One-pot Synthesis of 2, 5-Disubstituted Oxazoles Using Poly[styrene（iodosodiacetate）]

2,5-Disubstituted oxazoles were prepared conveniently by treatment of aromatic α-methyl ketones and nitriles with poly[styrene(iodosodiacetate)] in one-pot process.     

Novel Chiral Ferrocenyl Aziridino Alcohol Catalysts Promoting Asymmetric Addition of Diethylzinc to Aldehydes

Optically active aziridino alcohols containing ferrocenyl groups were prepared from commercially available L-threonine in excellent yields and used as catalysts to promote the asymmetric addition of diethylzinc to aryaldehydes to afford 1-arylpropanol in up to 84% enantiomeric excesses with moderate to good yields.     

Nickel Chloride Promoted Glaser Coupling Reaction in Hot Water

A Glaser coupling reaction of terminal alkynes in the presence of nickel chloride withoutany organics and bases in hot water has been developed, which produces the correspondinghomo-coupling products in good yields.     

Crystal Structures of Two Potential Tumor Imaging Agents and Therapeutic Agents Copper（Ⅱ） Ternary Complexes with Salicylidene-tyrosinato Schiff Base and Nitrogen-donor Chelating Lewis Base

The crystal structures of two potential tumor imaging agents and therapeutic agents -copper(Ⅱ) complexes with salicylidene-tyrosinato Schiff base and nitrogen-donor chelating Lewis base, [Cu(sal-tyr)(bipy)] 1 and [Cu(sal-tyr)(phen)]2CH3OH 2 are presented. Our work is helpful to get deep understanding of novel 64Cu tumor imaging agents and therapeutic agents.     

多小波子空间上的单小波表示

本文在较弱的条件下,建立了2重多小波子空间与单小波子空间的关系.即由2重多小波构造出单小波.一方面,这种单小波的平移伸缩与2重多小波的平移伸缩生成的子空间是完全相同的;另一方面,它具有插值性.因此通过构造出的单小波建立了多小波子空间上的Shannon型采样定理.     

2003年普通高等学校招生全国统一考试数学（理工农医类）（北京卷）

参考公式与文科相同一 选择题 :本大题共 1 0小题 ,每小题 5分 ,共 5 0分 .在每小题给出的四个选项中 ,只有一项是符合题目要求的 .( 1 ) ,( 2 )与文科 ( 1 ) ,( 2 )相同( 3)“cos2α=- 32 ”是“α=kπ+ 5π1 2 ,k∈Z”的(A)必要非充分条件(B)充分非必要条件(C)充分必要条件(D)既非充分又非必要条件( 4 )与文科 ( 4 )相同( 5 )极坐标方程 ρ2 cos2θ- 2 ρcosθ =1表示的曲线是(A)圆 (B)椭圆(C)抛物线 (D)双曲线( 6) ,( 7) ,( 8)分别与文科 ( 6) ,( 7) ,( 9)相同( 9)若数列 {an}的通项公式是an =3-n+ 2 -n+ ( - 1 ) n( 3-n- 2 -n)2 ,n…     

两个回归函数相等的Bootstrap检验

两个回归参数相等性检验一直是统计界感兴趣的问题之一．在这篇文章中，四个检验统计量被用于度量两曲线的差异，在原假设下统计量的分布采用向量数据的重复抽样来逼近，并给出了—些模拟结果．     

如何在大学数学课堂教学中培养学生创新思维

论述了在大学数学课堂教学中传授数学思想与数学方法的必要性与重要性 ,重点介绍了作者从大学数学教学中总结出来的一些数学思想与教学方法 .     

Multiple Scattering Effects of Ag Particles in Random Ag-SiN Film

A layer of 40nm-thick Ag-SiN film with Ag nano-particles embedded and distributed randomly in the SiN thin film were deposited by the method of radiant-frequency magnetron sputtering. Specimens orderly comprising a random Ag-SiN film and an optical phase change recording layer were exposed to a focused laser beam with wavelength of 69Ohm. It is shown that, with a random Ag-SiN layer deposited above the recording layer. Calculation by the finite difference time domain method of a 4Ohm-thick SiN film under a Gaussian beam irradiation has been carried out to simulate the near-field distribution in the film, which showed a huge local near-field intensity enhancement of about 200 times if small Ag particles with diameter of 6 nm were modelled inthe SiN film in the central region of the in cident laser spot.     

A Continuation Method of Parameter Inversion for Non-Equilibrium Convection-Dispersion Equation

Based on the homotopy mapping, a globally convergent method of parameter inversion for non-equilibrium convection-dispersion equations （CDEs） is developed. Moreover, in order to further improve the computational efficiency of the algorithm, a properly smooth function, which is derived from the sigmoid function, is employed to update the homotopy parameter during iteration. Numerical results show the feature of global convergence and high performance of this method. In addition, even the measurement quantities are heavily contaminated by noises, and a good solution can be found.