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71.
含k-次增生算子的Ishikawa迭代的收敛性问题 总被引:9,自引:0,他引:9
主要研究了非线性方程x Tx=f的Ishikawa迭代解.其中T为k-次增生的或增生的,并在一致光滑和任意的实Banach空间分别研究了上述方程的带误差的Ishikawa迭代解,从而推广了已知的一些结果。 相似文献
72.
Padma Gopalan Xuefa Li Mingqi Li Christopher K. Ober Chad P. Gonzales Craig J. Hawker 《Journal of polymer science. Part A, Polymer chemistry》2003,41(22):3640-3656
A modular approach has been developed for the synthesis of rod–coil block copolymers involving the initial preparation of a macroinitiator based on the rod block followed by the growth of the coil segment with living free-radical procedures. The key feature of this strategy is the utilization of an alkoxyamine group from the beginning of the synthesis, which serves as a solubilizing group and ensures that each rod block contains a single initiating fragment. Using this approach permits block copolymers based on insoluble biphenyl ester oligomers to be conveniently prepared with coil segments that range from styrenes to acrylates to 1,3-dienes. The tendency of the rod segments to crystallize is strongly dependent on the weight fraction of the rod segment and the chemical nature of the coil segment. Rod–coil molecules containing at least 25–35 wt % polystyrene or poly(n-butyl acrylate) coil segments show a two-dimensional hexagonal arrangement of rod aggregates, as characterized by transmission electron microscopy and small-angle X-ray scattering. Polyisoprene block copolymers exhibit a lamellar microstructure with short rigid domains in which the rod units lie in an interdigitated smectic C arrangement. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 3640–3656, 2003 相似文献
73.
Xiaohua He Hailiang Zhang Deyue Yan Xiayu Wang 《Journal of polymer science. Part A, Polymer chemistry》2003,41(18):2854-2864
A series of side‐chain liquid‐crystalline (LC) homopolymers of poly[6‐(4‐methoxy‐4′‐oxy‐azobenzene) hexyl methacrylate] with different degrees of polymerization were synthesized by atom transfer radical polymerization (ATRP), which were prepared with a wide range of number‐average molecular weights from 5.1 × 103 to 20.6 × 103 with narrow polydispersities of around 1.17. Thermal investigation showed that the homopolymers exhibit two mesophases, a smectic phase, and a nematic phase, and the phase‐transition temperatures of the homopolymers increase clearly with increasing molecular weights. A series of novel LC coil triblock copolymers with narrow polydispersities was synthesized by ATRP, and their thermotropic phase behavior was investigated with differential scanning calorimetry and polarized optical microscopy. The LC coil triblocks were designed to have an LC conformation of poly[6‐(4‐methoxy‐4′‐oxy‐azobenzene) hexyl methacrylate] with a wide range of molecular weights from 3.5 × 103 to 1.7 × 104 and the coil conformation of poly(ethylene glycol) (PEG) (number‐average molecular weight: 6000 or 12,000) segment. Their characterization was investigated with 1H NMR, Fourier transform infrared spectra, and gel permeation chromatography. Triblock copolymers exhibited a crystalline phase, a smectic phase, and a nematic phase. The phase‐transition temperatures from the smectic to nematic phase and from the nematic to isotropic phase increased, and the crystallization of PEG depressed with increasing molecular weight of the LC block. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 2854–2864, 2003 相似文献
74.
In this paper, the authors obtain the endpoint estimates for a class of non-standard commutators with higher order remainders and their variants. Moreover, the authors show that these operators are actually not bounded in certain cases.
75.
76.
In this paper we investigate the
probabilistic linear $(n,\delta)$-widths and $p$-average linear
$n$-widths of the Sobolev space $W^r_2$ equipped with the Gaussian
measure $\mu$ in the $L_{\infty}$-norm, and determine the
asymptotic equalities
\begin{eqnarray*}
\lambda_{n,\delta}(W^r_2,\mu,L_{\infty})
&\asymp&\frac{\sqrt{\ln
(n/\delta)}}{n^{r+(s-1)/2}},\\[3pt]
\lambda^{(a)}_n(W^r_2,\mu,L_{\infty})_p &\asymp&\frac{\sqrt{\ln
n}}{n^{r+(s-1)/2}}, \qquad 0 < p < \infty.
\end{eqnarray*} 相似文献
77.
