电磁型微电机定子绕组的研制

本文主要阐述应用微细加工技术研究和开发电磁型微电机定子绕组的制备工艺，重点介绍制备定子绕组所涉及到的各种材料及其用途。采用掩模电镀技术解决了平面工艺难以解决的线圈绕组。本研究结果为双层十七圈三对六组绕组系统。最小线宽为３μｍ，微电机直径为２ｍ，最大工作电流１２０ｍＡ，电阻值在２４－２５Ω之间。输出力矩为１．５μＮＭ，转子转速每分钟可达５００转。     

Triple quantum MQMAS spectroscopy of (I=7/2) in Na3Co(NO2)6 and trans-Co[(en2)(NO2)2]NO3 interplay between the quadrupole coupling and anisotropic shielding tensors

The purpose of this paper is to investigate the interplay between the chemical shielding anisotropy and quadrupole interaction in MQMAS spectra. in the compounds Na₃Co(NO₂)₆ and trans-Co[(en₂)(NO₂)₂]NO₃ provides model systems for such an investigation. Furthermore, only few results have been reported on the application of the MQMAS method to a spin I=7/2. The possibilities of the MQMAS spectroscopy for determining the relative orientation of the two tensors and its advantage over previous techniques are discussed. Reported experimental spectra at different spinning speeds of Na₃Co(NO₂)₆ are accurately reproduced by our theoretical simulations. The calculations are based on a recent approach, summarized in the present paper, which allows one to perform efficient simulations of MQMAS spectra including all interactions and their time-dependence throughout the experiment. This is necessary for calculating accurate MQMAS spectra including the spinning sideband pattern. In the case of trans-Co[(en₂)(NO₂)₂]NO₃ where the quadrupolar interaction and chemical shielding are stronger and their axes are non-coincident, the MQMAS spectrum is strongly distorted due to the unsufficient spinning speed and RF power. In this case, MAS at different spinning speeds is shown to provide valuable information.     

Multiple-magnetic field 139La NMR and density functional theory investigation of the solid lanthanum(III) halides

Results from a solid-state ¹³⁹La NMR spectroscopic investigation of the anhydrous lanthanum(III) halides (LaX₃; X=F, Cl, Br, I) at applied magnetic fields of 7.0, 9.4, 11.7, 14.1, and 17.6 T are presented and highlight the advantages of working at high applied magnetic field strengths. The ¹³⁹La quadrupolar coupling constants are found to range from 15.55 to 24.0 MHz for LaCl₃ and LaI₃, respectively. The lanthanum isotropic chemical shifts exhibit an inverse halogen dependence with values ranging from −135 ppm for LaF₃ to 700 ppm for LaI₃, which represents nearly half of the total lanthanum chemical shift range. The spans of the magnetic shielding tensors also vary widely, from 35 to 650 ppm for the solid LaF₃ through LaI₃. DFT calculations of the ¹³⁹La electric field gradient and magnetic shielding tensors have been performed and provide a qualitative interpretation of the trends observed experimentally.     

数字掩模制作控制系统误差特性研究

数字化掩模制作系统的核心控制部件是数字微镜。文中系统分析了数字微镜控制系统对数字化掩模制作系统精度的影响。指出误差来源主要为数字微镜帧刷新率、像素黑栅效应、像素量化和调制非线性等因素,并分别提出了相应的误差修正或补偿方法。提高系统的精缩倍数、像素分辨率以及占空比,可以降低这些误差来源的影响。     

电磁屏蔽膜设备的开发及应用

介绍了国内外对电磁屏蔽膜(EMI)研究的现状,比较了制备EMI膜的各种方法,指出采用磁控溅射法制备的EMI膜质量较好,并给出制备EMI膜的工艺流程。     

一种基于OTF稳定性的波前编码相位板优化方法

提出了一种简单的可用于光学系统中子午弧矢方向白光OTF稳定性评价的波前编码相位板参量优化方法.该方法仅以标准偏差来评价OTF在目标景深范围内的稳定性,并且结合自适应模拟退火算法在参量空间内优化得到相位板的最佳参量.使用该方法优化得到的相位板参量,可以大幅度提高光学系统的景深,并且可以获得更为清晰、稳定的成像.对应用波前编码技术前后光学系统的成像性能作了比较,并且考察了优化参量的容差性.     

地下工程中金属门非核电磁脉冲屏蔽效能研究

以圆形截面坑道为简化模型,运用旋转对称体时域有限差分法将三维问题转化为二维问题处理,计算了地下防护工程口部金属门对高功率微波、超宽带电磁脉冲的屏蔽效能,分析了门缝大小、门框嵌入岩土介质深度对屏蔽效能的影响,确定了场泄漏的主要途径.计算结果表明,门对坑道中不同的传输波模具有不同的屏蔽效能;泄漏场主要是通过门框的绕射进入工程内部,门缝的泄漏较小,门缝大小以及门框嵌入岩土介质的深度对屏蔽效能的影响是次要的;另外,通过门的泄漏场在工程内部迅速衰减;HPM的载频越高,UWB的脉宽越窄,门的屏蔽效能越好.最后对数值计算结果和实验测得数据进行了比较,二者吻合较好,证实了数值计算的有效性.     

13C shielding scale for MAS NMR spectroscopy

We have performed the direct measurements of ¹³C magnetic shielding for pure liquid TMS, solution of 1% TMS in CDCl₃ and solid fullerene. The measurements were carried out in spherical ampoules exploring the relation between the resonance frequencies, shielding constants and magnetic moments of ¹³C and ³He nuclei. Next the ¹³C shielding constants of glycine, hexamethylbenzene and adamantane were established on the basis of appropriate chemical shifts measured in the solid state. All the new results are free from susceptibility effects and can be recommended as the reference standards of ¹³C shielding scale in the magic angle spinning NMR experiments. Copyright © 2011 John Wiley & Sons, Ltd.     

Estimation of isotropic nuclear magnetic shieldings in the CCSD(T) and MP2 complete basis set limit using affordable correlation calculations

A linear correlation between isotropic nuclear magnetic shielding constants for seven model molecules (CH₂O, H₂O, HF, F₂, HCN, SiH₄ and H₂S) calculated with 37 methods (34 density functionals, RHF, MP2 and CCSD(T)), with affordable pcS‐2 basis set and corresponding complete basis set results, estimated from calculations with the family of polarization‐consistent pcS‐n basis sets is reported. This dependence was also supported by inspection of profiles of deviation between CBS estimated nuclear shieldings and shieldings obtained with the significantly smaller basis sets pcS‐2 and aug‐cc‐pVTZ‐J for the selected set of 37 calculation methods. It was possible to formulate a practical approach of estimating the values of isotropic nuclear magnetic shielding constants at the CCSD(T)/CBS and MP2/CBS levels from affordable CCSD(T)/pcS‐2, MP2/pcS‐2 and DFT/CBS calculations with pcS‐n basis sets. The proposed method leads to a fairly accurate estimation of nuclear magnetic shieldings and considerable saving of computational efforts. Copyright © 2013 John Wiley & Sons, Ltd.     

惯性平台系统的EMC分析与EMI设计

主要针对惯性平台系统的EMC(电磁兼容性)分析和EMI(电磁干扰)设计,给出了EMC的概念,介绍了与惯性平台系统有关的EMI源及其特点,给出了平台系统EMI的耦合途径.依据平台系统EMI的特点和耦合途径,提出了平台系统在进行地线设计、布线、滤波、屏蔽、防止静电放电等方面应遵循的准则和采取的措施.