喷丸镍基合金材料微区残余应力的切槽法测量研究

本文结合聚焦离子束-电子束(Focused ion beam-electron beam,简称FIB-EB)双束系统和真空镀膜工艺,进行微区散斑的制备工艺研究,并将所发展的微散斑制备工艺应用于喷丸镍基合金材料表面制斑,进而结合切槽法进行残余应力高温释放规律的测量研究。在FIB-EB双束系统下记录切槽前后制斑微区的图像,利用数字图像相关法计算切槽后的位移,结合InglisMuskhelishvili理论公式可计算得到残余应力。文中研究了不同温度及保温时间对残余应力释放的影响规律。结果表明,残余应力随保温时间的增长释放速度逐渐减小,最后残余应力趋于稳定值。同时,温度越高,残余应力释放越彻底,800℃下近乎完全释放。该工艺具有适用性好,效率高等优点,可望在材料微区变形测量中得到进一步应用。     

Two-phase flow patterns and size distribution of droplets in a microfluidic T-junction: Experimental observations in the squeezing regime

Generating micrometer sized droplets has been studied in a microfluidic system with T-junction geometry 250 μm in internal diameter and with PTFE capillary tubing. Several experiments were conducted by varying the flow rate of the dispersed phase from $2.78\cdot {10}^{-11}{\text{ m}}^3/\text{s}$ to $5.28\cdot {10}^{-9}{\text{ m}}^3/\text{s}$ and that of the continuous phase from $2.78\cdot {10}^{-10}{\text{ m}}^3/\text{s}$ to $1.94\cdot {10}^{-9}{\text{ m}}^3/\text{s}$. The visualization of different flow regimes (drop, plug, and annular) was carried out for three configurations (not inverted in a horizontal position, inverted in a horizontal position, and inverted in a vertical position) for low capillary numbers. The model of Gauss was also chosen for a droplet size distribution in the dispersed phase, with the flow quality x varying from 0.016 to 0.44. The evolution of the drop size distribution as a function of the flow quality in the dispersed phase shows that the variation coefficient of the droplet's diameter is inversely proportional to the flow quality.     

Experimental study on oil–water flow in horizontal and slightly inclined pipes

Oil–water two-phase flow experiments were conducted in a 15 m long, 8.28 cm diameter, inclinable steel pipe using mineral oil (density of 830 kg/m³ and viscosity of 7.5 mPa s) and brine (density of 1060 kg/m³ and viscosity of 0.8 mPa s). Steady-state data on flow patterns, two-phase pressure gradient and holdup were obtained over the entire range of flow rates for pipe inclinations of −5°, −2°, −1.5°, 0°, 1°, 2° and 5°. The characterization of flow patterns and identification of their boundaries was achieved via observation of recorded movies and by analysis of the relative deviation from the homogeneous behavior. A stratified wavy flow pattern with no mixing at the interface was identified in downward and upward flow. Two gamma-ray densitometers allowed for accurate measurement of the absolute in situ volumetric fraction (holdup) of each phase for all flow patterns. Extensive results of holdup and two-phase pressure gradient as a function of the superficial velocities, flow pattern and inclinations are reported. The new experimental data are compared with results of a flow pattern dependent prediction model, which uses the area-averaged steady-state two-fluid model for stratified flow and the homogeneous model for dispersed flow. Prediction accuracies for oil/water holdups and pressure gradients are presented as function of pipe inclination for all flow patterns observed. There is scope for improvement for in particular dual-continuous flow patterns.     

Investigation on heavy crude-water two phase flow and related flow characteristics

In this paper, heavy crude oil–water flows are studied in a horizontal stainless steel test section with 25.4 mm ID and overall length of 50 m. Crude oil (viscosity = 628.1 mPa s, interfacial tension with water = 10.33 mN/m at 60 °C) and water, collected from an oilfield, were used as test fluids. Visual observations, local sampling and pressure drop measurements were used to identify the flow patterns and their transitions. It was found that in all conditions studied there was a water-in-oil emulsion present. At low mixture velocities and water fractions this occupied the whole pipe cross section. As the velocity or the volume fraction increased water appeared to segregate. At high water fractions and mixture velocities annular flow appeared with the water-in-oil emulsion in the core surrounded by a water layer. The results were compared with those from a model oil with the same viscosity. At low water fractions there was a similarity between the patterns observed with the two oil systems characterized by water segregation from an oil continuous dispersion with increasing water fraction or mixture velocity. However, at high water fractions an oil-in-water dispersion formed with the model oil that was not seen with the crude oil. Pressure drop was generally higher for the crude oil system compared to the model one, while in both cases it decreased when water started to segregate and form layers in contact with the pipe wall. The differences between the two oil systems are attributed to the natural surfactants present in the heavy crude oil (such as asphaltenes and resins), which tend to accumulate on the water/oil interface, retard film drainage and maintain the stability of water drops in oil.     

