新型闪光X射线设备设计方案

本文叙述了我们正在研制的新型闪光X射线设备的设计方案。其主要特点是:(1)毫微秒脉冲发生器采用组件式结构与美国Hewlett-Pac ard公司的产品相似,(2)减少了Marx发生器回路的电感,可提高闪光X射线设备的输出电压及减少设备的体积,(3)采用多级触发,扩展了球隙开关的触发工作范围,(4)采用多尖阴极的爆炸发射闪光X射线管,增加了闪光X射线管的输出剂量及寿命。 改进后的设备,将达到和部份超过美国Hewlett-Packard公司产品的性能。     

小焦斑纳秒激光烧蚀铝平面靶的数值研究

用二维辐射流体程序Flash模拟了小焦斑纳秒激光与铝平面靶的相互作用过程,其中入射激光的聚焦半径为25 m,峰值强度约为1013 W/cm2,波长为532 nm。模拟发现激光通道上的等离子体出现了密度排空的现象,激光焦斑外侧出现环状的射流结构。激光通道上密度排空现象对电子热输运的计算较为敏感,对比干涉实验测量的密度分布,确定了模拟中限流因子的取值为0.08。通过考察辐射致冷与电子横向热输运对等离子体膨胀运动的影响,对环状射流结构的形成原因给出了物理解释,并在模拟上验证了辐射冷却在其形成过程中的主导作用。     

《C语言》网络考试系统的开发

以课程为例介绍网络考试系统的开发方法.     

用FlashMX制作物理课件的研究与探索

从物理教学的实践出发,对FlashHX多媒体课件的制作和应用进行了研究和探索,对课件的设计、制作以及应用中应注意的问题提出了一些新的思路和看法.     

Antioxidant activity guided separation of major polyphenols of marjoram (Origanum majorana L.) using flash chromatography and their identification by liquid chromatography coupled with electrospray ionization tandem mass spectrometry†

Marjoram extracts have been separated into polar and nonpolar parts using liquid–liquid extraction. Both polar and nonpolar parts of the extracts were further fractionated by flash chromatography. The obtained fractions (90 polar and 45 nonpolar fractions) were investigated for their antioxidant activities by 2,2‐diphenylpicrylhydrazyl and ferric ion reducing antioxidant power assays. A direct, positive, and linear relationship between antioxidant activity and total phenolic content of the fractions was observed. Based on antioxidant and total phenolic content data, the three fractions with the high antioxidant activities from polar and nonpolar part of the extract were analyzed for their constituent polyphenols by liquid chromatography coupled with electrospray ionization tandem mass spectrometry. Compounds were identified by matching the mass spectral data and retention time with those of authentic standards. Identification of the compounds for which there were no “in‐house” standards available was carried out by accurate mass measurement of the precursor ions and product ions generated from collision‐induced dissociation. Rosmarinic acid was found to be the strongest antioxidant polyphenol conferring the highest antioxidant activity to fractions 47 and 17 of polar and nonpolar part of the extract, respectively. The identification of the rosmarinic acid was further confirmed by ¹H NMR spectroscopy.     

工程制图网络课程的研究与开发

本文在介绍了基于Web的网络课程的特点基础上，重点阐述基于Web的工程制图网络课程的设计与开发，包括该网络课程的设计思想与系统实现。其中，对形象设计、导航设计和网络动画制作等内容作了重点介绍。     

Flash在《基础化学实验Ⅰ》课件制作中的应用

用Flash 5制作<基础化学实验Ⅰ>多媒体课件中的素材,并用Authorware 5 Attain作为集成工具,制作具有一定交互功能的、集教与学为一体的多媒体课件.     

Rapid discrimination of slimming capsules based on illegal additives by electronic nose and flash gas chromatography

The discrimination of counterfeit and/or illegally manufactured medicines is an important task in the pharmaceutical industry for pharmaceutical safety. In this study, 22 slimming capsule samples with illegally added sibutramine and phenolphthalein were analyzed by electronic nose and flash gas chromatography. To reveal the difference among the different classes of samples, principal component analysis and linear discriminant analysis were employed to analyze the data acquired from electronic nose and flash gas chromatography, respectively. The samples without illegal additives can be discriminated from the ones with illegal additives by using electronic nose or flash gas chromatography data individually. To improve the performance of classification, a data fusion strategy was applied to integrate the data from electronic nose and flash gas chromatography data into a single model. The results show that the samples with phenolphthalein, sibutramine and both can be classified well by using fused data.     

Sample enrichment in high speed narrow bore capillary gas chromatography

Reduction of the column diameter has proved to be a highly efficient tool to increase the speed of analysis. Unfortunately, the requirements for instrumental design with respect to sample input band width, low dead volume interfacing, and time constants of detection and registration systems are the more critical the smaller the inside diameter. Recently we reported input band widths as low as 1 ms [1] for gaseous samples at ppm concentration levels, without any preconcentration, in a study with narrow bore columns and thermal conductivity detection. In this study a simple versatile micro on-column cold trap/thermodesorption enrichment system for narrow bore columns is introduced and evaluated. The combination of considerable sample enrichment and preservation of the compatibility of the required input band width with column dimensions is critically examined. The process of thermodesorption (reinjection) which is the most critical step, is particularly emphasized. The system consists of a short aluminum coated fused silica or metal capillary with a low mass and a low cost electrical heating. Input band widths down to 1 ms are obtained without extreme demands on electrical power (300 watt). The potential of the system is illustrated with some extremely fast separations.     

基于flash的嵌入式文件系统

目前嵌入式手持设备与多媒体应用中大量数据存储在Flash中。本文针对Flash存储器的特点,设计了一种适合在嵌入式系统中使用的文件系统。该文件系统采用三层结构设计,为应用程序开发提供统一的标准API函数,具有良好的可维护性和移植性;另外,采用分布式文件分配表的存储结构．提高了文件系统的可靠性。