大学生学习焦虑心理研究

通过分析大学生学习焦虑心理的成因以及学习焦虑控制问题。论述了大学生学习焦虑心理与学习成绩的关系。     

拓扑线性空间中的Drop定理和Phelps引理以及Ekeland变分原理

将Phelps引理, Ekeland变分原理, Pareto有效性定理推广到拓扑线性空间,同时证明了这三个定理与郑喜印证明的拓扑线性空间中的Drop定理彼此等价．     

运用严格耦合波理论计算平面电介质光栅的衍射效率

本文阐述了严格耦合波理论的基本思想。针对横电波的情况，详细分析了运用严格耦合波理论实现光栅衍射效率计算的方法，并且进一步给出了编制计算衍射效率程序的步骤。通过一个具体计算实例表明：各衍射级分布的光能量之和等于入射光的能量，满足能量守恒定律，从而证实了计算结果的正确性。     

能量系统两种基本组合模型及其影响因子的分析

运用小偏差法分析了能量系统的两种基本组合模型中部件的效率、输入量以及各种部件或环节的损率等参数对系统总效率的影响,提议用相关的“影响因子”分析各种因素对系统总效率的影响程度。本文导得的公式与结论,不仅对于探求系统如何合理用能和参数的优化有一定作用,而且对于分析系统的动态特性也将有所裨益。     

镀铜铁屑-H_2O_2催化氧化降解含酚废水

采用镀铜铁屑代替传统Fenton体系中的FeSO4作为催化剂,通过改变H2O2与镀铜铁屑的投加量、溶液的pH值、反应温度、反应时间等条件,研究了该体系对处理苯酚废水的影响。结果表明,常温下处理实际含酚印染废水,在pH值为4~6,30%H2O2 12mL/L,镀铜铁屑5g/L,反应时间为45min时,COD去除率可达96%,其CODCr从5827mg/L降至419mg/L,色度从2000降至30,符合国家三级排放标准。     

A study of the oxidation of vegetable oils by inverse gas chromatography

Summary Inverse gas chromatography is shown to be suitable for the study of the oxidation of vegetable oils. With air as carrier gas characteristic plots of retention index versus time are obtained for hydroxylic test solutes that are consistent with the oxidation behaviour of vegetable oils. Shifts of retention are found to be accompanied by changes of column efficiency due to the oxidative crosslinking of polyunsaturated vegetable oils. The technique also leads to useful information concerning the oxidation of antioxidant inhibited systems. Presented at the 15th International Symposium on Chromatography, Nürnberg, October 1984     

Mesoporous material as catalyst for the production of fine chemical: Synthesis of dimethyl phthalate assisted by hydrophobic nature MCM-41

Aluminum, iron and zinc containing MCM-41 molecular sieves were prepared by the hydrothermal method. The catalyst was characterized by the XRD, BET (surface area), FT–IR and ²⁹Si, ²⁷Al MAS–NMR techniques. The catalytic activity of these molecular sieves was tested with esterification reaction used with phthalic anhydride (PAH) and methanol (MeOH) in the autoclave at 135 °C, 150 °C and 175 °C. Conversion increases with an increase in temperature and mole ratio. The activity of these catalysts followed the order: Al-MCM-41 (112) > Fe-MCM-41 (115) > Al-MCM-41 (70) > Al-MCM-41 (52) > Fe-MCM-41 (61) > Al, Zn-MCM-41 (104) > Al-MCM-41 (30). The reaction yielded both monomethyl phthalate (MMP) and dimethyl phthalate (DMP). The nature of the catalyst sites has been proposed using with water as an impurity. The selectivity of the dimethyl phthalate increases with increase in temperature and mole ratio. The weight of the catalyst was optimized at 0.07 g. The hydrophilic and hydrophobic nature of the catalyst has been explained by the influence of water and the external surface acidity also facilitates the reaction and this has been confirmed by the supporting reaction.     

A new type of two-dimensional packed + capillary column GC system. I. Theory

Summary To match the need of high efficiency capillary column (plate number N₂, Plate height H₂ and carrier gas linear velocity U₂), a new high efficiency packed column (N₁, H₁ and U₁) at high carrier gas velocity with small capacity factor has been developed in the light of theoretical discussion of factors effecting the column efficiency utilization ratio.     

TiO2光催化反应及其在环境保护中的应用

本文简要介绍了TiO2光催化剂的作用机理，讨论了影响TiO2光催化效率的因素及解决途径，综述了光催化在环境保护中的最新应用。     

Synthesis and fluorescent properties of some new unsymmetricbis-benzothiazolyl furans and thiophenes

Summary Some newmono- andbis-benzothiazolyl compounds with furan or thiophene nuclei were synthesized by multistep reactions from the corresponding furan and thiophene aldehydes. The data obtained from emission spectra show a large influence of the benzothiazole rings on the relative quantum efficiency of the compounds under investigation.

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Synthese und Fluoreszenzeigenschaften von neuen unsymmetrischenbis-Benzothiazolylfuranen und thiophenen

Zusammenfassung Einige neuebis-Benzothiazolylverbindungen mit einem Furan- bzw. Thiophenenring wurden in einer mehrstufigen Reaktion dargestellt. Die Fluoreszenzdaten der untersuchten Verbindungen zeigen einen großen Einfluß der Benzothiazolringe auf die relative Fluoreszenzquantenausbeute.