随焊氩气激冷控制铝/钢薄板焊接应力与变形数值模拟

采用有限元分析软件ANSYS,对不同焊接工艺条件下铝/钢异种金属薄板对接熔钎焊接过程进行数值模拟,建立了TIG电弧热源与氩气冷源模型,将常规焊接和随焊氩气激冷焊接的残余应力与变形进行对比分析,研究发现:随焊氩气激冷技术可使焊接纵向残余应力和变形分别降低32.8%和48.1%。为了验证数值模拟结果的准确性,进行了铝/钢异种金属薄板熔钎焊试验,将温度场与应力场的模拟值与试验值进行对比,结果显示两者吻合较好,表明随焊氩气激冷技术可有效控制铝/钢薄板焊接残余应力与变形。     

长治市高瓦斯矿井井下抽放煤层气综合利用对策和建议

针对煤矿瓦斯安全问题,就高瓦斯矿井瓦斯综合治理提出具体方案,介绍了瓦斯发电技术。     

金坛储气库岩盐蠕变特性及其实用本构研究

通过对金坛盐矿储气库岩盐大量的实验发现:在不同应力水平作用下,岩盐的瞬态蠕变变形介于0.1%到2%之间,一般高应力水平作用下的变形量较低应力水平作用下的变形大;试件的稳态蠕变率从0.0023%/h到0.15%/h变化不等,随应力水平的提高,岩盐蠕变率变化十分明显。表明:应力水平越高,瞬态蠕变变形和稳态蠕变率均越大;反之亦然。在分析应力水平与蠕变变形关系实验及理论分析的基础上,结合金坛储气库实际,建立了基于应力水平的岩盐瞬态及稳态蠕变综合本构方程。该本构方程理论计算与实验结果吻合较好,可为金坛储气库运营的稳定性分析提供一定的参考依据。     

往复式压缩机气体管道振动分析及消振方法

往复式压缩机气体管道振动是管道设计和机器运行中经常遇到的问题,往往影响到设备装置的正常运行。分析了通常引起往复式压缩机气体管道振动的原因及其消振方法。实例应用振动分析法采集数据。分析了振动原因,并提出了相应的消振措施。现场应用表明,效果较好。     

Found in the Folds: A Rediscovery of Ancient Egyptian Pleated Textiles and the Analysis of Carbohydrate Coatings

Charles T. Currelly, first director of the Royal Ontario Museum, participated in excavations of the tomb of King Nebhepetre, now known as Mentuhotep II, (Dynasty XI) in Deir el-Bahri, Egypt in 1906. He brought to Canada many objects from the excavations, and objects that he purchased while in Egypt; these formed the initial collection of the museum. Among the objects were seven fragments of fine linen cloth with intricate pleat patterns. Recently, the cloths became the subject of a study to learn how they had retained their pleats for 4000 years. Samples were examined and analysed using polarised light microscopy, scanning electron microscopy-electron dispersive X-ray spectrometry, gas chromatography-mass spectrometry, and pyrolysis-gas chromatography-mass spectrometry. Three of the cloths were likely fragments of clothing re-purposed as bandages and were found to be saturated in mummification balms composed of Pinaceae resin, Pistacia resin, and an essential oil characterised by a high abundance of cedrol, possibly originating from a juniper species. All seven of the cloths were found to have traces of polysaccharides from two probable sources: an arabinogalactan gum such as gum arabic or a fruit gum, and a polyglucoside, possibly starch.     

Chemometric Analysis of Urinary Volatile Organic Compounds to Monitor the Efficacy of Pitavastatin Treatments on Mammary Tumor Progression over Time

