Tribological Behavior of Multiply-Alkylated Cyclopentanes (MACs)-Cu Nanoparticles Composite Thin Film

Multiply-alkylated cyclopentanes (MACs) composite thin films containing Cu nanoparticles are fabricated on the octadecyltrichlorosilane (OTS)-modified substrate by a spin-coating technique. The thickness, wetting behavior, and nanoscale morphologies of the films are characterized by means of ellipsometry, contact angle measurement, and atomic force microscope (AFM). The friction and wear behaviors of the thin films sliding against Si₃N₄ ball are examined on a UMT-2MT tribometer in a ball-on-disk contact mode. The worn surfaces of the OTS-MAC-Cu composite film and the counterpart Si₃N₄ balls are investigated with a scanning electron microscope. Water contact angle on OTS-MAC-Cu composite film is higher than that of OTS-MAC film. OTS-MAC-Cu composite film exhibits higher load-carrying capacity and better friction reduction and antiwear behavior as compared with OTS-MAC film. This may be attributed to the load-carrying and self-repairing property of the Cu nanoparticles in the composite film and the formation of a transfer layer composed of OTS, MAC, and Cu on the rubbing surface of the counterpart ball.     

Infrared absorption spectra and structure of TiO2-SiO2 composites

The composites xTiO₂-(1−x)SiO₂ (x = 0.1, 0.5, 0.9) were obtained by coprecipitation from solutions of alkoxides: tetraethoxysilane (TEOS) and titanium tetraisopropoxide (TIPT). Intermolecular interaction of the components of the composite is apparent in the IR absorption spectra in the 928–952 cm⁻¹ region, and is connected with bending vibrations of the Si-O-Ti bond. Translated from Zhurnal Prikladnoi Spektroskopii, Vol. 75, No. 5, pp. 724–728, September–October, 2008.     

Preparation of nano-hydroxyapatite/poly(<Emphasis Type="SmallCaps">l</Emphasis>-lactide) biocomposite microspheres

Nano-hydroxyapatite (HA)/poly(l-lactide) (PLLA) composite microspheres with relatively uniform size distribution were prepared by a solid-in-oil-in-water (s/o/w) emusion solvent evaporation method. The encapsulation of the HA nanopaticles in microshperes was significantly improved by grafting PLLA on the surface of the HA nanoparticles (p-HA) during emulsion process. This procedure gave a possibility to obtain p-HA/PLLA composite microspheres with uniform morphology and the encapsulated p-HA nanoparticle loading reached up to 40 wt% (33 wt% of pure HA) in the p-HA/PLLA composite microspheres. The microstructure of composite microspheres from core-shell to single phase changed with the variation of p-HA to PLLA ratios. p-HA/PLLA composite microspheres with the diameter range of 2–3 μm were obtained. The entrapment efficiency of p-HA in microspheres could high up to 90 wt% and that of HA was only 13 wt%. Surface and bulk characterizations of the composite microspheres were performed by measurements such as wide angle X-ray diffraction (WAXD), thermal gravimetric analysis (TGA), environmental scanning electron microscope (ESEM) and transmission electron microscopy (TEM).     

铁电薄膜在红外辐射作用下的动力响应

本文研究了红外探测器中红外焦平面列阵的象元———铁电薄膜微桥在红外辐射作用下的输出信号。用层合板壳作为微桥结构的力学模型,中间一层为压电材料,上下两层为金属材料电极。采用了力-电-热耦合的控制方程和变分原理,考虑了铁电薄膜的惯性力,推导出了基于Mindlin假设的压电材料层合板有限元公式。以红外探测器在夜间从飞机上探测地面的坦克为例,用有限单元法模拟了铁电薄膜微桥在红外辐射作用下的力、热、电输出信号,并对结果作了分析比较。     

大空间三向组合平板网架研究

利用中心节点、交叉梁、三角形拉杆和空心板所构成承力单元的组合以及内部支承柱的自由布置,本文提出了一种新型大空间三向组合平板网架结构。相关的TDGS分析系统针对原型试验取得了较好的模拟效果。通过引入柱的局部影响区域这一全新概念,系统总结了加入内部支承柱前后网架结构的内力和变形规律,进而为进一步的工程应用提供了可行性建议。     

三氧化二铝-聚苯乙烯复合微球的制备

以Al2O3-PS复合材料为原料,采用乳液微封装法制备出掺杂Al2O3的PS空心微球。三相溶液分别是两个水相：蒸馏水（W1相）、5wt%PVA水溶液（W2相）和3wt%Al2O3-PS溶液（O相,苯和三氯甲烷混合物作溶剂）。所得微球表面粗糙度低于50nm。     

复合载体预制桩的分析与应用

由于滨州市许多地区原为池塘,后用建筑垃圾杂填土填平场地,不能直接作为地基持力层应用。通过实例,对浅部存在较好桩基持力层的建筑垃圾场地采用复合载体预制桩进行探讨分析。     

复合材料构件数字化精确成形技术与装备

在分析国内外复合材料预制体成形技术与装备研究现状基础上,分析了复合材料构件的成形制造目前存在用工密集制造效率低、形性精确成形调控难、成形过程自动化程度低等问题,介绍了数字化柔性导向三维织造成形方法和变曲率预制体铺放-缠绕-针刺一体化成形方法,提出了复合材料构件成形技术与装备的未来发展建议,以推动复合材料构件高效率、高性能、高质量的自动化数字化成形制造技术发展,更好地提升基于纤维预制体复合材料构件制造水平。     

海上合成编队指挥信息体系特征行为分析

探讨了海上合成编队指挥信息体系5个方面的特征行为,包括组成单元的"独立性"、组成结构模式演化的"不确定性"、指挥与信息流程的可变性、组成部分与整体间的"涌现性"以及部署区域上的分布性。海上合成编队指挥信息体系是典型的体系范例,在其设计、部署、运行与管理上,都需要从"系统观"转向"体系观"。     

卫星结构技术发展对新型复合材料的需求分析

 新材料、新工艺的不断进步和变革是卫星结构技术发展的基础和保障,结构技术的发展方向与需求又是新材料、新工艺发展的源动力。本文从设计角度出发,根据后续卫星型号发展趋势,梳理了结构专业技术的重点发展方向,提出了后续新型复合材料的应用需求。