发射光谱法同时测定地质样品中微量Ag和Mo

采用按Na2CO3：C：BaO：硅酸盐基体=11．25：48．75：15．00：25．00的比例配制的光谱缓冲剂，以Pd为Ag和Mo测定的内标元素，用发射光谱法测定了地质样品中的微量Ag和Mo，对Ag和Mo分析的RSD％分别为0．61％～3．5％和0．60％～2．3％。     

中国古代历法推没灭术算理分析

指出由于唐朝科学家张遂对灭给出了新的定义，从而，以《大衍历》为界，可将我国古代历法中的推没，灭术分为两个阶段；分析了这两个不同阶段里没，灭算法的数学原理；对没，灭在古历中的作用提出了初步的看法。     

高电荷态离子Arq+入射在金属表面形成靶原子X射线谱

本文报道低能高电荷Ar12+、Ar13+ 、Ar14+离子与金属Mo表面作用过程中Mo原子受激发射X射线和X射线强度随入射能量变化的实验结果.结果表明,低速高电荷离子与金属表面原子相互作用可有效地激发靶原子或靶离子内壳层电子而发射X射线.     

炮口制退器的焊接

炮口制退器的主要材料为PCrNi3Mo。对PCrNi3Mo钢实施焊接后出现的冷裂纹及残余奥氏体的原因进行了论述，提出了预防及解决措施，成功地解决了炮口制退器的焊接问题。     

Intra-elemental photoelectron line intensities and their significance to quantitative analysis

Intraelemental relative photoelectron line intensities for 20 pure elements obtained under ultrahigh vacuum (5·10^?9 torr) and high resolution with cleaned surfaces are presented. Theoretical and experimental aspects of relative photoelectron line intensities as well as other characteristics of significance to quantitative analysis are discussed. Experimental data are related to theoretical results and compared with other recent work.     

（NH_4）_2MOS_4在活性炭上浸渍过程的研究Ⅰ．浸渍参数对（NH_4）_2

（ＮＨ＿４）＿２ＭＯＳ＿４在活性炭上浸渍过程的研究Ⅰ．浸渍参数对（ＮＨ＿４）＿２ＭＯＳ＿４在活性炭上分布的影响秦慧芳，张成芳，陆岗，俞丰，朱子彬（华东理工大学无机化工研究所，上海２００２３７）关键词硫代钼酸铵，浸渍，活性炭，钼分布负载型催化剂制备一般...     

~（95）Mo NMR谱及其在钼化学研究中的应用

对~（９５）ＭｏＮＭＲ的特点、提供的信息、发展历史以及研究现状作了较为全面的介绍。结合本实验室研究工作和部分文献报道对其在钼化学研究中的应用进行了较为详细的论述，同时还指出影响~（９５）ＭｏＮＭＲ的因素并进行了简单分类和讨论。     

Investigation of thermostability and phonon–phonon interactions in Mo6S3I6 nanowires by Raman scattering spectroscopy

Detailed Raman scattering measurements were performed on molybdenum–sulfur–iodine nanowires (Mo₆S₃I₆). At room temperature, 21 well‐resolved Raman modes were experimentally observed for the first time in this new compound. The phase stability and vibrational properties of the nanowires were investigated by different temperature treatments. High‐temperature Raman spectra showed that the phase separation of Mo₆S₃I₆ nanowires took place between 573 and 673 K, followed by appearance of a new mode at 819 cm⁻¹ characteristic of the MoO₃ phase. Low‐temperature Raman scattering spectra showed a significant difference in phonon–phonon interactions between internal and external Raman modes of Mo₆S₃I₆ nanowires. These interesting vibrational properties can give new insights for improved material preparation and achievement of higher conductivity and other functional properties of these otherwise interesting materials. Copyright © 2009 John Wiley & Sons, Ltd.     

河南省钼多金属矿集区重磁异常特征及成矿预测

河南省钼矿资源丰富,集中分布于栾川、大别山地区,多与中酸性浅成-超浅成的岩浆侵入关系密切.省内已知的钼矿床多分布于重力低异常区或外围梯级带上,在航磁异常图上,钼多金属矿集区及附近的ΔT异常分布规律性不强,其异常性质及规模受成矿母岩、成矿类型及围岩性质控制.通过总结钼多金属矿集区的重力和航磁异常特征,建立了矿集区的地质、地球物理成矿模式,据此对夜长坪、南泥湖、东沟、涩港、吴陈河、汤家坪等矿集区进行找矿前景分析及成矿预测,认为夜长坪、南泥湖矿集区及新县岩体的东西两侧、商城岩体南侧找矿潜力大.