Volatile organic compounds (VOCs) in urine are potential biomarkers of breast cancer. Previously, our group has investigated breast cancer through analysis of VOCs in mouse urine and identified a panel of VOCs with the ability to monitor tumor progression. However, an unanswered question is whether VOCs can be exploited similarly to monitor the efficacy of antitumor treatments over time. Herein, subsets of tumor-bearing mice were treated with pitavastatin at high (8 mg/kg) and low (4 mg/kg) concentrations, and urine was analyzed through solid-phase microextraction (SPME) coupled with gas chromatography-mass spectrometry (GC-MS). Previous investigations using X-ray and micro-CT analysis indicated pitavastatin administered at 8 mg/kg had a protective effect against mammary tumors, whereas 4 mg/kg treatments did not inhibit tumor-induced damage. VOCs from mice treated with pitavastatin were compared to the previously analyzed healthy controls and tumor-bearing mice using chemometric analyses, which revealed that mice treated with pitavastatin at high concentrations were significantly different than tumor-bearing untreated mice in the direction of healthy controls. Mice treated with low concentrations demonstrated significant differences relative to healthy controls and were reflective of tumor-bearing untreated mice. These results show that urinary VOCs can accurately and noninvasively predict the efficacy of pitavastatin treatments over time.     

基于RBF网络的漏磁检测缺陷定量分析方法

为了正确评估油气管道的使用寿命和安全状况,需根据漏磁检测信号特征对缺陷进行准确的定量分析。提出一种基于径向基函数(RBF)神经网络、用于定量分析油气管道缺陷的迭代方法,给出了具体的算法步骤,并采用自适应学习机制来训练网络,既加快了该算法的收敛速度,又避免了陷入局部最小值问题。仿真结果表明:该方法不仅训练速度明显快于普通反向传播(BP)网络,而且最大量化误差仅为0.26%。该方法有助于提高漏磁检测的准确度,可为油气管道的安全评估提供可靠的依据。     

致密气藏多尺度支撑机理研究与应用

致密砂岩气作为重要的非常规天然气资源,需经过压裂改造才能实现有效开发。选取四川盆地致密砂岩露头岩芯,雕刻制作粗糙裂缝面岩板开展多尺度裂缝导流能力和支撑剂回流实验,分析导流能力及支撑剂回流的影响规律。研究表明,为了获得较高且稳定的导流能力,近井主裂缝需要有足够的支撑剂以提供更大的剩余缝宽,远井剪切裂缝只加入少量小粒径支撑剂也能有效改善高闭合应力条件下的导流能力;对于支撑剂充填的主裂缝,裂缝导流能力随着闭合应力和支撑剂浓度的变化存在临界闭合应力及临界支撑剂浓度。在支撑剂充填层中加入纤维,临界出砂流速呈数量级增长,可以有效预防压后裂缝的支撑剂回流。致密气藏多尺度支撑理念在四川盆地川西拗陷致密气储层开展的压裂工程实践取得了显著的增产效果,为中国致密气藏经济高效开发提供了有效支撑和借鉴。     

USAEME-GC/MS Method for Easy and Sensitive Determination of Nine Bisphenol Analogues in Water and Wastewater

A new, simple and sensitive method for isolating nine compounds from the bisphenol group (analogues: A, B, C, E, F, G, Cl₂, Z, AP) based on one-step liquid–liquid microextraction with in situ acylation followed by gas chromatography-mass spectrometry was developed and validated using influent and effluent wastewaters. The chemometric approach based on the Taguchi method was used to optimize the main conditions of simultaneous extraction and derivatization. The recoveries of the proposed procedure ranged from 85 to 122%, and the repeatability expressed by the coefficient of variation did not exceed 8%. The method’s limits of detection were in the range of 0.4–64 ng/L, and the method’s limits of quantification ranged from 1.3 to 194 ng/L. The developed method was used to determine the presence of the tested compounds in wastewater from a municipal wastewater treatment plant located in northeastern Poland. From this sample, eight analytes were detected. Concentrations of bisphenol A of 400 ng/L in influent and 100 ng/L in effluent were recorded, whereas other bisphenols reached 67 and 50 ng/L for influent and effluent, respectively. The removal efficiency of bisphenol analogues in the tested wastewater treatment plant ranged from 7 to approximately 88%.     

段塞流诱导柔性立管振动响应实验分析

在气液两相循环实验系统中开展了水动力段塞流诱导的悬链线型柔性立管振动响应测试,利用高速摄像非介入测试方法同步捕捉了柔性立管的振动位移与管内的段塞流动细节,预测了气体表观流速对水动力段塞流诱导柔性立管振动响应的影响规律,分析了振幅响应、模态权重、频谱变化以及管内流动特性.结果 表明,随着气体表观流速的增大,振动幅度逐渐增...