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51.
The strength of basic sites has been measured by pyrrole-IR on alkali metal cation exchanged β and X zeolites, as well as NaOH loaded Naβ. The influence of cation type and the structure of zeolites on their basicity has been studied. The acidic and basic properties of the samples were investigated by NH3-TPD and isopropanol reaction. It was shown that the strength of basic sites on samples could be characterized by the shift of vNH band in the pyrrole-IR spectra. The framework oxygen charges were calculated from the Sanderson electronegativity. The changes in basic properties with various alkali metal cation are consistent with the changes of local oxygen charges of the zeolite framework.  相似文献   
52.
We have used both reflection-geometry and grazing-incidence-geometry X-ray scattering to study thin films of C60 evaporated onto mica substrates via a hot-wall technique. The growth mode yields close-packed C60 planes, which are parallel to the substrate surface and which exhibit out-of-plane correlation lengths of 850 Å. In the film plane the C60 is at best pseudo-epitaxial, with a 0.9° distribution of crystallite orientations, a 450 Å in-plane correlation length, and a 3.7% lattice mismatch, better than obtained by other thin film techniques but far from the accepted definition of single crystal thin film epitaxy.  相似文献   
53.
井下抽油泵柱塞与泵筒运动规律的研究   总被引:1,自引:0,他引:1  
用三元振动模型,综合考虑油柱、抽油杆柱和油管柱的振动.建立起数学模型并离散化,然后用微机编程求解微分方程组.对不同工况下的抽油泵运动规律和抽油机示功图进行分析研究,得出了油管应予锚定的结论,并给出了不同抽油机的适用范围.为进一步研究抽油泵的井下工作机理和故障原因打下了基础.  相似文献   
54.
本文研究作为双层桥模型的梁方程耦合系统,利用Leray-Schauder不动点定理,得到了一个关于这种系统的解的存在性定理,它类似于McKenna和Walter文2中关于吊桥方程的一个定理。  相似文献   
55.
 应用高压原位差热方法,直接测量了压力下锗的固化参数─—固化温度与过冷度。高压差热信号表明,当压力大于3 GPa时,锗在凝固过程中可能发生结构相变。X射线结构分析表明,在最终的样品中除GeⅠ相外,还形成GeⅢ相和GeⅣ相。  相似文献   
56.
回顾用吴文俊先生提出的消元方法求解带参数的杨—Baxter方程的技巧和主要结果。  相似文献   
57.
与半群的完全不可逆生成集相关的几个性质   总被引:3,自引:3,他引:0  
讨论了半群环的两个性质以及关于半群的a.c.c.p.(主理想升链条件)的一个结论。  相似文献   
58.
59.
Surface relief formation at holographic recording on amorphous selenium films was demonstrated and investigated. The presence of this optical phase modulation component is essential for ensuring significant, stable and erasable optical recording in a-Se films at 290–320 K temperatures, where conventional photodarkening was known as insignificant and unstable. Photocrystallization can only be observed in super-exposed a-Se films at the given experimental conditions of hologram recording. Erasing behavior of surface relief gratings under heat treatment was also investigated in order to reveal further details of the mechanism. Photoinduced structural transformations within the amorphous phase, connected to local ordering under the condition of light-induced fluidity, are proposed as an explanation for the relief formation and erasing. The observed reversible optical recording process may be useful for the various optoelectronic applications of photoconductive a-Se layers. Received: 12 June 2000 / Accepted: 6 June 2001 / Published online: 30 August 2001  相似文献   
60.
Optimization of the surface texture for silicon carbide sliding in water   总被引:7,自引:0,他引:7  
Surface texturing has been recognized as an effective means to improve the tribological performances of sliding surfaces. Usually, generation additional hydrodynamic pressure to increase the load carrying capacity is regarded as the most significant effect of surface texture. In the case of silicon carbide sliding against identical material in water, the experimental results indicate that surface texture is also helpful to improve the running-in progress to smooth the contact surfaces, showing another reason to result in low friction. Based on the consideration of enhancing the generation of hydrodynamic pressure and improving running-in progress, a surface texture pattern, which was combined with large (circle, 350 μm in diameter) and small (rectangular, 40 μm in length) dimples, was designed to maximize the texture effect on the load carrying capacity of SiC surfaces sliding in water. The friction coefficient of such textured surface was evaluated and compared with that of untextured and those only with large or small dimples only. The friction reduction mechanisms of the patterns with different dimples in size are discussed.  相似文献   
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