公示写作理论及要素探析

公文写作与时俱进，新的文种随着时代的发展进步而应运而生。公示正是在人事制度改革的完善，选拔任用领导干部的公示制度的推行下被人们广泛运用于工作实践中的。目前，公示写作缺乏理论的构建与支撑，内容与形式尚未形成统一。因此，有必要对公示的一般特质、写作功效、要素构成以及理论实践进行探讨，以便更好地规范和指导今后的公示写作。     

13C CP MAS NMR of halogenated (Cl,Br, I) pharmaceuticals at ultrahigh magnetic fields

This work reports significantly improved spectral resolution of ¹³C CP MAS NMR spectra of chlorinated, brominated and iodinated solid organic compounds when such spectra are recorded at ultrahigh magnetic field strengths. The cause of this is the residual dipolar coupling between carbon atoms and quadrupolar halogen nuclides (chlorine‐35/37, bromine‐79/81 or iodine‐127), an effect inversely proportional to the magnetic field strength which declines in importance markedly at 21.1 T as compared to lower fields. In favorable cases, the fine structure observed can be used for spectral assignment, e.g. for Cl‐substituted aromatics where the substituted carbon as well as the ortho‐carbons show distinct doublets. The experimental results presented are supported by theoretical modeling and calculations. The improved spectral resolution in the studied systems and similar halogenated materials will be of particular interest and importance for polymorph identification, drug discovery and quality control in the pharmaceutical industry. Copyright © 2009 John Wiley & Sons, Ltd.     

Structure determination of salisomide and salisoflavan,two new secondary metabolites from Salsola imbricata,by 1D and 2D NMR spectroscopy

Chromatographic analysis of the alcoholic extract from Salsola imbricata yielded two new secondary metabolites, salisomide (1) and salisoflavan (2). Their structures were established with the help of spectroscopic techniques including COSY, HMQC and HMBC NMR experiments. Copyright © 2008 John Wiley & Sons, Ltd.     

Tetrapterosides A and B,two new oleanane‐type saponins from Tetrapleura tetraptera

From the stem bark of Tetrapleura tetraptera, two new oleanane‐type saponins, tetrapteroside A 3‐O‐{6‐O‐[(2E,6S)‐2,6‐dimethyl‐6‐hydroxyocta‐2,7‐dienoyl]‐β‐D ‐glucopyranosyl‐(1 → 2)‐β‐D ‐glucopyranosyl‐(1 → 3)‐β‐D ‐glucopyranosyl‐(1 → 4)‐[β‐D ‐glucopyranosyl‐(1 → 2)]‐β‐D ‐glucopyranosyl}‐3,27‐dihydroxyoleanolic acid (1), and tetrapteroside B 3‐O‐{ β‐D ‐glucopyranosyl‐(1 → 2)‐6‐O‐[(E)‐feruloyl]‐β‐D ‐glucopyranosyl‐(1 → 3)‐β‐D ‐glucopyranosyl‐(1 → 4)‐[β‐D ‐glucopyranosyl‐(1 → 2)]‐β‐D ‐glucopyranosyl}‐3,27‐dihydroxyoleanolic acid (2), were isolated. Further extractions from the roots led to the isolation of four known oleanane‐type saponins. Their structures were elucidated by the combination of mass spectrometry (MS), one and two‐dimensional NMR experiments. Copyright © 2009 John Wiley & Sons, Ltd.     

广义Stirling数偶的理论及应用

The object of this expository paper is to sum up several results concerning generalized Stirling number (GSN) pairs investigated earlier by the author. Also expounded in some detail are two kinds of extended GSN pairs with applications (illustrative examples).     

2Cr13钢调质后奥氏体粗晶遗传及其对性能的影响

本文对汽轮机末级叶片钢2Cr13粗晶马氏体在重新加热淬火后的粗晶遗传现象进行了研究,观察了在奥氏体化时恒温形成的动力学和组织结构。讨论了在相变区的加热速度、奥氏体化温度及保温时间对奥氏体晶粒的影响。研究表明,调质后粗晶奥氏体的遗传现象,是由于沿原奥氏体晶界碳化物偏聚析出的结果。还讨论了奥氏体晶粒度对调质后力学性能的影响,扫描及透射电镜观察结果表明,调质后的力学性能,主要取决于钢中碳化物的分布及尺寸。     

On the radical of a monomial ideal

Algebraic and combinatorial properties of a monomial ideal and its radical are compared. Received: 9 October 2004     

Stability of some low‐order approximations for the Stokes problem

Two‐level low‐order finite element approximations are considered for the inhomogeneous Stokes equations. The elements introduced are attractive because of their simplicity and computational efficiency. In this paper, the stability of a Q₁(h)–Q₁(2h) approximation is analysed for general geometries. Using the macroelement technique, we prove the stability condition for both two‐ and three‐dimensional problems. As a result, optimal rates of convergence are found for the velocity and pressure approximations. Numerical results for three test problems are presented. We observe that for the computed examples, the accuracy of the two‐level bilinear approximation is compared favourably with some standard finite elements. Copyright © 2007 John Wiley & Sons, Ltd.     

中国中青年男性全血比粘度参考值与地理因素的相关研究

为制定中国中青年男性全血比粘度参考值的统一标准提供科学依据，收集了中国各地用毛细管法测定的健康中青年男性全血比粘度参考值，并对其与地理因素的关系进行了研究，发现海拔高度是影响中青年男性全血比粘度参考值最主要的因素．随着海拔高度的逐渐增大，中青年男性全血比粘度参考值也在逐渐地增大，相关性很显著．用逐步回归分析的方法推导出了一个回归方程，如果知道了中国某地的地理因素，就可以用回归方程估算这个地区的中青年男性全血比粘度参考值，依据中青年男性全血比粘度参考值与地理因素的依赖关系把中国分为青藏区，西南区、西北区、东南区、华北区、东北区等６个区．     

一种特殊设计约束面的有限元网格优化问题

网格设计质量的优劣是有限元分析的关键，对一些特殊的设计约束面，网格的优化设计是建模时需要首先研究解决的问题，本文对两种材料在几何尺寸差异很大情况下的有限元网格进行了优化设计并对其进行了讨论。