Magnetic properties of lanthanum orthoferrite fine powders prepared by different chemical routes

Fine powders of lanthanum iron oxide, LaFeO₃, have been prepared by solid state reaction as well as sol-gel synthesis and nebulized spray pyrolysis. Structures, morphologies and magnetic susceptibility measurements of these powders have been examined. The powders prepared by all the three low-temperature routes contain nearly spherical particles with an average diameter of 40 nm. These samples show a lower Neel temperature than the powder prepared by solid state reaction besides showing much lower magnetic susceptibility at low temperatures. Dedicated to Professor C N R Rao on his 70th birthday     

Reversible 5′-end biotinylation and affinity purification of synthetic RNA

A reversible biotinylation phosphoramidite was synthesized and incorporated onto the 5′-end of an oligoribonucleotide on a solid phase synthesizer. After cleavage and deprotection, the crude synthetic oligomer mixture was incubated with NeutrAvidin^® coated microspheres, and the failure sequences removed by washing with a buffer followed by treating the microspheres with tetrabutylammonium fluoride to give a high quality unmodified full-length oligoribonucleotide.     

用通用DSP实现话带MODEM

概述了设计话带ＭＯＤＥＭ时所要考虑的基本问题。介绍了一种用通用ＤＳＰ设计的ＭＯＤＥＭ，并讨论了相应的控制程序和调制，解调程序的设计方法和结构框图，而且设计了一个简单实用的握手协议。最后，进一步分析了这种ＭＯＤＥＭ的特点和它的应用前景。     

电信网络管理的望族——TMOS

电信管理及运营支撑是爱立信公司为公用电信网提供的有关管理及运营支撑功能的综合方案，本文介绍了其中的公网管理系统和蜂窝移动网络管理系统。     

HIST: A hierarchical self test methodology for chips,boards, and systems

This article presents the HIST approach, which allows the automated insertion of self test hardware into hierarchically designed circuits and systems to implement the RUNBIST instruction of the IEEE 1149.1 standard. To achieve an optimal and throughout self testable system, the inherent design hierarchy is fully exploited. All chips and boards are provided with appropriate test controllers at each hierarchy level. The approach is able to detect all those faults, which are in the scope of the underlying self test algorithms. In this paper the hierarchical test architecture, the test controllers as well as all necessary synthesis procedures are presented. Finally a successful application of the HIST approach to a cryptography processor is described.     

话音ATM交换的实现─—ATM论坛电路仿真系列建议

近年来，随着ATM主干网络的建设和发展，研究ATM对现有通信业务的支持方式和适配技术是目前ATM技术研究的热点之一。话音ATM交换在降低话音通信成本和简化网络操作环境等方面提供了大量的技术手段，并且支持在单一网络环境中的多种综合业务传输。ATM论坛制定了电路仿真系列建议，话音ATM交换的技术已经基本成熟。文章通过对话音ATM交换在实现和优化方面的技术进行分析，并提出一种基于NativeModeATM的话音通信方式。     

Synthesis of the insect antifeedant CDE molecular fragment of 12-ketoepoxyazadiradione and related compounds

A diastereoselective synthesis of the model insect antifeedant 29 a CDE molecular fragment of 12-ketoepoxyazadiradione has been achieved in ten steps from indenone 9 in 44% overall yield. Several of the compounds obtained along the synthesis related to model compound 29 show significant antifeedant activity against Spodoptera littoralis and Spodoptera frugiperda.     

Iodine‐Catalyzed Friedlander Quinoline Synthesis under Solvent‐Free Conditions

Polyfunctional quinolines were synthesized using Friedlander method catalyzed by molecular iodine in high yields at 60 °C under solvent‐free conditions.