首页 | 本学科首页   官方微博 | 高级检索  
文章检索
  按 检索   检索词:      
出版年份:   被引次数:   他引次数: 提示:输入*表示无穷大
  收费全文   17627篇
  免费   1188篇
  国内免费   1054篇
化学   8824篇
晶体学   14篇
力学   279篇
综合类   145篇
数学   624篇
物理学   1569篇
综合类   8414篇
  2024年   41篇
  2023年   202篇
  2022年   495篇
  2021年   499篇
  2020年   424篇
  2019年   432篇
  2018年   417篇
  2017年   612篇
  2016年   670篇
  2015年   704篇
  2014年   879篇
  2013年   971篇
  2012年   1239篇
  2011年   1160篇
  2010年   907篇
  2009年   1072篇
  2008年   923篇
  2007年   1210篇
  2006年   1061篇
  2005年   937篇
  2004年   815篇
  2003年   627篇
  2002年   523篇
  2001年   426篇
  2000年   343篇
  1999年   328篇
  1998年   272篇
  1997年   249篇
  1996年   219篇
  1995年   190篇
  1994年   178篇
  1993年   156篇
  1992年   132篇
  1991年   135篇
  1990年   132篇
  1989年   92篇
  1988年   54篇
  1987年   62篇
  1986年   27篇
  1985年   10篇
  1984年   13篇
  1983年   5篇
  1982年   10篇
  1981年   2篇
  1980年   5篇
  1979年   4篇
  1976年   1篇
  1966年   1篇
  1959年   2篇
  1955年   1篇
排序方式: 共有10000条查询结果,搜索用时 15 毫秒
21.
We analyze the geometry of a rotating disk with a tangential acceleration in the framework of the theory of Special Relativity, using the kinematic linear differential system that verifies the relative position vector of time-like curves in a Fermi reference. A numerical integration of these equations for a generic initial value problem is made up and the results are compared with those obtained in other works.  相似文献   
22.
Syndiotactic polystyrene (sPS) has various crystalline forms such as α, β, γ, and δ forms, and a mesophase depending on the preparation method. In this study, we focused on the mesophase with the molecular cavity of sPS, which is obtained by step‐wise extraction of the guest molecules from the sPS δ form. To prepare the mesophase containing different shapes and sizes of the cavity, two kinds of the sPS δ form membrane cast from either toluene or chloroform solution were first prepared and then the guest molecules were removed by a step‐wise extraction method using acetone and methanol. We could succeed in the preparation of two kinds of mesophase with different shapes and sizes of the molecular cavity. Either toluene or chloroform vapor sorption to the sPS mesophase membranes was examined at 25 °C. Sorption analysis indicates that the mesophase with large molecular cavities can mainly sorb large molecules; on the other hand, the mesophase with small cavities can sorb only the small molecules, and is unable to sorb a large amount of large molecule because the cavity was too small to sorb the large molecules. Therefore, the sPS mesophase membrane has sorption selectivity based on the size of the molecular cavity. © 2003 Wiley Periodicals, Inc. J Polym Sci Part B: Polym Phys 42: 238–245, 2004  相似文献   
23.
工程施工中运输网络优化方案   总被引:5,自引:0,他引:5  
施工工地运输方案的优化设计可以归结为 :按施工期要求设计运输线路或验证已有线路通行能力 ,计算总线路中影响提高流量的关键路段 ,取得最小费用最大流 .本文运用图论理论这一数学工具把实际问题抽象为有向网络 ,进而建立数学模型 .此方法理论上严密 ,解题步聚直观清晰 ,对水利、公路、水路、铁路等其它运输系统有普遍意义 .  相似文献   
24.
含三正辛胺微胶囊对六价铬的富集   总被引:5,自引:0,他引:5  
本文将对六价铬有效的萃取剂TOA(三正辛胺)微胶囊化,制成填充柱型的酸性体系六价铬的富集分离装置。实验结果表明,微胶囊填充柱中每毫升TOA对六价铬的最大萃取容量为158.0g/mL,为纯TOA液相萃取的4.9倍。微胶囊经碱/水洗涤后,可再生使用。  相似文献   
25.
本文根据国家关键技术管理工作的特点,本着提高决策质量,满足用户要求的原则,分析和设计国家关键技术管理计算机系统,为高层次宏观决策提供丰富的信息支持。  相似文献   
26.
Summary A novel approach to solid phase extraction, based on the use of a highly selective molecularly imprinted polymer, is presented. The versatility of this type of sorbent for solid phase extraction was demonstrated in a model batch-wise pre-concentration of sameridine prior to gas chromatography. Problems associated with leakage of remaining imprint molecules during the desorption phase could be eliminated by the use of a close structural analogue of sameridine as the imprint species. It was found that a major benefit of the imprinted polymer was its specificity, which lead to distinctly cleaner chromatographic traces and ability to improve sensitivity by extracting sameridine from larger sample volumes.  相似文献   
27.
Banach空间上的框架与Riesz基   总被引:5,自引:0,他引:5  
朱玉灿 《应用数学》1998,11(4):24-30
本文讨论Banach空间上框架、无冗框架与Riesz基之间的关系及它们的稳定性.  相似文献   
28.
拟定了贫困地区经济发展中主导产业选择的五条原则,并提出了选择主导产业的一种方法,即先通过列表评分法求出各产业的优势度,再利用层次分析法确定各产业在合理发展工业中所占的相对地位,最后将两种结果相互参照确定主导产业部门。  相似文献   
29.
The technique of sirospun process is applied on a modified semi-worsted balloonless spinningframe to investigate the effect of spindle-speed,yarn-twist and strand-spacing on yarn properties.Yarn breaking strength,breaking extension,evenness and imperfection are examined on the basisof CCD experimental design.Yarn hairiness is particularly concerned,being found that all spinningparameters tested have significant effects on hairiness and that the minimum number of hairs oc-curs at the strand-spacing of 14.4 mm.Compared to conventional single spun yarn,experimentshave revealed the greatest advantage of using sirospun process is that all sirospun yarns have muchless hairiness.A new sirospun yarn fault,so called“loop”,has also been examined.The most likely cause forthis yarn fault is the strand-tension unbalance between the two strands when low tension spinningis applied.Further analysis and some initial tests have been carried out in the hope of overcomingthis loop fault which is an important obstacle to the application of balloonless spinning.  相似文献   
30.
Ali Liazid  Jamal Brigui 《Talanta》2007,71(2):976-980
The stability of Ochratoxin A during its extraction using different extraction techniques has been evaluated. Microwave-assisted extraction and pressurised liquid extraction, in addition to two other reference methods of extraction, i.e. ultrasound-assisted and magnetic stirring-assisted extraction, were evaluated. The effect of extraction temperature using the cited techniques was checked.The results show that Ochratoxin A can be extracted using microwave-assisted extraction at temperatures up to 150 °C without degradation. Pressurised liquid extraction can be used at temperatures up to 100 °C, for extraction times of less than 30 min. Further, both ultrasound-assisted extraction and magnetic stirring extraction can be applied at temperatures up to 65 °C.High-performance liquid chromatography combined with fluorescence detection using a Chromolith RP-18e column at a flow rate of 5 mL min−1 was used to quantify the Ochratoxin A. The retention time for the Ochratoxin A was 1.3 min. The limits of detection (LOD) and of quantification (LOQ) were 0.03 and 0.10 μg L−1, respectively.  相似文献   
设为首页 | 免责声明 | 关于勤云 | 加入收藏

Copyright©北京勤云科技发展有限公司  京ICP备09084417号