长江源头典型湖泊表层沉积物中多氯联苯残留状况

选择地处长江源头典型湖泊之一的红枫湖为试区,对该水域的14个典型采样点表层沉积物中多氯联苯(PCBs)残留量进行了调研,以揭示长江源头典型湖泊中PCBs的残留现状,以及各种同系物在湖泊底质中的分布特征.结果表明:PCBs残留总量介于ND~87.7 ng/g之间,平均值在27.2 ng/g,主要以4~6氯联苯为主.按残留量均值从高到低的几种同系物依次是:PCB138>PCB153>PCB126>PCB180>PCB105;检出率较高的几种同系物依次是:PCB153>PCB138>PCB126>PCB180.PCBs含量具有明显的地域性,以花鱼洞大桥为界限,将湖分为南北两湖,PCBs总含量北湖明显高于南湖.初步认为工业污染和PCBs理化性质是造成百花湖底质中PCBs来源的主要原因.     

AutoCAD与Protel在电路设计领域中的应用

从基本绘图，开放性，元器件库，三维功能，图主图形输出等方面分析比较了ＡｕｔｏＣＡＤ和Ｐｒｏｔｅｌ在电路设计领域应用的特点，供该领域的人员选择设计软件时参考。     

印刷电路板设计及关键技术的探索与实践

通过对元件库“杂交”扩充，实现了以简单的方式完成复杂的设计，并就PCB设计中的疑难技术作了介绍。     

无铅焊接技术对印制电路板可靠性的影响

阐述了无铅焊接中焊料及其工艺特点,并与有铅焊接进行了比较.分别通过SMT再流焊接和手工焊接陈述了无铅焊接技术在军品上的应用,论述了无铅(混合)焊接对PCB可靠性的影响.     

电子设计自动化之教学探讨

探讨学生在学习电子设计自动化——Protel时容易出现的一些错误,以及教师在教学中应注意的教学方式。     

Fast and parallel determination of PCB 77 and PCB 180 in plasma using ultra performance liquid chromatography with diode array detection: A pharmacokinetic study in Swiss albino mouse

A simple, sensitive and reproducible ultra‐performance liquid chromatography (UPLC) method has been developed and validated for simultaneous estimation of polychlorinated biphenyl (PCB) 77 and PCB 180 in mouse plasma. The sample preparation was performed by simple liquid–liquid extraction technique. The analytes were chromatographed on a Waters Acquity H class UPLC system using isocratic mobile phase conditions at a flow rate of 0.3 mL/min and Acquity UPLC BEH shield RP₁₈ column maintained at 35°C. Quantification was performed on a photodiode array detector set at 215 nm and PCB 101 was used as internal standard (IS). PCB 77, PCB 180, and IS retention times were 2.6, 4.7 and 2.8 min, respectively, and the total run time was 6 min. The method was validated for specificity, selectivity, recovery, linearity, accuracy, precision and sample stability. The calibration curve was linear over the concentration range 10–3000 ng/mL for PCB 77 and PCB 180. Intra‐ and inter‐day precisions for PCBs 77 and 180 were found to be good with CV <4.64%, and the accuracy ranged from 98.90 to 102.33% in mouse plasma. The validated UPLC method was successfully applied to the pharmacokinetic study of PCBs 77 and 180 in mouse plasma.     

提高抗干扰能力的PCB布局

介绍了干扰的种类与PCB特性,给出了详细的各种抗干扰方案,研究了具有模拟电路的单片机系统如何实现合理的PCB布局问题,以ATMega16单片机的测温系统为例,详细介绍了PCB布局,可为设计基于单片机的测温系统提供参考。     

车载移动卫星通信系统电磁屏蔽研究

为了减少外界电磁脉冲对车载移动卫星通信系统的电磁损伤,通过设置带孔缝的屏蔽腔体对系统内部各组件进行电磁防护。应用传输线理论,将带孔缝的屏蔽腔体建模成传输线,腔体内部的PCB板建模成特殊的传输层,求解出腔体内任意点的屏蔽效能。仿真结果表明：本文所建模型可以很好地拟合实验数据,验证了本文模型的准确性,很好地解决了运算速度与精确度之间的矛盾。模型给出了电磁脉冲入射角、极化角、腔体和孔缝尺寸等对屏蔽效能的影响,为工程实践中进行电磁屏蔽提供了很好的理论基础。     

图像处理技术在焊点检测中的应用

将图像处理技术引入PCB焊点检测中,对焊点进检测：用LOG算子进行图像滤波和增强,然后利用最优阈值法进行图像分割,接下来进行形态学处理,最后用颗粒分析获得目标特征参数实现焊点分析．经过试验表明,该系统操作简单,效率高,可以很好地实现对焊点质量的检测．     

Column Chromatographic Procedure for the Determination of Polychlorinated Biphenyls in Certain Industrial Oils

Abstract

Certain oils cause considerable interference in the determination of PCBs by gas chromatography with electron capture detection, requiring time-consuming sample clean-up procedures. Column chromatography, using small, radially-compressed silica columns, is used to isolate PCBs in various oil matrices, thus permitting quantitative analysis. Pure mineral oil, phosphate ester, glycol-base, and sulfonated mineral oils were studied.