由27Al的核磁共振谱看高岭土与针铁矿的胶结本质

通过对高岭土与针铁矿的人工胶结样的²⁷ Al核磁田共振谱的分析,认为氢键生成是胶结本质。     

Special IR properties of palladium nanoparticles and their aggregations in CO molecular probe infrared spectroscopy

Dispersed Pd nanoparticles (Pdn) have been synthesized by reducing H2PdCI4 with ethanol, and stabilized using poly(vinylpyrrolidone) (PVP). The Pdn is applied to the glassy carbon substrate to form a thin film, and then the potential cyclic scanning at 50 mV.s^-1 from -0.25 to 1.25 V was carried out for about 30 min to form the aggregations of Pdn (Pdn^ag). FTIR spectroscopy of both transmission and reflection modes was employed to study CO adsorption on Pdn and Pdn^ag in both solidlliquid and solidlgas interfaces. It has been revealed that CO adsorption on Pdn film yields two IRbands near 1964 and 1906 cm-1, which are assigned to IR absorption of CO bonded on asymmetric and symmetric bridge sites, respectively. In contrast to the IR properties of CO adsorbed on Pdn, only species of CO bonded on asymmetric bridge sites was determined on Pdn^ag, and the direction of the IR band near 1963 cm^-1 is completely inverted. The full width at half-maximum (FWHM) of the COB^as band near 1964 cm^-1 is measured to be 14 cm^-1 on Pdn film, while it is 24 cm^-1 on Pdn^ag film. The results of the present study demonstrated that the inverting of the IR band direction is a general phenomenon that is closely related to the interaction between nanoparticles in aggregation of Pdn.     

混凝土施工缝留置位置与处理

砼施工缝留置原则运用于结构受剪力较小且便于施工的部位,但在施工中技术人员应根据砼构件的受力分析,重点结合《规范》条款规定的构件位置正确理解留置施工缝,并检测施工缝处砼强度后继续浇筑后续砼。     

河南省石人山自然保护区针阔叶混交林群落生态特征(Ⅱ)(续完)

采用法瑞学派植被生态学的研究方法,在确定群落最小面积的基础上设置典型样地研究了石人山自然保护区油松 锐齿栎混交林、油松 短柄枹混交林等针阔叶混交林的生境特征和群落的基本生态学特征,为自然保护区管理和植物群落生物多样性的保护提供了科学理论依据.     

自动调线机控制系统选针器定位的实现

设计了一种基于单片机的自动调线机控制系统,介绍了系统的各个组成部分及工作原理,详细设计了增量式旋转编码器对自动调线机的选针器准确定位的方法,实例证明该定位方法能够使系统准确、稳定地工作。     

摆线针轮行星减速器的变形计算

针齿销和柱销是摆线针轮行星减速器中易变形的零件。文章根据针齿销和柱销的结构及受载情况 ,应用材料力学的分析方法 ,得出其简化的力学模型及弯曲变形的挠曲线方程、转角方程 ,进而求出最大挠度及最大转角 ,建立了刚度条件。文中还对针齿销和柱销的弯曲变形对整机的扭转变形的影响进行了分析 ,求出了整机的扭转变形。     

灌注桩施工过程中砼试件留置数量的探讨

本文结合工程实例,分析了灌注桩试块留置数量差异的原因,结合以前施工经验,提出本工程灌注桩的砼试块留置的办法,并对《建筑地基基础工程质量验收规范》提出合理化建议。     

不保留式留置针在宫颈癌化疗中对血管保护的对比研究

目的：通过应用不保留式留置针,观察其对宫颈癌患者化疗时血管的保护作用。方法：选取宫颈癌初次化疗患者60例,随机分为对照组和实验组各30例。结果：实验组患者静脉炎发生率和液体外渗情况均低于对照组。结论：不保留式留置针可以对化疗中得血管起到很好的保护作用,应在临床上推广使用。     

黑龙江省大亮子河森林公园8种白腐真菌的培养特性研究

对黑龙江省大亮子河森林公园天然林进行了全面调查,采集鉴定8种大亮子河森林公园针叶林、阔叶林以及针阔混交林中常见的白腐真菌。它们是盘拟层孔菌、蔷红拟层孔菌、环纹革盖菌、全缘孔菌、小刺猴头、黄白卧孔菌、烟色刺耳和变红栓菌。