单晶生长用AlN粉料的烧结提纯工艺实验研究

使用自主研发的钨系统中频感应加热炉对AlN粉料进行了烧结提纯处理实验,并用XRD、SEM、IGA和GDMS等表征方法分析了烧结后的样品.实验发现,高温(2 250℃)长时间(50 h)烧结提纯工艺效果显著,但AlN粉料损耗高达47.37％;而低温(小于2 000℃)分段式短时间(每段10h)烧结提纯工艺粉料损耗低于2％,但是提纯效果一般.通过对实验结果的综合分析,提出了一种AlN粉料烧结提纯的改进工艺,最终得到了氧含量仅238 ppm、碳含量135 ppm的高质量AlN单晶生长原料,并且显著增加了原料的利用率.     

A System for Determination of Precise Isotopic Vapor Pressure Differences from —20 to 110 °C,including Temperature Control to 0·001 over that Range)

An experimental system for the precise measurement of small vapor pressure differences over the range —20 to 110°C is described.     

电器设备泄漏电流检测及相关要求

评定电器安全性能是否可靠过程中,最重要的一个参数是泄漏电流检测.一些现代电器产品和家用电器都需要较高的安全级别作为保障,因此,进行电器设备泄漏电流检测变得尤其重要.参考相关资料以及一些实践型的电器检验工作,本文将从电器设备泄漏电流检测的各个环节入手展开细致的研究,并总结经验.     

Schnell-Methode zur Umsetzung von Kohlenwasserstoffen zu Wasserstoff für die Isotopenanalyse

Es wird eine weiterentwickeltes, isotopenanalytisches Verfahren zur probenchemischen Umsetzung von Kohlenwasserstoffen mit Chromium zu Wasserstoff bei 1300 K vorgestellt. Die erzielten Testergebnisse zeigen anhand der gemessenen δD-Werte, daβ Quarzöfen bei diesen Temperaturen noch keine die Isotopenmeβwerte beeinflussende Diffusion von Wasserstoff durch die Wandung zulassen. Auβerdem erfolgte die Reaktion nahezu spontan und vollständig, was die Methode zeitlich sehr effektiv macht.

A modified isotope analytical method is presented for the chemical reaction of hydrocarbons with chromium at 1300 K to form hydrogen. The test results obtained (i.e. the measured δD-values) show that at this temperature quartz heating tubes do not allow hydrogen to diffuse through the wail, which fact would influence the isotopic composition. Furthermore the reaction proceeds nearly spontaneously and quantitatively, which yields an effective method, especially with respect to time.     

G伺服在光纤筛选设备中的应用

文章探讨了新型G系列伺服系统的特点,其在光纤筛选设备上的应用;光纤筛选设备的控制原理,在光纤生产环节中的作用,发挥G系列伺服优异性能,提升筛选速度提高设备的利用效率.     

Electronic Structure and Thermoelectric Properties of Si-Based Clathrate Compounds

Thermoelectric properties of Au-substituted Si-based clathrates, Ba₈AuGa₁₃Si₃₂ and Ba₆A₂AuGa _x Si_45−x (A = Sr, Eu, x = 13, 14), were experimentally and theoretically investigated. The polycrystalline samples of the Au-substituted Si-based clathrates were prepared by using the spark plasma sintering technique. The electronic structure of Ba₆A₂AuGa₁₃Si₃₂ was theoretically calculated by ab initio calculations, and the thermoelectric properties of Ba₆A₂AuGa _x Si_45−x were estimated through the calculated electronic structure. The effective mass of Ba₆A₂AuGa _x Si_45−x was experimentally estimated to be greater than that of Ba₈AuGa₁₃Si₃₂. Experimentally observed electronic properties agree with the calculations for Ba₆A₂AuGa _x Si_45−x . The maximum ZT value of Ba₆Sr₂AuGa₁₄Ge₃₁ is about 0.5 at 850 K. The calculated thermoelectric properties agree very well with the experimental results in the range from room temperature to 900 K.     

Size Effect on Properties of Varistors Made From Zinc Oxide Nanoparticles Through Low Temperature Spark Plasma Sintering

Conditions for the elaboration of nanostructured varistors by spark plasma sintering (SPS) are investigated, using 8‐nm zinc oxide nanoparticles synthesized following an organometallic approach. A binary system constituted of zinc oxide and bismuth oxide nanoparticles is used for this purpose. It is synthesized at room temperature in an organic solution through the hydrolysis of dicyclohexylzinc and bismuth acetate precursors. Sintering of this material is performed by SPS at various temperatures and dwell times. The determination of the microstructure and the chemical composition of the as‐prepared ceramics are based on scanning electron microscopy and X‐ray diffraction analysis. The nonlinear electrical characteristics are evidenced by current–voltage measurements. The breakdown voltage of these nanostructured varistors strongly depends on grain sizes. The results show that nanostructured varistors are obtained by SPS at sintering temperatures ranging from 550 to 600 °C.     

基于模糊神经网络的雷达对抗效能评估

雷达对抗装备作战效能评估是一个复杂问题,涉及因素多,而且部分因素存在信息不完全和不确定的问题,而模糊系统理论是处理这类问题的有力工具。提出利用模糊系统理论来评估雷达对抗装备的作战效能,建立了作战效能评估的指标体系,结合神经网络的自适应功能,提出了基于模糊神经网络的作战效能评估模型。仿真结果表明该方法简单有效而且可行。     

论现场总线系统及其应用技术

介绍FCS的结构、特点，及其与DCS系统的对照与集成并用。最后简述了以FCS为基础的控制系统与网络系统的构建、形成与开发，并结合我国目前的实际情况提出FCS在应用中要考虑的一些实际问题，及选择FCS的一些建议。