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51.
彭双潮 《光谱学与光谱分析》1999,19(1):123-124
本文利用波动光学的简单方法讨论光栅单色仪的分辨极限与步进电机参数的联系,为最佳利用分辨极限提供了简单可行的实验方法,也给出了用步栅单色仪的分辨率可供参考的例证。 相似文献
52.
In this paper, we present a new phase-field model including combined effects of edge diffusion, the Ehrlich-Schwoebel barrier, deposition and desorption to simulate epitaxial growth. A new free energy function together with a correction to the initial phase variable profile is used to efficiently capture the morphological evolution when a large deposition flux is imposed. A formal matched asymptotic analysis is performed to show the reduction of the phase-field model to the classical sharp interface Burton-Cabrera-Frank model for step flow when the interfacial thickness vanishes. The phase-field model is solved by a semi-implicit finite difference scheme, and adaptive block-structured Cartesian meshes are used to dramatically increase the efficiency of the solver. The numerical scheme is used to investigate the evolution of perturbed circularly shaped small islands. The effect of edge diffusion is investigated together with the Ehrlich-Schwoebel barrier. We also investigate the linear and nonlinear regimes of a step meandering instability. We reproduce the predicted scaling law for the growth of the meander amplitude, which was based on an analysis of a long wavelength regime. New nonlinear behavior is observed when the meander wavelength is comparable to the terrace width. In particular, a previously unobserved regime of coarsening dynamics is found to occur when the meander wavelength is comparable to the terrace width. 相似文献
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Ordered nanofacet structures on vicinal 6H-SiC(0 0 0 1) surfaces, consisting of pairs of a (0 0 0 1) basal plane and a facet, are investigated in terms of stable surface stacking of the (0 0 0 1) basal planes. The surface termination of S3 (or S3*), i.e., ABC (or A*C*B*), was suggested by a structural model based on quantized step-bunching, which typically gives a one-unit-cell bunched step configuration at the facet. Here, we evaluate the surface termination at basal planes covered with a layer of silicon oxynitride by means of quantitative low-energy electron diffraction (LEED) analysis combined with scanning tunneling microscopy (STM), and show the validity of the structural model proposed. 相似文献
56.
R. J. Sobey 《国际流体数值方法杂志》1983,3(6):567-581
A successful and economical fractional step algorithm for the convection-dispersion-reaction equation is described. Exact solutions are adopted for the reaction and convection steps, the latter by the introduction of a moving co-ordinate system. The dispersion step uses an optimized finite difference algorithm which specifically accommodates the grid non-uniformity. The excellent performance of the algorithm is confirmed by numerical experiments together with computations of the Fourier response and integrated square error characteristics. 相似文献
57.
在许多领域,直接倍频仍作为频率合成的主要手段。阶跃恢复二极管单级倍频次数可达10-20以上.可由晶体振荡器直接倍频到微波,得到稳定的频率输出[1-2]。本文介绍了采用阶跃恢复二板管产生梳状波的方法,具有工作频带宽、频率稳定度高、噪声低、电路简单等优点,经制作电路板验证,电路的频带,单边带相位噪声和频率分辨率都达到了预先的设计要求,取得了预期的效果。 相似文献
58.
This problem deals with the thermo-visco-elastic interaction due to step input of temperature on the stress free boundaries of a homogeneous visco-elastic isotropic spherical shell in the context of generalized theories of thermo-elasticity. Using the Laplace transformation the fundamental equations have been expressed in the form of vector–matrix differential equation which is then solved by eigen value approach. The inverse of the transformed solution is carried out by applying a method of Bellman et al. [R. Bellman, R.E. Kolaba, J.A. Lockette, Numerical Inversion of the Laplace Transform, American Elsevier Publishing Company, New York, 1966]. The stresses are computed numerically and presented graphically in a number of figures for copper material. A comparison of the results for different theories (TEWED (GN-III), three-phase-lag method) is presented. When the body is elastic and the outer radius of the shell tends to infinity, the corresponding results agree with the result of existing literature. 相似文献
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Fernanda das Neves Costa Ian Garrard Antonio Jorge Ribeiro da Silva Gilda Guimarães Leitão 《Journal of separation science》2013,36(14):2253-2259
This paper describes the isolation of flavonoids and other aromatic compounds from an ethyl acetate extract of leaves of Siparuna glycycarpa using stepwise elution counter‐current chromatography (CCC). The elution profile yielded the following compounds: diglycosylated flavonoids, quercetin 3‐O‐rutinoside and quercetin 7‐O‐rutinoside, followed by monoglycosylated flavonoids, kaempferol‐3‐O‐β‐glucopyranoside, kaempferol‐3‐O‐β‐rhamnopiranoside, kaempferol‐3‐O‐β‐6′′(p‐coumaroyl) glucopyranoside, and quercetin‐3‐O‐β‐glucopyranoside, and then free phenolics, protocatechuic acid, and 2′,6′‐dihydroxy‐4, 4′‐dimethoxydihydrochalcone, which shows that this type of elution covers a broader range of polarity than the traditional isocratic mode. This makes it more suitable to perform separations of mixtures containing large differences in hydrophobicity. A GC analysis of a blank CCC run was performed to determine if changes in the mobile phase composition affect the chromatographic process. Results showed a gradual variation of the composition of the mobile phase emerging after the step gradient, favoring the selectivity of the solvent system. 相似文献