基于P-V双因素的网络激光标刻性能研究

传统激光标刻技术已在实际工业生产中普遍应用,但其系统最优标刻性能控制参数存在寻找及设置较为困难、繁琐等问题。针对该问题,本文设计了一种基于嵌入式网络激光标刻模式的新型激光标刻控制模型,并在该模型下通过相关数据预处理算法分析单一标刻影响因素对激光标刻性能的影响;再通过对实验数据的数理统计分析得出二值图像的标刻性能变化规律,最终得出在该材质及类似组成工件下的激光标刻的最优参数快速选择模型和性能最优值域。研究结果表明,该模型为最优激光标刻性能控制参数的快速选择提供了可靠的方法,为进一步研究激光标刻性能影响参数提供了重要参考。     

Structural,optical, and photocatalytic properties of the spray deposited nanoporous CdS thin films; influence of copper doping,annealing, and deposition parameters

Nanoporous thin films of Cd_1−xCu_xS (0≤x≤0.06) were grown on a heated glass substrate employing a home-made spray pyrolysis technique. The influences of [Cu]/[Cd] and the annealing in the range 300–500 °C on the structural and morphological properties of the films were investigated by X-ray diffraction (XRD), Fourier transformation infrared spectroscopy (FTIR), field emission scanning electron microscope (FE-SEM) and atomic force microscopy (AFM). The influences of Cu doping ratio, solution flow rate, and the deposition time on the optical properties and photocatalytic activity of these films are also reported. The films are of polycrystalline nature and hexagonal structure. Increasing the Cu doping ratio and annealing temperature improve the (1 0 1) preferential orientation. The crystallite size is ranged from 23.82 to 32.11 nm. XRD and FTIR reveal the formation of CdO in the 6% Cu-doped CdS film annealed at 400 °C and in all films annealed at 500 °C. The pure CdS film is of a porous structure and the close-packing and porosity of the films increase with increasing Cu%. Also, the pore diameter can be controlled from 50 to 15 nm with the increase of Cu content. The films showed transmittance below 70%. The optical band gap of the films is decreased from 2.43 to 1.82 eV with increasing Cu% and flow rate/deposition time. Additionally, the refractive indices and dispersion parameters of the films are also affected by the deposition conditions. Cu doping enhanced the films' photostability as well as the photocatalytic removal of methylene blue (MB).     

基于合成规则的相似性推理及其在焊接参数设计中的应用

焊接过程是典型的复杂过程,应用模糊逻辑建立焊接参数推理系统可快速实现焊接工艺参数设计.近似推理机制是模糊系统研究和开发中的一个重要组成部分,在现有的相似性推理方法的基础上,融合经典的合成规则推理技术,提出一种新的基于合成规则的相似性推理方法.以CO_2保护焊焊接规范参数设计为背景介绍模糊推理在焊接领域的应用,运行结果表明,采用方法建立的模糊推理模型具有较高的推算精度,能够满足焊接工艺参数设计的要求.     

基于层次分析的主成分分析法及其应用

在分析了传统的层次分析法和主成分分析法的优缺点的基础上,扬长避短的将两种方法结合在一起,讨论了基于层次分析的主成分分析法.与新兴的决策评估方法相比,例如直觉模糊层次分析法,基于层次分析的主成分分析法更具有简洁性和直观性.最后,将方法应用于登陆作战的目标选择,得到了与实战结果相同的结论,验证了方法的可行性.     

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??In this paper, we estimate parameters of gamma life distribution and normal life distribution by EM algorithm based on Type-II hybrid censored data. The covariance matrices are derived as well. Some numerical examples are also presented for illustration.     

N_2O分解催化剂Co-Al尖晶石型复合氧化物制备参数的优化

以柠檬酸为配合剂,用溶胶-凝胶法制备了一组不同组成的Co-Al复合氧化物(CoAl_2O_4、CoCo0.5Al1.5O4、CoCoAlO_4、CoCo_(1.5)Al_(0.5)O_4、Co_3O_4),用于催化分解N_2O.用N_2物理吸附、X射线衍射(XRD)、扫描电镜(SEM)、H2程序升温还原(H2-TPR)、X射线光电子能谱(XPS)等技术对催化剂进行了结构表征,考察了复合氧化物组成、母液pH值、配合剂用量等制备参数对催化剂活性的影响.结果表明:用Al取代Co_3O_4中部分Co制备Co-Al复合氧化物,提高了催化剂的比表面积和催化活性,其中组成为CoCo_(1.5)Al_(0.5)O_4、母液pH=2、柠檬酸/金属离子(摩尔比)为1的催化剂活性较高.在CoCo_(1.5)Al_(0.5)O_4表面浸渍K2CO3溶液制得K改性催化剂,弱化了钴-氧化学键,提高了催化活性.其中0.02K/CoCo1.5Al0.5O4催化剂在有氧有水气氛400℃连续反应50h,N_2O转化率达97.1%.     

