The drawing behavior of Y-Ba-Cu-O sol from non-aqueous solution by a complexing process

A complexing process is developed to prepare Y-Ba-Cu-O superconducting fibers. The process is not identical to typical sol-gel processes; here the resulting gel network is built up by hydrogen bonding linkage among complexing species in non-aqueous solution. Cu acetate, [Cu(OAC)₂], Ba methoxyethoxide [Ba(ORE)₂] and Y acetate [Y(OAC)₃] are used as precursors for preparing homogeneous gels while -methacrylic acid (HOAA) and diethylenetriamine (DETA) as complexing agents, and methoxyethanol (REOH) as solvent. Fibers drawn from a sol obtained through reduced pressure present no or little deformation at 80°MoC via adjusting the amount of DETA and HOAA. Cu(OAC)₂, Ba(ORE)₂ and Y(OAC)₃ in the complexing process have been demonstrated to form gels without hydrolysis and condensation at ambient atmosphere. The relationships between the drawing behavior of sols and gel structure with different amounts of DETA and HOAA are suggested. The concentration region of drawing the gel fibers with no or little deformation heated at 80°MoC is also found.     

VISCOELASTIC BEHAVIOR OF THE NON-HOOKE DEFORMATION BEFORE YIELDING IN UNIAXIAL DRAWING OF AMORPHOUS POLY(ETHYLENE TEREPHTHALATE)*

Viscoelastic behavior of the non-Hooke deformation of amorphous PET film before yield was investigated in thetemperature region 74--80.5℃ around the glass transition temperature. The film specimen was drawn to yield point followedby unloading to zero stress, then the residual deformation was held constant, while the subsequent evolution of the stress wasrecorded. An induction period was found in the course of stress evolution fol1owed by a stress step-increase. The inductionperiod decreases with increasing drawing temperature with an activation energy of 1.10 MJ/mol·K, which is attributed tothe time needed for the relaxation of rubbery deformation through cooperative internal rotations. At temperatures lower than74℃, there is no stress increase or the induction period becomes too long to be observed. Thus the nature of anelasticity inthe non-Hooke region before yielding is attributed to stress induced rubbery deformation. The experimental results areinterpreted in terms of Perez' rheological model of a series connected Hooke spring and a Voigt element consisting of aparallel connected elastic spring and a dashpot.     

Two-beam interference detection of the changes in fibre structural parameters during low drawing process

A Pluta polarizing interference microscope with a fibre stretching device attached was used to detect the changes in molecular structure that occur during the fibre cold drawing process. Fibres drawn with low draw ratios show different types of deformation mechanisms. The interference patterns recorded at different draw ratios are used to relate the deformation mechanisms with the measured structural parameters. Some optical parameters are measured such as; refractive indices nand n birefringence n, the polarizability per unit volume , the orientation distribution function f(θ), the angle θ between the stretching direction and the chain axis, and the angle θ_m which the transition dipole moment of the molecular species makes with the molecular axis (chain axis). Three polymeric fibres (Polyethylene terephthalate PET, Polypropylene PP and Polyamide PA) were used in this study and their interferograms are illustrated.     

中国境内IGS站数据处理及地壳运动研究

利用中国境内国际GPS大地测量和地球动力学服务(IGS)站的GPS单天数据,使用GAMIT软件对其进行基线解算.以单天解的基线结果作为输入量,利用所介绍的台站漂移数学模型,求解台站漂移速度,得到地壳运动信息;再根据板块运动欧拉定理,求解中国大陆整体的欧拉矢量.结果表明,在ITRF2000框架下,求解的台站漂移速度与IGS公布的结果相近,由此求解的中国大陆整体的欧拉矢量与采用IGS公布数据计算的结果相近.     

二元函数图形绘制及特征分析实验设计

介绍了二元函数及图形的相关数学知识和mathematica软件平台的相关知识，给出了二元函数及图形特征研究的内容与要求，完成了空间图形及交线、截面、相交面的图形的绘制及相关特征分析的实验设计。     

矢量数据与位映象数据之间的转换技术研究

以内存缓冲区为虚拟设备,提供了一种与设备无关的矢量数据与位映像数据之间的转换方法.该方法特别适合于嵌入式系统汉字点阵及图形点阵显示以及非标准打印设备的输出等方面的应用.     

系泊浮桥运动的非线性动力特性

研究系泊分段线性恢复刚度对浮桥运动的影响，根据系泊浮桥的分段线性刚度，提出了浮桥动力响应的非线性分析模型．考虑浮桥的横荡运动，计算上下游锚链的系泊力及确定分段线性刚度，建立了浮桥横荡运动方程．以长1000m的浮桥为例，得到了浮桥横荡周期为4．33s，及不同波浪作用下浮桥横荡运动响应的幅频特性．计算表明，由于系泊刚度的分段线性，浮桥运动出现幅值跳跃，并且刚度比越大，幅值跳跃越大．     

任意空间预应力束引伸量实用CAD电算求解法

空间顸应力束引伸量的求解是桥梁施工控制中的重要环节，介绍了在CAD图形软件下，空间预应力束引伸量的求解过程，对单端张拉、双端对称张拉、双端不对称张拉以及斜腹板中预应力束引伸量的求解方法作了详细阐述。     

用AUTHORWARE开发多媒体教学软件

以一类常见的函数图像为例，用AUTHORWARE实现编程，使用设计窗口中的框架、交互、导航连接等图标以及超文本应用的来完成这类曲线的绘制及相关的课件(CAI)制作过程，同时使用自定义函数和引入外部函数来完善Authorware的图形类函数。