水发食品中甲醛含量快速检测的实验研究

利用品红亚硫酸钠溶液与醛类物质反应后颜色深浅与浓度成正比的原理,使用5种标准浓度的甲醛溶液与希夫试剂反应显色后制作标准比色卡。用待测样品显色后的溶液与制作的标准比色卡进行比对,判断甲醛浓度范围。该方法具有现象明显、灵敏准确、药品易得的优点。因此,可用作中学生课外兴趣实验的实施项目,配制的希夫试剂和制作的标准比色卡也可用于家庭检测水发食品中甲醛含量。     

Requirements vs acceptability in proficiency testing schemes and other interlaboratory comparisons

Many laboratories take part in proficiency testing schemes, external quality assessment programmes and other interlaboratory comparisons. These have many similarities but also important differences in their modus operandi and evaluation of performance of participating laboratories. This paper attempts to highlight both the similarities and differences. It also puts particular emphasis on requirements called ”target values for uncertainty” and their meaning. Received: 24 January 2001 Accepted: 25 January 2001     

无穷维最优控制系统的N阶近似

讨论一类用无穷维系统方程描述的最优控制问题，把它看作为Ｈｉｌｂｅｒｔ空间上求算子方程的最小均方解的问题．在无穷维算子近似理论的基础上，用无穷矩阵奇异值分解方法得到无穷维最优控制问题解的形式，并研究这个解的有限维近似形式，建立一个有限的Ｎ阶最优控制系统，使得它的控制律与无穷维系统的控制之间误差最小     

Liposomal structure: A comparative study on light scattering and chromatography techniques

Liposomes play an important role in medical and pharmaceutical science as, nanoscale drug carriers. One of the most important features is their size and size distribution, influencing both their bio-distribution and their targeting efficiency to tumors and also therapeutic activity of liposomal antitumor drugs. In this study, the effect of preparation method and molecular interaction on size and shape of liposome was studied. The size and shape characterization of liposomes was performed by asymmetrical flow field-flow fractionation coupled online with multi-angle light scattering (AF4-MALS). The size distributions obtained by AF4-MALS were compared to mean particle sizes and size distribution measured with other standard method such as Photon Correlation Spectroscopy (PCS). Furthermore, the effect of molecular interaction (hydrophilic and hydrophobic model drugs) on liposomal structure was assessed.     

An improved method of characterizing fatty acids by equivalent chain length values

A method has been developed for calculating more accurate and reproducible equivalent chain length (ECL) values of 33 straight-chain fatty acids (FA), with various positions and numbers of cis double bonds, chromatographed on DB-Wax and DB-1 columns. The dependence of ECL values on the position and the number of double bonds is described, as is a method of utilizing these relationships for the characterization of FA by gas chromatography.     

Entire functions sharing one small function CM with their shifts and difference operators

In this article, we mainly devote to proving uniqueness results for entire functions sharing one small function CM with their shift and difference operator simultaneously. Let f(z) be a nonconstant entire function of finite order, c be a nonzero finite complex constant,and n be a positive integer. If f(z), f(z + c), and ?_c~n f(z) share 0 CM, then f(z + c) ≡ Af(z),where A(= 0) is a complex constant. Moreover, let a(z), b(z)( ≡ 0) ∈ S(f) be periodic entire functions with period c and if f(z)-a(z), f(z + c)-a(z), ?_c~n f(z)-b(z) share 0 CM, then f(z + c) ≡ f(z).     

Limit laws for upper and lower extremes from stationary mixing sequences

The aim of this paper is to examine the weak limiting behavior of upper and lower extremes from stationary sequences satisfying dependence conditions similar to D and D′ introduced by Leadbetter (Z. Wahrsch. Verw. Gebiete28 (1974), 289–303). By establishing the convergence in distribution of an associated sequence of point processes, the joint limiting distribution of any collection of upper and lower extremes can be determined. Sufficient and, in some cases, necessary conditions for the asymptotic independence of the upper and lower extremes are also given.     

A new framework for implicit restarting of the Krylov–Schur algorithm

This paper introduces a new framework for implicit restarting of the Krylov–Schur algorithm. It is shown that restarting with arbitrary polynomial filter is possible by reassigning some of the eigenvalues of the Rayleigh quotient through a rank‐one correction, implemented using only the elementary transformations (translation and similarity) of the Krylov decomposition. This framework includes the implicitly restarted Arnoldi (IRA) algorithm and the Krylov–Schur algorithm with implicit harmonic restart as special cases. Further, it reveals that the IRA algorithm can be turned into an eigenvalue assignment method. Copyright © 2014 John Wiley & Sons, Ltd.     

Schatten properties,nuclearity and minimality of phase shift invariant spaces

We extend Feichtinger's minimality property on the smallest non-trivial time-frequency shift invariant Banach space, to the quasi-Banach case. Analogous properties are deduced for certain matrix spaces.We use these results to prove that the pseudo-differential operator $\mathrm{Op}(a)$ is a Schatten-q operator from $M^{\infty }$ to $M^p$ and r-nuclear operator from $M^{\infty }$ to $M^r$ when $a\in M^r$ for suitable p, q and r in $(0,\infty ]$.