动物皮肤斑纹形成模式的数值模拟及定性分析

高级生物生命组织的形成机制是十分吸收人的课题，动物皮肤斑纹的变化和复杂性是其中的一个问题，文中对由活化质－基质和一个交换系统组成的系统，采用交替方向隐格式，进行了数值模拟，给出了二维和三维图像，其结果与长颈鹿的皮脸斑纹相符，用中心流形法，对系统的平衡点稳定性作了分析，原始数据条件下，其平衡点是稳定的，而当参数变化较大时，可能会发生突变。     

扣槽式干挂建筑瓷板幕墙试验研究

通过对１６件建筑瓷板的破坏性试验，探讨了瓷板幕墙扣槽式干挂支承的破坏形态、承载力、以及抗剪切和抗弯的计算公式 。     

Shedding patterns of the near-wake vortices behind a circular cylinder

The unsteady incompressible Navier-Stokes equations have been accurately solved for the laminar flow past a circular cylinder in the Reynolds number range 50–200. A direct elliptic solver called the SEVP is used to rapidly advance the streamfunction in time, facilitating the overall convergence to the fully periodic or quasi-steady state. A new integral-series method is developed for the far-field streamfunction condition on a finite two-dimensional computational domain. The use of fourth-order Hermitian relations for the convection terms in the conservation-form vorticity transport equation has also contributed to the good comparison of the present results with the earlier experimental data. The vortex-shedding patterns visualized by the experimentalist are numerically reproduced here in the given Reynolds number range. Discussions that may be helpful in interpreting the behaviour of the shedding frequency are presented in the main text.     

A new family of heavy transition metal coordination compounds and its application,I. Design,synthesis and characterization of volatile organohafnium precursors

The first three representatives of a new family of volatile organohafnium compounds suitable as metallo-organic chemical vapour deposition precursors were synthesized. A combination of cyclopentadienyl and alkoxo-ligands with a bicyclo[2.2.1]heptanc framework was used. Volatility at relatively low temperatures for hafnium compounds was found and the precursors were characterized by elemental analysis and spectroscopic methods (IR, ¹H and ¹³C NMR, mass spectrometry and mass-analysed ion kinetic energy spectroscopy). The outlook for use in hafnium functional materials synthesis was derived from the fragmentation data.     

Heat transfer measurements and correlations for air–water flow of different flow patterns in a horizontal pipe

Heat transfer coefficients were measured and new correlations were developed for two-phase, two-component (air and water) heat transfer in a horizontal pipe for different flow patterns. Flow patterns were observed in a transparent circular pipe using an air–water mixture. Visual identification of the flow patterns was supplemented with photographic data, and the results were plotted on the flow regime map proposed by Taitel and Dukler and agreed quite well with each other. A two-phase heat transfer experimental setup was built for this study and a total of 150 two-phase heat transfer data with different flow patterns were obtained under a uniform wall heat flux boundary condition. For these data, the superficial Reynolds number ranged from 640 to 35,500 for the liquid and from 540 to 21,200 for the gas. Our previously developed robust two-phase heat transfer correlation for a vertical pipe with modified constants predicted the horizontal pipe air–water heat transfer experimental data with very good accuracy. Overall the proposed correlations predicted the data with a mean deviation of 1.0% and an rms deviation of 12%.     

E面和H面方向图等化的双模圆锥喇叭设计

介绍用于Φ7.3 m Cassegrain天线的高功率馈源喇叭的设计。为使E面和H面方向图在照射区域内具有高的等化度,选择双模圆锥喇叭作为馈源的结构形式。由于高功率源采用BJ-32波导输出信号,故馈源系统中还应包含一个矩形到圆形的模式转换器,将TE10模转换为TE11模。设计了双模圆锥喇叭和模式转换器,并进行了功率容量估算。测试结果表明,所设计的馈源达到了设计要求,理论计算结果和实验测试数据吻合良好。