Influence of oxidation time on semiconductive behaviour of thermally grown oxide films on AISI 304L

The oxide films formed on AISI 304L stainless steel at 300 °C in the oxidation time range between 2 and 4 h have been studied by photoelectrochemistry. Photocurrents were investigated as a function of the wavelength of the incident light and the electrode potential. The investigation allowed the determination of the semiconductive properties of the oxides. The oxide films showed n-type behaviour. A duplex structure of the oxide films has been suggested on the basis of the photocurrent spectra, with an internal oxide layer having an optical gap (E_g2 = 2.16-2.3 eV) depending on the applied potential and oxidation time, higher to that of the external oxide layer (E_g1 ≈ 1.9 eV). Significant variations in the amplitude of the photocurrent were detected as a function of the applied potential and the oxidation time.     

轻型汽车后桥半轴断裂件的组织及断口特征

采用光学显微镜和扫描电子显微镜等手段，对某轻型汽车40Cr后桥半轴断裂件的组织及断口特征进行了分析结果表明：半轴在调质处理时的淬火温度不够高，使其表层和心部组织中存在较多的铁素体相，造成了工件最终的硬度和疲劳强度不足，导致半轴在使用中发生扭转疲劳断裂．     

Determination of ultra-trace gold in natural water by graphite furnace atomic absorption spectrophotometry after in situ enrichment with thiol cotton fiber

A simple method of determining ultra-trace Au in natural water was presented by using graphite furnace atomic absorption spectrophotometry (GFAAS) after in situ enrichment with thiol cotton fiber (TCF). The sample solution was adjusted to pH 1.5-2.0 with HCl, then the water sample was passed through a column packed with 0.10-0.20 g TCF and the flow rate was controlled at 20-40 ml min⁻¹. The effects of interferences, such as complexing and oxidizing agents and other elements adsorbed on TCF were overcome by chemical treatments prior to the desorption of Au. The adsorbed Au was adsorbed with 2.0 ml hot acid, then it was extracted with 1.00 ml methyl isobutylketone (MIBK). For a 5 l water sample, the detection limit of Au is 0.02 ng l⁻¹. The relative standard deviation (R.S.D.) for the determination of 1.44 ng l⁻¹ Au was 9.4%.The method was applied to determine ultra-trace Au both in suspended phase and soluble phase in natural water, the concentrations of total Au in natural water samples range from 0.51 to 67.82 ng l⁻¹. The recovery of added 0.50-6.00 ng l⁻¹ Au was 80-95%. The method is useful in prospecting for Au deposits by means of hydrogeochemical methods. The enrichment is carried out in the field, and then the determination of Au is completed later in the laboratory.     

Influence of the Interaction between Two Neighboring Periodically Curved Fibers on the Stress Distribution in a Composite Material

A method is developed for a stress analysis in an infinite elastic body containing two neighboring periodically cophasaly curved fibers located along two parallel lines. The stress distribution is studied when the body is loaded at infinity by uniformly distributed normal forces in the fiber direction. The investigation is carried out within the framework of a piecewise homogeneous body model with the use of exact three-dimensional equations of elasticity theory. Numerical results related to the stress distribution considered and the influence of interaction between the fibers on this distribution are given.     

Numerical Modeling of Solitons in a Low Birefringent Optical Fiber

A numerical investigation, based on the split-step Fourier transform algorithm of all optical switching of solitons in a low birefringent optical fiber is presented. The numerical algorithm is described in detail. This revised version was published online in August 2006 with corrections to the Cover Date.     

利用模式的对称性研究光子晶体光纤的色散

由光子晶体光纤的对称性可以得到模式分布的对称性，根据模式的对称性选择适当的展开函数，可以使计算量大大减少。计算了六角结构光子晶体光纤的色散特性，得到了波长在1．55pm处色散为零时，光子晶体光纤的结构参量所满足的方程。     

斐索梯度折射率光纤透镜传感实验

采用LD泵浦的单纵模Nd：YVO4倍频激光器、梯度折射率光纤透镜等器件构成斐索梯度折射率光纤透镜传感实验仪．本文介绍了实验装置和实验原理，并给出了实验结果。     

一种控制掺铒光纤激光器超混沌的方法——非线性延时反馈参数调制法

提出一种非线性延时反馈参数调制法来控制混沌/超混沌，给出了利用这种方法控制处于超混沌状态的双环掺铒光纤激光器的方案.数值模拟表明，只要延时时间和反馈强度合适就可以把双环掺铒光纤激光器从超混沌状态成功地控制到不同的周期状态. 关键词： 掺铒光纤激光器 超混沌 非线性延时反馈参数调制 混沌控制     

表面纤维直径与羊毛机织精纺面料的刺痒感

通过前臂试验对26种轻薄型羊毛机织精纺面料和7种其他纤维的轻薄型机织面料的刺痒感进行了比较研究,并用显微镜对部分轻薄型羊毛机织面料的表面纤维分布进行了研究。结果表明多数毛织物在温度为(24±1)℃、相对湿度为(65±5)％的条件下存在刺痒感,并且毛织物的刺痒感与其表面纤维的平面直径及直径大于26μm的表面纤维根数密切相关。