Relative versions of some star-selection principles

We introduce some relative versions of star selection principles first considered in [5], [11]. Some of the work extends results from [4], [5] and gives some examples.      

向量变分不等式的严格可行性问题

本篇文章首先定义了向量变分不等式的严格可行点概念,其次在假设了映射是强(D)-伪单调的情况下,证明了向量变分不等式解集非空有界与其严格可行点存在的等价性问题,推广了在数量变分不等式上得到的相应结果．     

Ultra <Emphasis Type="Italic">LI</Emphasis>-ideals in lattice implication algebras and <Emphasis Type="Italic">MTL</Emphasis>-algebras

A mistake concerning the ultra LI-ideal of a lattice implication algebra is pointed out, and some new sufficient and necessary conditions for an LI-ideal to be an ultra LI-ideal are given. Moreover, the notion of an LI-ideal is extended to MTL-algebras, the notions of a (prime, ultra, obstinate, Boolean) LI-ideal and an ILI-ideal of an MTL-algebra are introduced, some important examples are given, and the following notions are proved to be equivalent in MTL-algebra: (1) prime proper LI-ideal and Boolean LI-ideal, (2) prime proper LI-ideal and ILI-ideal, (3) proper obstinate LI-ideal, (4) ultra LI-ideal. This work was supported by the Zhejiang Provincial Natural Science Foundation of China (Grant No. Y605389) and K. C. Wong Magna Fund in Ningbo University.     

试就猝死病例谈中老年教职工保健工作

本文报告5例心性猝死(3例为冠心病性猝死),年龄为39—69岁。认为冠心病是中老年教职工猝死的主要原因,因而提出学校对他们的保健重点应放在防治冠心病上。     

Electronic structure and vibrational spectra of cis-diammine(orotato)platinum(II), a potential cisplatin analogue: DFT and experimental study

Orotic acid (vitamin B₁₃) is a key intermediate in biosynthesis of the pyrimidine nucleotides in living organisms, moreover, it may serve as the biological carrier for some metal ions. cis-Diammine(orotato)platinum(II), cis-[Pt(C₅H₂N₂O₄)(NH₃)₂] can be considered as a new potential cisplatin analogue. The FT-Raman and FT-IR spectra of the title complex are reported, for the first time. The molecular structure, vibrational frequencies, and the theoretical infrared and Raman intensities have been calculated by the density functional mPW1PW91 method. The detailed vibrational assignment has been made on the basis of the calculated potential energy distribution. The theoretically predicted IR and Raman spectra show very good agreement with experiment. Natural bond orbital (NBO) analyses were performed for cisplatin, carboplatin and the title complex. The results provided new data on the nature of platinum–ligand bonding in these compounds. Strong intramolecular hydrogen bond between the orotate ligand and the coordinated ammonia group stabilizes the structure of the platinum(II) complex. Thus, it is suggested that the orotate ligand in the title complex is more inert to the substitution reactions than the chloride ligands in cisplatin.     

在Triton X—100存在下,用2-(5-溴-2-吡啶偶氮)-5-二乙胺基苯酚(5-Br-PADAP)分光光度测定方钍石中的钍

方钍石是钍来源的重要含钍矿物。目前测定钍的含量的方法较多,虽有用5-Br-PADAP测定钍的方法的报导,但未见有在triton X-100存在下,用5-Br-PADAP直接测定方钍石中钍的含量的报导。Triton X-100的存在,使测定的酸度增加,从而增加干扰元素的干扰比;并且增加了络合物的稳定时间。本文采用5-Br-PADAP作显色剂,在氯乙酸-氯乙酸钠缓冲体系中用triton X-100表面活性剂胶束增溶分光光度测定方钍石(人工样品)中钍的含量,获得较满意的结果。在25毫升中,钍的比耳定律范围在0～20微克,摩尔吸光系数为5.2×10~4升·摩尔~(-1)·厘米~(-1),Sandell灵敏度为0.0045微克钍(IV)/厘米~2。我们对两种含量的方钍石人工样品进行了测试,结果良好,回收率在97.3～101.4％之间,此方法可靠,精密度较高,误差符合微量组分的测定要求,我们对样品测定结果表示满意。     

Irn(n=2-25)团簇基态结构的遗传算法研究

用遗传算法结合Gupta紧束缚模型势研究了Irn(n=2-25)团簇的基态结构.分析了Irn(n=2-25)团簇的基态结构随团簇尺寸的变化规律.计算结果表明,Irn(n=2-25)团簇的每个原子的平均束缚能和平均第一近邻随团簇尺寸的增加而增大,以总束缚能的二阶差分为判据,Irn(n=2-25)团簇的幻数是4、7、9、13、15、19、23.     

26Al的加速器质谱测量及其应用

26Al是一个在多个学科都非常有意义的放射性核素。主要介绍了国内外在利用加速器质谱技术测量26Al时所开展的各种测量方法、各自的优缺点和测量灵敏度，并介绍了目前利用^26Al在地球科学、生物医学、核物理以及天体物理等诸多方面的应用研究工作。     

Finite element error estimates for non-linear elliptic equations of monotone type

Summary In this paper we shall consider the application of the finite element method to a class of second order elliptic boundary value problems of divergence form and with gradient nonlinearity in the principal coefficient, and the derivation of error estimates for the finite element approximations. Such problems arise in many practical situations — for example, in shock-free airfoil design, seepage through coarse grained porous media, and in some glaciological problems. By making use of certain properties of the nonlinear coefficients, we shall demonstrate that the variational formulations associated with these boundary value problems are well-posed. We shall also prove that the abstract operators accompanying such problems satisfy certain continuity and monotonicity inequalities. With the aid of these inequalities and some standard results from approximation theory, we show how one may derive error estimates for the finite element approximations in the energy norm.     

正丁基苝四羧酸二酰亚胺的晶型和性能研究

文章合成了N,N'-二正丁基苝四羧酸二酰亚胺,并纯化、调晶,进行了IR、元素分析、X射线等测定.分析该化合物在DMF中的紫外光谱(最大吸收波长524.80 nm)、荧光光谱(最大发射波长539.0 nm)、Stokes位移(数值15 nm)等光谱性质.在400～700 nm范围内,α晶型薄膜紫外-可见吸收出现很强的吸收峰,且由β型变为α型,最大吸收波长有明显的红移(545 nm变为580 nm).X射线粉末衍射也反映出α晶型的2θ在26.0°处衍射峰CPS为2 508,β型在25.2°为1 891.α,β晶型作为电荷产生材料制得的功能分离型有机光导体,在光源滤波波长λ=532 nm曝光下,测得含α,β感光体达到饱和电位的时间分别为46,93.98 s,光衰电位(5.3千伏电压负充电电晕,1～2 s后的表面电位)分别为727和525 V,半衰曝光量分别为4.32,4.34μJ·cm-2,残余电位分别为30和45 V等光导性能数值.