relaxation of substitutional donors in silicon investigated using self‐consistent multiple scattering Xα (MSXα) method within the framework of the standard muffin‐tin potential approximation is extended to substitutional donors in germanium and substitutional acceptors in both silicon and germanium. Incorporating the effect of lattice relaxation surrounding the impurity makes the model suitable for both shallow and deep levels. Chemical trends of some aspects of impurity states, such as local lattice relaxation and charge transfer, of the impurities both in silicon and germanium are inferred. © 2004 Wiley Periodicals, Inc. Int J Quantum Chem, 2004     

Specific heat and related thermophysical properties of liquid Fe-Cu-Mo alloy

The specific heat and related thermophysical properties of liquid Fe77.5Cu13Mo9.5 monotectic alloy were investigated by an electromagnetic levitation drop calorimeter over a wide temperature range from 1482 to 1818 K. A maximum undercooling of 221 K (0.13 Tm) was achieved and the specific heat was determined as 44.71 J·mol-1·K-1. The excess specific heat, enthalpy change, entropy change and Gibbs free energy difference of this alloy were calculated on the basis of experimental results. It was found that the calculated results by traditional estimating methods can only describe the solidification process under low undercooling conditions. Only the experimental results can reflect the reality under high undercooling conditions. Meanwhile, the thermal diffusivity, thermal conductivity, and sound speed were derived from the present experimental results. Furthermore, the solidified microstructural morphology was examined, which consists of (Fe) and (Cu) phases. The calculated interface energy was applied to exploring the correlation between competitive nucleation and solidification microstructure within monotectic alloy.     

关于半线性热方程整体解的注记

利用Besov空间的热核刻画及压缩映射原理,研究半线性热方程ut-△u＝u|u|a的初值问题,得到了当初值u0∈Lp0(Rn)且||u0||(B·)p-n (1/p0-1/p),∞(Rn)(p0＝na/2,p＞p0)充分小时,整体解的存在性及在一定条件下解的惟一性.     

供应链管理在中国企业中的应用实践

通过分析供应链管理演变及有关供应链管理的基础理论,为深圳华阳显像管股份有限公司的供应链管理的优化提供理论依据.论证了深圳华阳显像管股份有限公司实施供应链管理的可行性和效用度、优化供应链管理的具体策略及全面提高企业核心竞争力的保证措施.对中国企业入世后参与国际市场竞争,在供应链管理的优化方面是一次探索与实践.