On the optimal parameters of GMSSOR method for saddle point problems

For solving saddle point problems, SOR-type methods are investigated by many researchers in the literature. In this short note, we study the GMSSOR method for solving saddle point problems and obtain the optimal parameters which minimize the spectral (or pseudo-spectral) radii of the iteration matrices.     

单入射波长及纤芯存在光致双折射的长周期光纤光栅的折射率传感分析

利用全矢量耦合模方程提出并分析了一种基于纤芯存在光致双折射的长周期光纤光栅的环境折射率传感测量方法.以波长为谐振波长的完全偏振光为入射波,通过分析不同环境折射率下输出光的偏振态在邦加球上与参考点间球面距离的变化测量环境折射率.分析表明,在环境折射率1～1.30范围内包层半径为20.75 μm的长周期光纤光栅传感器线性特性良好,灵敏度为0.356/RIU,可应用于湿度和气体的折射率测量;该分析方法适用于其他类型的双折射长周期光纤光栅传感器的设计.     

改进的孔隙模型评价流体性质与裂缝孔隙度

随着勘探开发的不断深入,渤海油田面临越来越多的疑难储层,这类储层流体性质识别与裂缝孔隙度评价成为测井评价的难点。本文依据Biot理论,描述了存在裂隙条件下的含裂隙Biot理论,形成改进的孔隙介质模型。根据该模型利用阵列声波测井数据进行反演得到裂缝孔隙度,同时通过流体置换,得到不同流体对应的岩石体积模量,对其进行交会判别流体性质,实现了阵列声波测井裂缝孔隙度定量评价与流体性质识别综合应用。利用该模型对渤海油田十几口井进行计算,结果表明该方法对于常规砂泥岩和复杂岩性储层均能取得较好效果,本文提出的储层流体性质识别与裂缝孔隙度评价方法,有助于扩展阵列声声波测井的应用范围。     

Effect of non-acoustic parameters on heterogeneous sonoporation mediated by single-pulse ultrasound and microbubbles

Sonoporation—transient plasma membrane perforation elicited by the interaction of ultrasound waves with microbubbles—has shown great potential for drug delivery and gene therapy. However, the heterogeneity of sonoporation introduces complexities and challenges in the realization of controllable and predictable drug delivery. The aim of this investigation was to understand how non-acoustic parameters (bubble related and bubble-cell interaction parameters) affect sonoporation. Using a customized ultrasound-exposure and fluorescence-imaging platform, we observed sonoporation dynamics at the single-cell level and quantified exogenous molecular uptake levels to characterize the degree of sonoporation. Sonovue microbubbles were introduced to passively regulate microbubble-to-cell distance and number, and bubble size. 1 MHz ultrasound with 10-cycle pulse duration and 0.6 MPa peak negative pressure were applied to trigger the inertial collapse of microbubbles. Our data revealed the impact of non-acoustic parameters on the heterogeneity of sonoporation. (i) The localized collapse of relatively small bubbles (diameter, D < 5.5 μm) led to predictable sonoporation, the degree of which depended on the bubble-to-cell distance (d). No sonoporation was observed when d/D > 1, whereas reversible sonoporation occurred when d/D < 1. (ii) Large bubbles (D > 5.5 μm) exhibited translational movement over large distances, resulting in unpredictable sonoporation. Translation towards the cell surface led to variable reversible sonoporation or irreversible sonoporation, and translation away from the cell caused either no or reversible sonoporation. (iii) The number of bubbles correlated positively with the degree of sonoporation when D < 5.5 μm and d/D < 1. Localized collapse of two to three bubbles mainly resulted in reversible sonoporation, whereas irreversible sonoporation was more likely following the collapse of four or more bubbles. These findings offer useful insight into the relationship between non-acoustic parameters and the degree of sonoporation.