粤西士人的诗学精神——“粤西士人研究”之四

粤西士人的文学结社体现出其身份自觉,对文学创作活动有很大的促进,粤西女诗人在家族文学集体中的文学创作也有很大的提高,有很多优秀作品。粤西士人的诗、画结合体现出新的艺术趣味,从题画诗可见一斑。有了身份自觉,粤西士人辑集本土人士的文学作品,弘扬粤西文化。粤西士人的文学结社使其在历史的某一阶段引领全国文学的发展。     

电路分析课程的教学探索

电路分析是电类专业必修的一门专业基础课,其教学质量及效果对后继课程的学习有着重要的影响.结合教学实践,探索出一种类比教学法,取得了较好的教学效果.     

基于关联规则和语义规则的本体概念提取研究

为解决基于非结构化文本的中文领域本体概念提取效率和准确率不理想的问题, 提出了一种基于关联规则和语义规则的领域本体概念提取方法。利用领域一致性和相关性检查以及关联规则分别获取候选概念和关系集合, 计算候选概念在领域术语关系中的深度和广度, 利用深度和广度信息反馈概念隶属度的思想, 定量分析术语与领域的隶属程度, 进行本体概念的领域隶属度检查, 完成领域本体概念的提取。实验结果表明, 该方法提高了领域本体概念的提取效率和准确率, 具有可行性和合理性, 领域本体概念的提取准确率提高了12%左右。     

Studies on the Photochemical Oxidation of 1,3-Diphenylisobenzofuran and Cis-Cyclooctene in N,N-Dimethylformamide–Propanol Binary Mixture

Kinetic studies on the photochemical oxidation of 1,3-diphenylisobenzofuran have been carried out in binary liquid mixtures of N,N-dimethylformamide (DMF) with 1-propanol (PrOH). The strongest influence of solvating effects upon the course of this reaction was observed for compositions of the studied mixture corresponding respectively to ca. 50?mol% of PrOH. Additionally, we have carried out analogous studies of photooxidation of cis-cyclooctene. Similarly as previously, the noticeable influence of solvating effects upon the course of this reaction corresponded to ca. 50?mol% of DMF. We suspect that the mechanism of this effect is associated with the formation of the polar intermediate during the ene reaction being easier.     

An Experimental Study of a Flux Modulated Solid State Metathesis Reaction

A solid state metathesis (SSM) reaction was investigated with respect to the formation of rare‐earth carbodiimides, the role of the co‐produced salt (LiCl), and the eutectic flux medium (LiCl/KCl). A SSM reaction is characterized by an exothermic reaction in which a salt (often LiCl) is coproduced. When the salt melts, it can serve as a useful medium for the crystallization of a desired product. An improved crystal growth can be observed by using an eutectic flux. However, the composition of an eutectic LiCl/KCl flux is altered when LiCl is produced during the reaction. The thermal effects concerning the endothermic melting of the flux and the exothermic ingnition of the SSM reaction may compensate each other, which is not necessarily a drawback for the reaction to proceed.     

Metal-containing polyurethanes from tetradentate Schiff bases: synthesis,characterization, and biocidal activities

N,N′-bis(salicylidene)thiosemicarbazide Schiff base has been synthesized by the reaction of thiosemicarbazide with salicylaldehyde and then reacted with formaldehyde to generate phenolic groups, resulting in the formation of Schiff-base monomeric ligand. It was further incorporated with transition metals, Mn⁺², Co⁺², Ni⁺², Cu⁺², and Zn⁺², to form Schiff-base metal complex, which was then polymerized with toluene 2,4-diisocyanate to form metal-chelated polyurethanes. Monomeric ligand, its metal complexes, and its metal polychelates were characterized and compared by elemental analysis, FT-IR, ¹H NMR, thermal, and biocidal activities to evaluate the enhancement in physical and chemical properties on coordination with metal and on polymerization. SEM images of ligand and polymer metal complexes showed changes in surface morphology, while electronic spectra of polymer metal complexes were used to predict the geometry. Antimicrobial activities were determined by using agar-diffusion method with Staphylococcus aureus, Escherichia coli, Bacillus subtilis (bacteria), Aspergillus niger, Candida albicans, and Aspergillus flavus (yeast). The polymeric ligand had varied antibacterial and antifungal activities, enhanced after chelation and polymerization. Comparative results show that coordination of metal to the ligand enhances its physical and chemical properties which were meliorated on polymerization.     

基于刻辞网络关联度的甲骨字考释难度量化方法

为了提高未解读甲骨字考释研究的效率,提出了一种未解读甲骨字考释难度量化方法,可帮助研究者优先选择出难度较低的甲骨字进行针对性研究,避免在考释难度极大的甲骨字上做大量无用功。先把所有甲骨刻辞构建为一个庞大的甲骨刻辞网络;再通过网络节点间的关联关系,计算出未解读甲骨字和已解读甲骨字之间关联关系;计算结果可以作为未解读甲骨字考释难度的量化数据;并通过实验验证了方法的有效性。     

浅析Blum-Kulka翻译中衔接与连贯的转换

以色列学者Shoshana Blum-Kulka在1986年写了一篇关于翻译中衔接与连贯转换的文章。文中,她将翻译转换的思想与衔接连贯两种手段结合起来,结合实验研究,提出了翻译研究的新方法。本文试图分析Blum-Kulka此理论的意义与局限性。     

Study of the Influence of Parent-brand Similarity,Association,and Complimentary Fit on Co-brand Attributes

In this paper,it investigates the factors affecting successive brand alliance in which two brands from different product categories are featured together to introduce a co-brand.Based on the brand alliance theories,the degree of association,similarity,and complimentary fit between parents brands are important factors in determining successive brand alliance.By using the 5P's,which are premium price,perceived quality,product features,performance,and perceived image,as the measuring scale in brand attributes ...     

Studies on Poly(Dialkoxyphosphazenes) for the Medical Applications

Abstract

The presence of trace of chlorine in poly(diorganophosphazenes) [-N=P(OR)2-]., where R = C₂H₅, CH₂CF₃, C₂F₅, C₄H₅, C₆H₁₃, C₈H₁₇, C₁₂H₂₅, CH₂C₆H₅ in many cases leads to the substantial changes of their physicochemical properties and limits application possibilities of this class of polymers especial for the medical materials. Despite the optimization of reaction conditions for each nucleophilic alkoxy substituent, the obtained poly(dia1koxyphosphaenes) exhibited some physicochemical anomalies.