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71.
林劭彦 《厦门理工学院学报》2005,13(1):98-101
以 2004年台湾岛内由于选举而引发的大规模群众抗议活动为样本, 总结和分析泛蓝泛绿双方的主要攻防策略, 并在此基础上, 就运动的手段和策略等问题, 对群众运动的组织提出某些规范性意见。 相似文献
72.
The stability of Ochratoxin A during its extraction using different extraction techniques has been evaluated. Microwave-assisted extraction and pressurised liquid extraction, in addition to two other reference methods of extraction, i.e. ultrasound-assisted and magnetic stirring-assisted extraction, were evaluated. The effect of extraction temperature using the cited techniques was checked.The results show that Ochratoxin A can be extracted using microwave-assisted extraction at temperatures up to 150 °C without degradation. Pressurised liquid extraction can be used at temperatures up to 100 °C, for extraction times of less than 30 min. Further, both ultrasound-assisted extraction and magnetic stirring extraction can be applied at temperatures up to 65 °C.High-performance liquid chromatography combined with fluorescence detection using a Chromolith RP-18e column at a flow rate of 5 mL min−1 was used to quantify the Ochratoxin A. The retention time for the Ochratoxin A was 1.3 min. The limits of detection (LOD) and of quantification (LOQ) were 0.03 and 0.10 μg L−1, respectively. 相似文献
73.
On‐line coupling of LC and ICP‐MS has been used for fractionation and detection of species of Cu, Fe, I, Se and Zn in human serum. It has been shown that anion exchange chromatography provided better separation capability (both intra‐ and inter‐element) than size‐exclusion chromatography. The mobile phases for ion exchange chromatography consisted of Tris–HNO3 buffer and ammonium salt (nitrate, acetate or formate). Formate was found to be the best mobile phase counter ion, enabling good chromatographic separation, and is acceptable for mass spectrometry too. The quantitative evaluation of element concentrations adhering to individual fractions was performed by the peak area normalization method. The repeatability of results ranged from 3 to 15% (depending on the element concentration level) and represented the main part of the result uncertainty. The accuracy of Cu and Zn fraction determinations was confirmed by comparison with the isotope dilution technique. Copyright © 2006 John Wiley & Sons, Ltd. 相似文献
74.
E. V. Ermanyuk 《Experiments in fluids》2002,32(2):242-251
This paper presents a study on affine similitude for the force coefficients of an arbitrary body oscillating in a uniformly
stratified fluid. A simple formula is derived that gives a relation between the force coefficients for a body oscillating
in homogeneous and uniformly stratified ideal fluids. In particular, it implies the existence of a universal nondimensional
similitude criterion for a family of affinely similar bodies, namely, the bodies that can be transformed into each other by
vertical dilation of the initial coordinate system. Theoretical results are verified by experiments with a set of spheroids
having different length-to-diameter ratios. The experimental technique for evaluation of the frequency-dependent force coefficients
is based on Fourier analysis of the time-history of damped oscillation tests.
Received: 25 September 2000 / Accepted: 6 July 2001 Published online: 29 November 2001 相似文献
75.
Buffer gas beam coolers may become excellent beam preparation devices for high-resolution mass separation. The small beam
emittance provided makes efficient isobar resolution a realistic goal. In order to fulfill the needs of future facilities
providing high-intensity beams of rare isotopes, it is desirable to increase the beam intensity limit of such devices from
typically several tens of nanoamperes to microamperes. This requires the usage of high-voltage radiofrequencies in a low-pressure
gas environment. A buffer gas beam cooler, dedicated to this purpose, is under development at the NSCL. The study of voltage
breakdowns under such conditions and the design of an electrode system minimizing them is mandatory.
相似文献
76.
298K毛吸附溴化烷基三甲铵的性质及自由能 总被引:1,自引:0,他引:1
用液 /固吸附计量置换模型 ( SDM- A) ,研究了 2 98K羊毛纤维吸附溴化烷基三甲铵阳离子表面活性剂 CTAB和 DTAB的吸附等温线 ,结果表明它们均遵从 SDM- A的线性作图关系 .用 SDM-A的线性参数βα 和 q/z很好地描述了碳氢链长及加盐效应对于吸附性质的影响规律 ,特别是能定量地描述加盐效应对于吸附同时具有的促进和抵消两种相反作用的程度 ,并用 SDM- A的热力学 ,由线性参数计算得到了不同体系的吸附亲和能 ΔGA,解吸能 ΔGD 及总过程的自由能 ΔGP.一个吸附体系中 ,ΔGA 为常数且为较大的负值 ;ΔGD 为随溶液体相浓度 c增大而增大的正值 ;ΔGP为与 lgc呈线性关系的较小的负值 .计算所得结果能很好地解释实验事实 ,并可从更深层次上揭示吸附机理 . 相似文献
77.
78.
简析"静止液体内部压强公式验证"实验的设计策略 总被引:1,自引:1,他引:0
“静止液体内部压强公式验证”在现行教材中有两种实验方法。通过分析实验的设计策略,说明其作用、效果及操作上的困难,指出合理的与不合理诸因素,从而提出改进实验的方法,化难为易,提高实验教学效果。 相似文献
79.
P. Paasche T. Valenzuela D. Biswas C. Angelescu G. Werth 《The European Physical Journal D - Atomic, Molecular, Optical and Plasma Physics》2002,18(3):295-300
We have examined experimentally the motional spectrum of an electron cloud confined in a Penning trap. When the axial oscillation
is excited by a radio frequency field the resonance exhibits a double structure. Both components depend differently on the
number of trapped electrons and have different shape and width. We conclude that one of them corresponds to the excitation
of the individual electrons while the other is the center-of-mass mode of the cloud. The threshold behaviour of the center-of-mass
resonance suggests that it is a parametric instability of a Mathieu type equation of motion.
Received 11 July 2001 and Received in final form 12 November 2001 相似文献
80.