Hydrophilic segmented block copolymers based on poly(ethylene oxide) and monodisperse amide segments
Debby Husken Jan Feijen Reinoud J. Gaymans 《Journal of polymer science. Part A, Polymer chemistry》2007,45(19):4522-4535
Segmented block copolymers based on poly(ethylene oxide) (PEO) flexible segments and monodisperse crystallizable bisester tetra‐amide segments were made via a polycondensation reaction. The molecular weight of the PEO segments varied from 600 to 4600 g/mol and a bisester tetra‐amide segment (T6T6T) based on dimethyl terephthalate (T) and hexamethylenediamine (6) was used. The resulting copolymers were melt‐processable and transparent. The crystallinity of the copolymers was investigated by differential scanning calorimetry (DSC) and Fourier Transform infrared (FTIR). The thermal properties were studied by DSC, temperature modulated synchrotron small angle X‐ray scattering (SAXS), and dynamic mechanical analysis (DMA). The elastic properties were evaluated by compression set (CS) test. The crystallinity of the T6T6T segments in the copolymers was high (>84%) and the crystallization fast due to the use of monodisperse tetra‐amide segments. DMA experiments showed that the materials had a low Tg, a broad and almost temperature independent rubbery plateau and a sharp flow temperature. With increasing PEO length both the PEO melting temperature and the PEO crystallinity increased. When the PEO segment length was longer than 2000 g/mol the PEO melting temperature was above room temperature and this resulted in a higher modulus and in higher compression set values at room temperature. The properties of PEO‐T6T6T copolymers were compared with similar poly(propylene oxide) and poly(tetramethylene oxide) copolymers. © 2007 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 45: 4522–4535, 2007 相似文献
78.
一种PN码自适应捕获门限的改进算法 总被引:1,自引:0,他引:1
文献[1]提出了一种用于直扩系统的PN码自适应门限算法。但该文献也指出,此算法对门限总数十分敏感。当门限总数设置不当时,系统的平均捕获时间将显著增加。这限制了该算法在实际中的应用。本文就此提出了改进,给出了算法及电路框图。仿真结果表明,与原方案相比,改进算法改善了对门限总数的敏感性,降低了PN码平均捕获时间。 相似文献
79.
ROI-based Watermarking Scheme for JPEG 2000 总被引:1,自引:0,他引:1
Yu-Cheng Fan Arvin Chiang Jan-Hung Shen 《Circuits, Systems, and Signal Processing》2008,27(5):763-774
A new region of interest (ROI)-based watermarking method for JPEG 2000 is presented. The watermark is embedded into the host
image based on the characteristics of the ROI to protect rights to the images. This scheme integrates the watermarking process
with JPEG 2000 compression procedures. Experimental results have demonstrated that the proposed watermark technique successfully
survives JPEG 2000 compression, progressive transmission, and principal attacks. 相似文献
80.
Vitali Vogel Jean‐Franois Gohy Bas G. G. Lohmeijer Jacomina A. Van Den Broek Winfried Haase Ulrich S. Schubert Dieter Schubert 《Journal of polymer science. Part A, Polymer chemistry》2003,41(20):3159-3168
In aqueous solutions, amphiphilic block copolymers in which a polystyrene (PS) segment is connected to a poly(ethylene oxide) (PEO) block via a bis(2,2′:6′,2″‐ terpyridine ruthenium) complex can form micelles. Such micelles of the protomer type PS20‐[Ru]‐PEO70, according to the preparation procedure representing frozen micelles, were studied by sedimentation velocity and sedimentation equilibrium analysis in an analytical ultracentrifuge and by transmission electron microscopy, with different techniques applied for the sample preparation. The particles obtained were surprisingly multifarious in size. In ultracentrifugation experiments performed at relatively low salt concentrations, the distributions of the sedimentation coefficient s20,w showed a pronounced peak at 9.6 S and a broad, only partly separated second peak around 14 S. The molar mass of the particles at the peak was around 430,000 g/mol, corresponding to an aggregation number of approximately 85. The average hydrodynamic diameter of the particles in the peak fraction was approximately 13 nm. In electron micrographs of negatively stained samples, spheres of diameters between 10 and 25 nm were the most abundant particles, but larger ones with a wide size range were also visible. The latter particles apparently were composed of smaller ones. The data from both sedimentation analysis and electron microscopy showed that (1) the studied compound formed primary micelles of diameters around 20 nm and (2) the primary micelles had a tendency toward aggregation. © 2003 Wiley Periodicals, Inc. J Polym Sci Part A: Polym Chem 41: 3159–3168, 2003 相似文献