Determination of Easy Axis in a Chemical Ferromagnet, 4-(p-Chlorobenzylideneamino)–TEMPO (TEMPO=2,2,6,6-Tetramethylpiperidin-1-Oxyl)

The trapping sites for muon and muonium in ferromagnetic p-Cl–Ph–CH=N–TEMPO [(4-(p-chlorobenzylideneamino)–TEMPO (TEMPO = 2,6,6-tetramethyl-piperidin-1-yloxyl)] and the hyperfine interaction tensors for these sites are obtained using first-principles Unrestricted Hartree–Fock theory. The calculated hyperfine interactions are used to compare the calculated zero field muon spin rotation (μSR) frequencies for different choices for the easy axis and the observed frequency. It has been concluded that the two trapping centers that can best explain the observed μSR frequency are a trapped singlet muonium near the radical oxygen and a trapped muon site near the chlorine. The direction of the easy axis also is determined to be the b-axis of the monoclinic lattice. This direction for the easy axis is confirmed by determining the direction of the distributed magnetization in the molecular solid which leads to a minimum dipole–dipole interaction energy. The consequences of this agreement for the easy axis direction by two independent procedures are discussed. This revised version was published online in September 2006 with corrections to the Cover Date.     

Ultrasound‐assisted matrix solid phase dispersive extraction for the simultaneous analysis of β‐lactams (four penicillins and eight cephalosporins) in milk by high performance liquid chromatography with photodiode array detection

The application of ultrasound‐assisted matrix solid phase dispersive extraction for the confirmatory analysis of 12 β‐lactam antibiotics in milk by high performance liquid chromatography with photodiode array detection has been proposed herein. Four penicillins (cloxacillin, dicloxacillin, oxacillin, and amoxicillin) and eight cephalosporins (cefaclor, cefadroxil, ceftiofur, cefuroxime, cefoperazone, cefazolin, cephalexin, and cefotaxime) are effectively extracted using a mixed sorbent of Quick Easy Cheap Effective Rugged Safe technique and OASIS HLB providing a matrix free from any endogenous interference. Examined analytes were well resolved on an Inertsil ODS‐3 analytical column with a mobile phase of CH₃COONH₄ (0.05 M) and acetonitrile delivered under a gradient program. 1,7‐Dimethyl‐xanthine was used as internal standard. The method was validated meeting the European Legislation determining linearity, selectivity, stability, decision limit, detection capability, accuracy, precision, and ruggedness according to the Youden approach. Recoveries of all antibiotics rated from 85.0 to 115.7%, while RSD values were <12.7%. Finally, the method was successfully applied to milk samples purchased from local market.     

Analysis of questioned documents: A review

During the last years (2000–2014), many publications concerning the forensic analysis of questioned documents have been published, and new techniques and methodologies are nowadays employed to overcome forensic caseworks. This article reviews a comprehensive collection of the works focused on this issue, including dating studies, the analysis of inks from pens and printers, the analysis of paper, the analysis of other samples related to questioned documents and studies on intersecting lines. These sections highlight the most relevant analytical studies by a wide range of analytical techniques. Separation and spectrometric techniques are critically discussed and compared, emphasizing the advantages and disadvantages of each one. Finally, concluding remarks on the research published are included.     

致密围岩煤与瓦斯突出单一煤层瓦斯防治技术应用

针对主采煤层单一、围岩硬度密度大、顶底板不易跨落、瓦斯赋存不易向外泄、不利采掘的煤与瓦斯突出性矿井,充分发挥技术导向作用,从实际应用、安全、经济等综合方面优选瓦斯治理措施,逐步取得并形成适宜矿井特点的瓦斯治理模式,较好地促进矿井安全高效生产。     

高校图书馆计算机丢失数据恢复工作探讨

阐述了高校图书馆开展数据恢复工作的必要性,详细介绍了易我数据恢复向导恢复数据的优势与使用方法,强调了使用易我数据恢复向导需要注意的一些问题。     

"求真"与"喻俗"新探

从辩证唯物主义两点论出发，以现代视角对一千多年前翻译家玄奘提出的“既须求真，又须喻俗”的标准进行了探讨，进而指出，在翻译流派如林。理论丛生的今天，“求真”与“喻俗”可成为超越时代局限的翻译标准。     

简易自动喷水灭火系统的设计应用

为了充分了解小型建筑物新(改扩)建消防设施设置的实用性和经济性,以简易自动喷水灭火系统的设计和应用为研究对象。结果表明:在做好充分的设计参数调研后,如何根据建筑物的外在特点及使用性质使用简易自动喷水灭火系统进行合理的设计,使之既满足了消防安全要求,又实现了建筑物的功能要求,达到减少火灾危险,节省消防投资资金的作用,更重要的是有效的预防群死群伤事故的发生,保护人民生命财产安全。该成果对简易自动喷水灭火系统的设计应用具有一定的参考价值和指导意义。     

磁各向异性测量实验装置

介绍一种自制的磁各向异性测量装置，该装置结构简单，造价低廉，在测量过程中显示工作原理清楚直观，使用磁性薄膜中小颗粒作为样品，测量结果稳定可靠，适合学生实验使用。     

磁场中凝固的DyFe1.9合金的〈100〉织构

研究了巨磁致伸缩材料TbFe1.9、DyFe1.9等合金在磁场中凝固的织构取向.由于DyFe1.9对X-射线的消光效应,在X-射线衍射图上观察不到(100)的衍射峰.但是通过对{222}和{220}极图的分析,可以确认当冷却速率为0.7℃/min,磁场强度为140 mT时,平行于磁场方向的〈100〉取向是样品中的主要织构.在接近的凝固条件下,TbFe1.9合金的〈111〉取向可以获得,并直接在X-射线衍射图上观察到.实验意味着在磁场中凝固的技术是制备沿易轴取向的磁性材料的可靠方法.     

任意四面体绕质心轴的转动惯量

转动惯量是力学中一个重要的物理量,对有对称性的匀质物体较容易给出转动惯量的解析式,而对缺少对称性的一般四面体给出转动惯量的解析式却不容易,本文给出了求取四面体绕质心轴转动惯量的一种方法.