离子交换-原子捕集-火焰原子吸收光谱法测定水中的超痕量镍

在文中所述条件下,镍的原子捕集灵敏度较常规法高320倍,即在离子交换法浓缩仅40倍的情况下,可使镍的测定灵敏度提高12800倍,从而成功实现了ppt级超痕量镍的测定。     

Image recovery via total variation minimization and related problems

Summary. We study here a classical image denoising technique introduced by L. Rudin and S. Osher a few years ago, namely the constrained minimization of the total variation (TV) of the image. First, we give results of existence and uniqueness and prove the link between the constrained minimization problem and the minimization of an associated Lagrangian functional. Then we describe a relaxation method for computing the solution, and give a proof of convergence. After this, we explain why the TV-based model is well suited to the recovery of some images and not of others. We eventually propose an alternative approach whose purpose is to handle the minimization of the minimum of several convex functionals. We propose for instance a variant of the original TV minimization problem that handles correctly some situations where TV fails. Received December 21, 1995 / Revised version February 26, 1996     

U型钢＋工字钢联锁与锚注加固技术在巷道维修中的应用

白坪煤业公司11采区轨道运输上山受地应力及采动影响，巷道变形严重，经过对围岩应力的分析，采取u型钢＋工字钢联锁与锚注加固技术对巷道进行维修加固。通过实践证明，使用U型钢＋工字钢联锁与锚注加固技术，效果比较明显，有效的控制了巷道的变形。满足了安全生产的需要。     

高位钻孔瓦斯抽采参数优化设计

基于采空区覆岩裂隙分布规律、覆岩裂隙瓦斯流动规律和高位钻孔抽采技术研究现状,从覆岩"竖三带"、"O"形圈和U型通风条件下采动裂隙瓦斯流动规律出发,找出高位钻孔的理论合理布置区域,指出工作面后方50m范围内覆岩裂隙发育状况是高位钻孔层位设计的关键,针对祁南煤矿32煤层的特点,结合现场采用数值模拟方法模拟不同开采速度条件下覆岩裂隙发育规律,优化设计高位钻孔的抽采参数,在34下2工作面和3410工作面的现场试验中,高位钻孔抽采浓度和抽采率得到大大提高,取得了较好的抽采效果,验证了研究的正确性。     

Systematics on fission fragment mass distribution of neutron induced 235U fission

Based on the neutron induced fission fragment mass distribution data up to neutron energy 20 MeV measured with the double kinetic energy method (KEM) and the radio active method (RAM), the systematics of fission fragment mass distribution was investigated by using 5 Gaussian model and the systematics parameters were obtained by fitting the experimental data. With the systematics, the yields of any mass A and at any energy in the region from 0 to 20 MeV of neutron energy can be calculated. The calculated results could well reproduce the experimental data measured with KEM, but show some systematical deviation from the data measured by RAM, which reflects some systematical deviations between the two kinds of measured data.The error of systematics yield was calculated in an exact error transformation way, including from the error of the experimental yield data to the error of the discrete parameters, then to the systematics parameters,and at last to the yield calculated with systematics.     

氨酯键和脲键对嵌段聚氨酯和嵌段聚脲性质影响的研究

用溶液聚合法合成了四种聚氨酯、聚脲模型化合物.并用凝胶渗透色谱,应力—应变,广角X射线衍射等手段检验了在相界面或在硬段微区,不同键对聚合物分子量、力学性质和聚合物形态的影响.     

智能制造系统的一种研究方法

把制造系统描述为互相连接的信息、数据、知识处理单元的集合，把数据、知识处理单元抽象为信息处理单元，构造制造系统的抽象模型，据此提出了一种从这种抽象模型展开对智能制造系统研究的方法．     

对美国海权之路"天时"的思考

踏上海权之路伊始,美国极力避免挑战海军强国,通过与法国的私掠战、第二次英美战争以及南北内战锻炼了自己的海军队伍。19世纪末,利用英国受困于欧洲的有利国际形势,美国通过在大西洋采取守势,向太平洋扩张,实现了海权的振兴。美国的海权发展历程表明,只有在适宜的国际环境下,应“天时”而动,才能突破海权强国的围剿,实现海权的飞跃。     

Two closely linked rice U14 boxC/D snoRNAs

By analysis of the conserved elements in yeast U14 boxC/D snoRNA. the conserved elements in rice U14 boxC/D snoRNA have been speculated. Through computer search of the international rice genome database, two rice U14 snoRNA gene candidates are obtained. These two putative U14 snoRNA genes are closely linked on rice chromosome 2. The coding sequences of these two snoR-NAs exhibit the hallmark structure of boxC/D antisense snoRNA. They both have conserved boxC and boxD sequences and a 14nt-long complement to the sequence between 414nt and 427nt of rice 18S rRNA (according to GenBank accession no. X00755). The experimental evidence shows that these two snoRNAs are involved in the methylation of the complementary sequence of rice 18S rRNA. The existence and localization of these two snoRNAs are proved by RT-PCR and Northern blot. Further analysis shows that both of the newly found rice snoRNAs have high homology with maize U14 snoRNA. and they are named rice U14.1 snoRNA and U14.2 snoRNA respectively. The gene sequence encoding these two snoRNAs has been deposited in the GenBank database under accession number of AF332622.     

合成U3snRNA基因上游启动区构建ACC合成酶反义RNA-核酶嵌合基因的植物表达载体

利用反义 RNA和核酶进行基因表达调控是当今植物分子生物学的研究热点之一 .但在转基因植物中 ,利用 RNA聚合酶 型启动区表达效率不高 .番茄 U3sn RNA基因由 RNA聚合酶 来转录 ,具有较高的转录效率 ,为一般转录效率的 1 0 0～ 1 0 0 0倍 .我们人工合成了番茄 U3sn RNA基因上游启动区 ( 1 5 2 bp) ,构建到番茄 ACC合成酶的反义 RNA-核酶嵌合 DNA序列的上游 ,然后将“启动区 -反义 RNA-核酶嵌合 DNA序列”插入到植物双元表达载体p GA6 4 3中 ,并用三亲融合法导入农杆菌 LBA4 40 4中 ,为研究 U 3sn RNA上游启动区增强反义 RNA-核酶基因的表达奠定了基础