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921.
922.
Ralph E. Taylor-Smith Richard A. Register 《Journal of Polymer Science.Polymer Physics》1994,32(12):2105-2114
The nature and extent of phase mixing in blends of hydroxyl-functionalized polystyrene and poly(ethyl acrylate) (PS/PEA), where the driving force for mixing is hydrogen bonding, are characterized by several techniques. Small-angle x-ray scattering (SAXS) shows a reduction in average domain size with increasing functionalization level, a result also evident from scanning electron microscopy (SEM). Together, the two techniques reveal a very broad distribution of domain sizes. At high functionalization levels, both SAXS and SEM indicate a high degree of “in-domain” mixing, with little or no pure PS or PEA remaining in the blends. Mathematical modeling of dynamic mechanical thermal analysis (DMTA) data is employed to quantify this progression. Initially, mixing is primarily interfacial, but as the functionalization level increases, the mixed interphase rapidly grows to occupy the entire material. In agreement with the SAXS and SEM results, DMTA modeling shows that further increases in the functionalization level suppress the amplitude of composition variations in the sample. The onset of extensive in-domain mixing coincides with the marked changes in stress-strain behavior observed previously in these materials. © 1994 John Wiley & Sons, Inc. 相似文献
923.
Youn Tae Kim Chi Hoon Jun Jong-Tae Baek Hyung Joun Yoo Sang-Koo Chung 《Journal of Electronic Materials》1995,24(10):1413-1417
In this study, we have investigated sensitivities of the ion implanted silicon wafers processed by rapid thermal annealing
(RTA), which can reveal the variation of sheet resistance as a function of annealing temperature as well as implantation parameters.
All the wafers were sequentially implanted by the arsenic or phosphorous implantations at 40, 80, and 100 keV with the dose
level of 1014 to 2 × 1016 ions/cm2. Rapid thermal annealing was carried out for 10 s by the infrared irradiation at a temperature between 850 and 1150°C in
the nitrogen ambient. The activated wafer was characterized by the measurements of the sheet resistance and its uniformity
mapping. The values of sensitivities are determined from the curve fitting of the experimental data to the fitting equation
of correlation between the sheet resistance and process variables. From the sensitivity values and the deviation of sheet
resistance, the optimum process conditions minimizing the effects of straggle in process parameters are obtained. As a result,
a strong dependence of the sensitivity on the process variables, especially annealing temperatures and dose levels is also
found. From the sensitivity analysis of the 10 s RTA process, the optimum values for the implant dose and annealing temperature
are found to be in the range of 1016 ions/cm2 and 1050-1100°C, respectively. The sensitivity analysis of sheet resistance will provide valuable data for accurate activation
process, offering a guideline for dose monitoring and calibration of ion implantation process. 相似文献
924.
Ti扩散铌酸锂光波导特性的热固定技术 总被引:1,自引:1,他引:0
在Ti扩散铌酸锂光波导中,因光致折变效应而导致光波导特性漂移.在光波相干性的导波光学器件中,光致折变效应的影响尤为严重.本文报道了稳定光致折变效应的热固定技术实验结果;并提出在光波导特性的热固定过程中,不是H~+离子起主导作用这一看法. 相似文献
925.
Visible photoluminescence (PL) of nanocrystalline silicon (nc-Si) embedded in single crystal CaF2 formed on Si(1 1 1) has been studied and the influence of ex situ rapid thermal annealing (RTA) on the surface morphology and PL spectra has been studied. It has been found that the PL intensity and uniformity was improved by RTA with appropriate temperature and short annealing time. 相似文献
926.
In this article we discuss the finite element discretization of the two-dimensional, incompressible, and turbulent boundary layers. The formulation of the momentum equation is essentially due to Baker and Soliman [1] with some modifications.The versatility and the accuracy of the method is established by considering several test cases. The predictions are satisfactory and compare favorably with alternative numerical techniques. 相似文献
927.
分析了制作高功率连续激光反射镜材料的热性能、缺陷及其加工工艺, 提出了制作高功率激光反射镜应考虑的几个关键问题: 反射镜材料的综合热性能比值S, 材料的微观结构、缺陷的大小和晶向的选择, 以及加工工艺的设计。并介绍了实验结果。 相似文献
928.
Naren Noolu Nikhil Murdeshwar Kevin Ely John Lippold William BaeslackIII 《Journal of Electronic Materials》2004,33(4):340-352
Gold-aluminum ball bonds were thermally exposed at constant elevated temperatures, and the resultant phase transformations
studied in detail. The as-bonded microstructure of a Au-Al ball bond essentially consisted of a reaction zone (termed “alloyed
zone” (AZ) in the as-bonded condition) between the Au bump and the bonded Al metallization. It is the growth of the reaction
zone between the Au bump and the bonded Al metallization and also the nonbonded Al metallization during thermal exposure that
gave rise to the various phase transformations. Au4Al, Au8Al3, and Au2Al are the predominant phases that grew across the ball bond until the bonded Al metallization is available to take part in
the interdiffusion reactions. After the complete consumption of the bonded Al metallization, the Au-Al phases reverse transformed
resulting in the formation of the Au4Al phase in the entire reaction zone across the ball bond (RZ-A). The lateral interdiffusion reactions resulted in the nucleation
and the growth of all of the Au-Al phases given by the phase diagram. Kidson’s analysis and Tu et al.’s treatment were extended
to a five-phase binary system to explain the phase transformations in thermally exposed Au-Al ball bonds. It is possible for
all of the Au-Al phases to grow across a ball bond uninhibited as long as the bonded metallization is available. However,
the supply limitation of the bonded metallization gives rise to reverse transformations where Al-rich phases transform to
Au-rich phases and eventually result in the formation of the Au4Al phase in the entire RZ-A. If infinite time is allowed, Au4Al would dissolve; the extent of which is dependent on the solubility of Al in Au. No supply of Au lateral to the bond causes
the reverse transformation of the Au4Al phase, giving rise to the lateral growth of the remaining Au-Al phases. If infinite time is allowed, the lateral phase
transformations would result in the formation of a phase that is dependant on the relative proportion of Au and Al present
in the nonbonded metallization (NBM) and Au4Al below the void line. Hence, the presence of a phase in a particular location of a ball bond is dependent on the time and
temperature of thermal exposure. 相似文献
929.
单层结构白色聚合物电致发光器件制备及其性能 总被引:7,自引:4,他引:3
选择梯形对次苯基聚合物(I.PPP)为母体和蓝色发光材料,掺杂MEH-PPV、OXD-7、PMMA分别作为橙红色发光材料、电子传输材料和绝缘介质材料,用旋涂法制成结构为ITO/白色发光层/A1的单层白色有机发光器件。对器件进行热处理(最佳热处理条件为180℃,1h)后,发现器件的发光性能得到明显改善。驱动电压25V时器件的发光亮度由42cd/m^2提高到355cd/m^2,色坐标为(x=0.332,y=0.347),非常接近于白色等能点。 相似文献
930.