牙轮钻头滑动轴承接触参数的计算及力学分析

应用边界元法（ＢＥＭ）计算了两种牙轮钻头大滑动轴承的接触参数,讨论了外载荷、配合间隙、材料配对组合等因素对滑动轴承接触力学性质的影响。计算结果表明,小尺寸钻头上载荷的减小值与轴承结构尺寸的减小值不成比例关系,这是小直径钻头寿命短的原因之一。滑动轴承载荷增大时,峰值接触压力的变化幅度比接触区域的变化幅度大,前者又比载荷的变化幅度小,这说明该类接触问题是非线性的。轴承系统的径向间隙越小,相应的峰值接触压力越低;轴承摩擦副材料硬度越低,相应的峰值接触压力越低。     

南北洋平原排涝减灾对策探讨

福建省莆田市木兰溪下游河网密集,南北洋平原涝灾频繁,根据现状对其成因进行分析,对存在问题进行总结,提出相应的治理措施与对策。     

Synthesis of polymers in aqueous solutions: Synthesis of polysulfide by reaction of bis(4‐mercaptophenyl) sulfide with bis(4‐chloro‐3‐nitrophenyl) sulfone using various bases in aqueous solutions

The polycondensation of bis(4‐mercaptophenyl) sulfide (BMPS) with bis(4‐chloro‐3‐nitrophenyl) sulfone (BCNPS) was examined using various organic or inorganic bases in mixed solvents of N‐methyl‐2‐pyrrolidone (NMP) with water or in plain water. The reaction of BMPS with BCNPS proceeded smoothly to give the corresponding polysulfide in mixed solvents of NMP with water at 60 °C using 1,8‐diazabicyclo[5.4.0]undecene‐7 as a base, although the rate of the reaction decreased gradually as the water in the solvent increased. Polysulfide can also be obtained by reaction in plain water using appropriate organic bases such as tripropylamine (TPA) or quinoline. The polysulfide with a number‐average molecular weight of 45,100 was synthesized in 62% yield when the reaction of BMPS with BCNPS was performed using TPA as a base at 60 °C for 48 h in plain water. © 2000 John Wiley & Sons, Inc. J Polym Sci A: Polym Chem 38: 3399–3404, 2000     

惠东黄蚜小蜂空间分布特征及林间应用研究

研究惠东黄蚜小蜂的方位动态,结果表明:在马尾松林中的不同坡位上、树冠不同方位上其平均密度差异不显著;在树冠的不同层次上其平均密度差异显著,主要表现为下层>中层>上层.应用聚集度指标法和回归分析法测定惠东黄蚜小蜂空间分布特征,结果表明:12块标准地惠东黄蚜小蜂聚集度指标均服从聚集分布.Iwao和Taylor幂法则回归方程分别为:M·=1.1447-x+1.7983和S2=2.90681-0.8501x,两个方程的相关系数较高,表明惠东黄蚜小蜂的种群分布在一切密度下都是聚集的,分布的基本成分是疏松的个体群,这种种群聚集与其寄主害虫松突圆蚧的空间分布特征有关.最后列出其最适抽样数和序贯抽样方案.     

黄道周政治教化思想的工具与目的阐论

晚明大儒黄道周的《缁衣集传》,对儒家政治教化思想中工具与目的的关系有详细的论述。在黄道周看来,礼乐制度是使“民有孙心”的正确工具,政治刑赏须在礼乐制度下运行。而礼乐之所以能运行,背后需有美德教化作为支撑,因为君主的德行是众善所归,众善归于君子之德正是民有孙心的体现。黄道周认为这是民众的一种政治需求,即君主须具有德行才能获得民众的信任。“民有孙心”既是黄道周政教思想的教化目的,同时也是通往终极目的——达到易简之政的工具。易简的道理运用于政治运作中,就是达到上下易事易知、明朗通透,不需求助于烦难的政治手段,反映了黄道周在面临晚明时期君民上下隔绝的问题时所作出的思考与应对方案。     

2-烷基-6-甲氧基-1,4-苯醌的全合成

3,5-二甲氧基苯甲醛经格氏、氧化反应制到3,5-二甲氧基苯基烷基酮, 然后在微波辐射下经黄鸣龙还原和选择性脱甲基化、Teuber氧化反应制得目标化合物, 产率均在50%以上. 产物结构经IR, 1H NMR, 元素分析等进行了表征.     

怀菊花中微量铁的测定

为探讨邻二氮菲分光光度法测定怀菊花中微量元素铁含量的可行性,怀菊花的药理功效、食用营养价值与微量元素含量可能存在的关系,根据铁离子与特定显色剂显色产生可见吸收,采用混合酸y（HNO3）：V（HClO4）=4＋1对怀菊花样品湿法消化处理,在pH2～9的溶液中试剂与铁生成稳定的橙色络合物,并用分光光度法测定了怀菊花中微量元素铁含量。结果表明,所选的怀菊花中铁含量303．9～337．9μg／g,加标回收率为90．2％～100．6％。分光光度法操作简便、干扰离子少,测量快速、结果准确度和灵敏度高,易推广和 普及使用。     

Determination and pharmacokinetic study of chlorogenic acid in rat dosed with Yin-Huang granules by RP-HPLC

A reversed-phase high-performance liquid chromatographic (RP-HPLC) method was described for the determination of chlorogenic acid (CGA) in rat plasma using protocatechuic acid as internal standard (IS). CGA in plasma was extracted with acetonitrile, which also acted as deproteinization agent. Chromatographic separation was performed on a Kromasil C18 column with methanol-0.2 m acetic acid (pH 3.0, 25:75, v/v) as mobile phase at a flow-rate of 1.0 mL/min with an operating temperature of 30 degrees C and UV detection at 300 nm. The standard curve was found to be linear over the concentration ranges of 0.4-2.5 microg/mL and 2.5-40 microg/mL, and the limit of quantification (LOQ) was 0.4 microg/mL. The analytical precision and accuracy were validated by relative standard deviation (RSD) and relative error, which were in ranges 3.14-10.78% and -2.20-5.00%, respectively. The average recovery of CGA was 87.59%. The method was successfully applied to the pharmacokinetic study of CGA in Yin-Huang granules.     

安塞油田高52井区长10油层沉积微相研究

通过野外剖面观察、岩心描述和测井资料分析,确定了高52井区长10油层主要为三角洲平原亚相沉积,主要沉积微相有分流河道、河道边缘(天然堤、决口扇)、分流间湾和泛滥平原等,分流河道是本区占主导地位的骨架砂体,在图像粒度分析的基础上,通过绘制各类粒度图,对该区砂体形成的水动力条件及形成环境进行了分析。根据岩心微相和测井微相分析,对长10油层沉积微相进行了研究,掌握了沉积微相的时空展布和变化规律。同时探讨了沉积相与油气关系,结果表明:沉积微相控制着储层的物性和含油性,分流河道是主要的有利储层,为该区进一步高效开发提供了技术支持。     

文献信息资源共建共享模式探究——以淮安高校联合体为例

图书馆信息资源的共建共享是提高信息资源社会价值最有效的方法之一。分析了淮安高校联合体图书馆文献资源的共享现状,提出了淮安地区高校联合体文献信息资源共建共享的对策。